Low-energy-consumption fiber yarn production process

文档序号:81625 发布日期:2021-10-08 浏览:42次 中文

阅读说明:本技术 一种低能耗纤维丝生产工艺 (Low-energy-consumption fiber yarn production process ) 是由 董国防 王�华 张学刚 杨国星 于 2021-06-15 设计创作,主要内容包括:本发明提供一种低能耗纤维丝生产工艺,具体涉及到纤维丝生产技术领域。本发明包括以下步骤:控制锅炉膛出口负压和锅炉运行氧量;锅炉通过排渣装置进行排渣;所述排渣装置由转动装置、连接装置、驱动装置、装渣桶和打开装置组成,所述排渣装置的下端设有安装底座。本发明提出的一种低能耗纤维丝生产工艺,能够降低电力能耗和生产成本。(The invention provides a low-energy-consumption fiber yarn production process, and particularly relates to the technical field of fiber yarn production. The invention comprises the following steps: controlling the negative pressure of the boiler furnace outlet and the boiler operation oxygen amount; the boiler carries out slag discharge through a slag discharge device; the slag discharging device consists of a rotating device, a connecting device, a driving device, a slag containing barrel and an opening device, and the lower end of the slag discharging device is provided with an installation base. The low-energy-consumption fiber yarn production process provided by the invention can reduce the electric energy consumption and the production cost.)

1. The production process of the low-energy-consumption fiber yarn is characterized by comprising the following steps of:

s1: soaking the pulp with sodium hydroxide water solution and curing agent to convert cellulose into alkali cellulose, and dissolving out hemicellulose;

s2: the alkali cellulose is squeezed to be converted into blocky alkali cellulose;

s3: crushing the blocky alkali cellulose on a crusher to form loose floccules;

s4: placing flocculent alkali cellulose in oxygen to cause oxidative cracking of the flocculent alkali cellulose and reduce the average polymerization degree;

s5: reacting the alkali cellulose in the S4 with carbon disulfide to generate cellulose xanthate;

s6: dissolving cellulose xanthate in dilute sodium hydroxide solution to obtain viscose;

s7: placing the viscose at 75 ℃ to gradually hydrolyze and saponify the sodium cellulose xanthate in the viscose, and simultaneously filtering and defoaming to remove bubbles and impurities;

s8: and (3) allowing the viscose in the S7 to pass through a spinneret orifice to form a trickle and enter an acid-containing coagulating bath, neutralizing alkali in the viscose, coagulating the trickle into a filament, and decomposing the cellulose xanthate to regenerate the hydrated cellulose.

2. The production device of the low energy consumption fiber yarn production process according to claim 1, comprising a boiler-powered slag discharge device, and is characterized in that: the slag discharging device consists of a rotating device, a connecting device, a driving device, a slag containing barrel and an opening device, and the lower end of the slag discharging device is provided with an installation base;

the driving device consists of a supporting rod, a first gear, a first chain and a motor, wherein the lower end of the supporting rod is connected with the mounting base, the first gear is rotationally connected with the supporting rod, the motor drives the first gear to rotate, and the first gear is meshed with the first chain;

the rotating device consists of a fixing plate, a second gear, a second chain and a fixing rod, wherein two ends of the fixing rod are respectively connected with the supporting rod and the fixing plate, the second gear is rotatably connected with the fixing plate, and the second gear is meshed with the second chain;

the connecting device comprises a first connecting piece, a second connecting piece, a first connecting rod, a second connecting rod, a third connecting rod, a first connecting block and a second connecting block, one end of the first connecting piece is connected with the annular end surface of the first chain, the other end of the first connecting piece is connected with one end of the first connecting rod in a rotating way, the other end of the first connecting rod is connected with one side upper end of the first connecting block in a rotating way, the lower end of the other side surface of the first connecting block is connected with one end of the second connecting rod, the other end of the second connecting rod is connected with one side upper end of the second connecting block in a rotating way, the lower end of the other side surface of the second connecting block is connected with one end of the third connecting rod, one end of the second connecting piece is connected with the annular end surface of the second chain, and the other end of the second connecting piece is connected with the third connecting rod in a rotating way, the other end of the third connecting rod is connected with the side wall of the slag containing barrel.

3. The production device of the low energy consumption fiber yarn production process according to claim 2, wherein: the slag bucket comprises a bottom plate, three coamings and a sliding plate, wherein the lower ends of the coamings are connected with the edge of the upper end of the bottom plate, and the sliding plate is connected with the coamings in a sliding manner.

4. A low energy consumption apparatus for producing a filament according to claim 3, wherein: and limiting bulges are arranged on two sides of the sliding plate.

5. The production device of the low energy consumption fiber yarn production process according to claim 4, wherein: the edge of bounding wall be equipped with spacing protruding phase-match spacing spout, spacing protruding with the tank bottom sliding connection of spacing spout.

6. The production device of the low energy consumption fiber yarn production process according to claim 2, wherein: the opening device is composed of a top rod, a sliding barrel, a spring and a roller shaft, wherein two ends of the roller shaft are respectively connected with the end part of the sliding barrel in a rotating mode, the top rod is connected with the installation base, the inner side wall of the sliding barrel is connected with the side wall of the top rod in a sliding mode, two ends of the spring are respectively connected with the inner barrel bottom of the sliding barrel and the top rod, and the opening device is arranged on the side of the slag containing barrel.

7. The production device of the low energy consumption fiber yarn production process according to claim 2, wherein: the first connecting piece with all be equipped with three protruding end on the second connecting piece, it is three protruding end all is equipped with the mounting hole.

8. The production device of the low energy consumption fiber yarn production process according to claim 2, wherein: the mounting base is provided with a reinforcing plate, the fixing rod penetrates through the reinforcing plate, the reinforcing plate is provided with an annular hole for the second connecting rod to slide, and the second connecting rod is connected with the hole wall of the annular hole in a sliding mode.

9. The production device of the low energy consumption fiber yarn production process according to claim 5, wherein: one end of the bottom plate is lower than the other end, the sliding plate and the horizontal plane form an included angle of 80 degrees, and the sliding plate is arranged above one end of the bottom plate.

Technical Field

The invention belongs to the technical field of fiber yarn production, and particularly relates to a low-energy-consumption fiber yarn production process.

Background

Viscose fiber, called viscose fiber for short, is one kind of artificial fiber. The main raw material of the viscose fiber is chemical pulp, including cotton pulp and wood pulp, and the viscose fiber is prepared by separating natural cellulose through chemical reaction and regenerating the natural cellulose.

A production method of regenerated polyester fiber (No. CN201210200380.4) discloses a production method of regenerated polyester fiber, which is to prepare the regenerated polyester fiber through esterification, copolymerization, filtration, crystallization and spinning processes. The method makes full use of waste PET, not only reduces the production cost of the polyester staple fiber, but also greatly protects the environment and saves petroleum resources, but the power consumption in the preparation process is not reduced.

In view of the above circumstances, there is a need for a low-energy fiber production process capable of reducing power consumption and production cost.

Disclosure of Invention

The invention aims to provide a low-energy-consumption fiber yarn production process which can reduce electric energy consumption and production cost.

The invention provides the following technical scheme:

a low-energy-consumption fiber yarn production process comprises the following steps:

s1: soaking the pulp with sodium hydroxide water solution and curing agent to convert cellulose into alkali cellulose, and dissolving out hemicellulose;

s2: the alkali cellulose is squeezed to be converted into blocky alkali cellulose;

s3: crushing the blocky alkali cellulose on a crusher to form loose floccules;

s4: placing flocculent alkali cellulose in oxygen to cause oxidative cracking of the flocculent alkali cellulose and reduce the average polymerization degree;

s5: reacting the alkali cellulose in the S4 with carbon disulfide to generate cellulose xanthate;

s6: dissolving cellulose xanthate in dilute sodium hydroxide solution to obtain viscose;

s7: placing the viscose at 75 ℃ to gradually hydrolyze and saponify the sodium cellulose xanthate in the viscose, and simultaneously filtering and defoaming to remove bubbles and impurities;

s8: and (3) allowing the viscose in the S7 to pass through a spinneret orifice to form a trickle and enter an acid-containing coagulating bath, neutralizing alkali in the viscose, coagulating the trickle into a filament, and decomposing the cellulose xanthate to regenerate the hydrated cellulose.

Preferably, the slag discharging device consists of a rotating device, a connecting device, a driving device, a slag containing barrel and an opening device, and the lower end of the slag discharging device is provided with a mounting base;

the driving device consists of a supporting rod, a first gear, a first chain and a motor, wherein the lower end of the supporting rod is connected with the mounting base, the first gear is rotationally connected with the supporting rod, the motor drives the first gear to rotate, and the first gear is meshed with the first chain;

the rotating device consists of a fixing plate, a second gear, a second chain and a fixing rod, wherein two ends of the fixing rod are respectively connected with the supporting rod and the fixing plate, the second gear is rotatably connected with the fixing plate, and the second gear is meshed with the second chain;

the connecting device comprises a first connecting piece, a second connecting piece, a first connecting rod, a second connecting rod, a third connecting rod, a first connecting block and a second connecting block, one end of the first connecting piece is connected with the annular end surface of the first chain, the other end of the first connecting piece is connected with one end of the first connecting rod in a rotating way, the other end of the first connecting rod is connected with one side upper end of the first connecting block in a rotating way, the lower end of the other side surface of the first connecting block is connected with one end of the second connecting rod, the other end of the second connecting rod is connected with one side upper end of the second connecting block in a rotating way, the lower end of the other side surface of the second connecting block is connected with one end of the third connecting rod, one end of the second connecting piece is connected with the annular end surface of the second chain, and the other end of the second connecting piece is connected with the third connecting rod in a rotating way, the other end of the third connecting rod is connected with the side wall of the slag containing barrel.

Preferably, the slag containing barrel consists of a bottom plate, three enclosing plates and a sliding plate, the lower ends of the enclosing plates are connected with the edge of the upper end of the bottom plate, and the sliding plate is connected with the enclosing plates in a sliding manner.

Preferably, two sides of the sliding plate are provided with limiting bulges.

Preferably, the edge of the enclosing plate is provided with a limiting sliding groove matched with the limiting protrusion, and the limiting protrusion is in sliding connection with the groove bottom of the limiting sliding groove.

Preferably, the opening device comprises a push rod, a sliding barrel, a spring and a roller shaft, two ends of the roller shaft are respectively connected with the end part of the sliding barrel in a rotating mode, the push rod is connected with the installation base, the inner side wall of the sliding barrel is connected with the side wall of the push rod in a sliding mode, two ends of the spring are respectively connected with the inner barrel bottom of the sliding barrel and the push rod, and the opening device is arranged on the side of the slag containing barrel.

Preferably, the first connecting piece and the second connecting piece are provided with three convex ends, and the three convex ends are provided with mounting holes.

Preferably, a reinforcing plate is arranged on the mounting base, the fixing rod penetrates through the reinforcing plate, an annular hole for the second connecting rod to slide is formed in the reinforcing plate, and the second connecting rod is in sliding connection with the hole wall of the annular hole.

Preferably, one end of the bottom plate is lower than the other end, the sliding plate and the horizontal plane form an included angle of 80 degrees, and the sliding plate is arranged above one end of the bottom plate.

The invention has the beneficial effects that:

the invention controls the negative pressure of the boiler furnace outlet and the running oxygen amount of the boiler, can reduce the power consumption of the equipment and reduce the production cost;

the slag discharging device is convenient for containing and transporting residues in the boiler, the slag containing barrels are uniformly arranged along the second chain, and the slag containing barrels can descend when ascending, so that the motor is ensured to only do work on the transportation of the residues, and the power consumption of the motor is reduced;

the slag charging barrel can realize the storage and transportation of slag without additionally arranging equipment for storing slag.

Drawings

The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention and not to limit the invention. In the drawings:

FIG. 1 is a side sectional view of a slag discharging device in example 2 of the present invention;

FIG. 2 is a side sectional view of a slag discharging device in accordance with embodiment 1 of the present invention;

FIG. 3 is a cross-sectional view of a slag ladle of the present invention;

FIG. 4 is a schematic view of the structure of the opening device of the present invention;

FIG. 5 is a front view of a reinforcing plate according to example 2 of the present invention;

fig. 6 is a schematic structural diagram of a first connecting member according to embodiment 3 of the present invention.

1. Installing a base; 2. a support bar; 3. a motor; 4. a first chain; 5. a first gear; 6. a fixing plate; 7. a second gear; 8. a second chain; 9. fixing the rod; 10. a first connecting member; 11. a first connecting rod; 12. a first connection block; 13. a second connecting rod; 14. a second connecting block; 15. a third connecting rod; 16. A second connecting member; 17. a slag bucket is filled; 18. a slide plate; 19. a base plate; 20. enclosing plates; 21. a limiting bulge; 22. a limiting chute; 23. a top rod; 24. a spring; 25. a slide cylinder; 26. a roll shaft; 27. a reinforcing plate; 28. Annular ring; 29. and (7) installing holes.

Detailed Description

Example 1

As shown in fig. 2, fig. 3 and fig. 4, a low energy consumption fiber yarn production process comprises the following steps: s1: soaking the pulp with sodium hydroxide water solution and curing agent to convert cellulose into alkali cellulose, and dissolving out hemicellulose;

s2: the alkali cellulose is squeezed to be converted into blocky alkali cellulose;

s3: crushing the blocky alkali cellulose on a crusher to form loose floccules;

s4: placing flocculent alkali cellulose in oxygen to cause oxidative cracking of the flocculent alkali cellulose and reduce the average polymerization degree;

s5: reacting the alkali cellulose in the S4 with carbon disulfide to generate cellulose xanthate;

s6: dissolving cellulose xanthate in dilute sodium hydroxide solution to obtain viscose;

s7: placing the viscose at 75 ℃ to gradually hydrolyze and saponify the sodium cellulose xanthate in the viscose, and simultaneously filtering and defoaming to remove bubbles and impurities;

s8: and (3) allowing the viscose in the S7 to pass through a spinneret orifice to form a trickle and enter an acid-containing coagulating bath, neutralizing alkali in the viscose, coagulating the trickle into a filament, and decomposing the cellulose xanthate to regenerate the hydrated cellulose.

Controlling the negative pressure of the boiler furnace outlet to be 0-50Pa, and controlling the boiler operation oxygen amount to be 2%.

The slag discharging device consists of a rotating device, a connecting device, a driving device, six slag containing barrels 17 and an opening device, and the lower end of the slag discharging device is provided with a mounting base;

the driving device consists of a supporting rod 2, two first gears 5, a first chain 4 and a motor 3, wherein the lower end of the supporting rod 2 is connected with the mounting base 1, the first gears 5 are rotatably connected with the supporting rod 4, the shell of the motor 3 is connected with the supporting rod 2, the output shaft of the motor 3 is connected with the first gears 5, the motor 3 drives the first gears 5 to rotate, the first gears 5 are meshed with the annular first chain 4, and the two first gears 5 are positioned on the same vertical plane;

the rotating device consists of a fixed plate 6, two second gears 7, a second chain 8 and two fixed rods 9, wherein two ends of each fixed rod 9 are respectively connected with the corresponding supporting rod 2 and the corresponding fixed plate 6, the fixed rods 9 penetrate through inner annular holes of the annular first chains 4, the second gears 7 are rotatably connected with the fixed plates 6, the second gears 7 are meshed with the annular second chains 8, and the two second gears 7 are positioned on the same vertical plane;

the connecting device comprises a first connecting piece 10, a second connecting piece 16, a first connecting rod 11, a second connecting rod 13, a third connecting rod 15, a first connecting block 12 and a second connecting block 14, one end of the first connecting piece 10 is connected with the annular end surface of the first chain 4, the other end of the first connecting piece 10 is rotatably connected with one end of the first connecting rod 11, the other end of the first connecting rod 11 is rotatably connected with the upper end of one side surface of the first connecting block 12, the lower end of the other side surface of the first connecting block 12 is connected with one end of the second connecting rod 13, the other end of the second connecting rod 13 is rotatably connected with the upper end of one side surface of the second connecting block 14, the lower end of the other side surface of the second connecting block 14 is connected with one end of the third connecting rod 15, one end of the second connecting piece 16 is connected with the annular end surface of the second chain 8, the other end of the second connecting piece 16 is rotatably connected with the third connecting rod 15, the other end of the third connecting rod 15 is connected with the side wall of the slag containing barrel 17, and the connecting device is convenient for the driving device to drive the rotating device to transport the boiler residues.

The slag containing barrel 17 consists of a bottom plate 19, three enclosing plates 20 and a sliding plate 18, the enclosing plate 20 adjacent to the sliding plate 18 is connected with a third connecting rod 15, the lower end of the enclosing plate 20 is connected with the upper end edge of the bottom plate 19, the sliding plate 18 is in sliding connection with the enclosing plates 20, the two sides of the sliding plate 18 are provided with limiting bulges 21, the edge of the enclosing plate 20 is provided with a limiting sliding groove 22 matched with the limiting bulges 21, the limiting bulges 21 are in sliding connection with the groove bottom of the limiting sliding groove 22, and the limiting bulges 21 and the limiting sliding groove 22 are convenient for the sliding plate 18 to stably slide and prevent the sliding plate 18 from separating from the enclosing plates 20; the bottom plate 19 and the horizontal plane form an included angle of 30 degrees, the sliding plate 18 and the horizontal plane form an included angle of 80 degrees, and the sliding plate 18 is arranged above the lower end of the bottom plate 19.

The opening device is arranged at one side of the falling of the slag containing barrel 17, the opening device consists of a push rod 23, two sliding barrels 25, a spring 24 and a roll shaft 26, two ends of the roll shaft 26 are respectively and rotatably connected with the end parts of the two sliding barrels 25, the push rod 23 is connected with a vertical mounting rod of the mounting base 1, the inner side wall of the sliding barrel 25 is in sliding connection with the side wall of the push rod, two ends of the spring 24 are respectively connected with the inner barrel bottom of the sliding barrel 25 and the push rod 23, the opening device is arranged at one side of the slag containing barrel, when the slag containing barrel 17 falls, the sliding plate 18 is contacted with the roll surface of the roll shaft 26, the coaming 20 and the bottom plate 19 continue to descend, the sliding plate 18 is not moved, the slag in the slag containing barrel 17 slides down along the bottom plate 19, when the limit protrusion 21 slides to the upper end of the limit chute 22, the spring 24 is compressed, the slide plate 18 moves down, the roller shaft 26 rolls, when the slide 18 is separated from the roller shaft 26, the lower end of the slide 18 is again in contact with the bottom plate 19, opening the device to facilitate the dumping of the slag.

Example 2

As shown in fig. 1, fig. 3 and fig. 4, a low-energy fiber yarn production process comprises the following steps: s1: soaking the pulp with sodium hydroxide water solution and curing agent to convert cellulose into alkali cellulose, and dissolving out hemicellulose;

s2: the alkali cellulose is squeezed to be converted into blocky alkali cellulose;

s3: crushing the blocky alkali cellulose on a crusher to form loose floccules;

s4: placing flocculent alkali cellulose in oxygen to cause oxidative cracking of the flocculent alkali cellulose and reduce the average polymerization degree;

s5: reacting the alkali cellulose in the S4 with carbon disulfide to generate cellulose xanthate;

s6: dissolving cellulose xanthate in dilute sodium hydroxide solution to obtain viscose;

s7: placing the viscose at 75 ℃ to gradually hydrolyze and saponify the sodium cellulose xanthate in the viscose, and simultaneously filtering and defoaming to remove bubbles and impurities;

s8: and (3) allowing the viscose in the S7 to pass through a spinneret orifice to form a trickle and enter an acid-containing coagulating bath, neutralizing alkali in the viscose, coagulating the trickle into a filament, and decomposing the cellulose xanthate to regenerate the hydrated cellulose.

Controlling the negative pressure of the boiler furnace outlet to be 0-50Pa, and controlling the boiler operation oxygen amount to be 2%.

The slag discharging device consists of a rotating device, a connecting device, a driving device, six slag containing barrels 17 and an opening device, and the lower end of the slag discharging device is provided with a mounting base;

the driving device consists of a supporting rod 2, two first gears 5, a first chain 4 and a motor 3, wherein the lower end of the supporting rod 2 is connected with the mounting base 1, the first gears 5 are rotatably connected with the supporting rod 4, the shell of the motor 3 is connected with the supporting rod 2, the output shaft of the motor 3 is connected with the first gears 5, the motor 3 drives the first gears 5 to rotate, the first gears 5 are meshed with the annular first chain 4, and the two first gears 5 are positioned on the same vertical plane;

the rotating device consists of a fixed plate 6, two second gears 7, a second chain 8 and two fixed rods 9, wherein two ends of each fixed rod 9 are respectively connected with the corresponding supporting rod 2 and the corresponding fixed plate 6, the fixed rods 9 penetrate through inner annular holes of the annular first chains 4, the second gears 7 are rotatably connected with the fixed plates 6, the second gears 7 are meshed with the annular second chains 8, and the two second gears 7 are positioned on the same vertical plane;

the connecting device comprises a first connecting piece 10, a second connecting piece 16, a first connecting rod 11, a second connecting rod 13, a third connecting rod 15, a first connecting block 12 and a second connecting block 14, one end of the first connecting piece 10 is connected with the annular end surface of the first chain 4, the other end of the first connecting piece 10 is rotatably connected with one end of the first connecting rod 11, the other end of the first connecting rod 11 is rotatably connected with the upper end of one side surface of the first connecting block 12, the lower end of the other side surface of the first connecting block 12 is connected with one end of the second connecting rod 13, the other end of the second connecting rod 13 is rotatably connected with the upper end of one side surface of the second connecting block 14, the lower end of the other side surface of the second connecting block 14 is connected with one end of the third connecting rod 15, one end of the second connecting piece 16 is connected with the annular end surface of the second chain 8, the other end of the second connecting piece 16 is rotatably connected with the third connecting rod 15, the other end of the third connecting rod 15 is connected with the side wall of the slag containing barrel 17, and the connecting device is convenient for the driving device to drive the rotating device to transport the boiler residues.

The mounting base 1 is provided with a reinforcing plate 27, the fixing rod 9 penetrates through the reinforcing plate 27, the reinforcing plate 27 is provided with an annular hole 28 for the second connecting rod 13 to slide, the second connecting rod 13 is connected with the annular hole 28 in a sliding mode, and the reinforcing plate 27 is convenient for the connecting device to be stably connected.

The slag containing barrel 17 consists of a bottom plate 19, three enclosing plates 20 and a sliding plate 18, the enclosing plate 20 adjacent to the sliding plate 18 is connected with a third connecting rod 15, the lower end of the enclosing plate 20 is connected with the upper end edge of the bottom plate 19, the sliding plate 18 is in sliding connection with the enclosing plates 20, the two sides of the sliding plate 18 are provided with limiting bulges 21, the edge of the enclosing plate 20 is provided with a limiting sliding groove 22 matched with the limiting bulges 21, the limiting bulges 21 are in sliding connection with the groove bottom of the limiting sliding groove 22, and the limiting bulges 21 and the limiting sliding groove 22 are convenient for the sliding plate 18 to stably slide and prevent the sliding plate 18 from separating from the enclosing plates 20; the bottom plate 19 and the horizontal plane form an included angle of 30 degrees, the sliding plate 18 and the horizontal plane form an included angle of 80 degrees, and the sliding plate 18 is arranged above the lower end of the bottom plate 19.

The opening device is arranged at one side of the falling of the slag containing barrel 17, the opening device consists of a push rod 23, two sliding barrels 25, a spring 24 and a roll shaft 26, two ends of the roll shaft 26 are respectively and rotatably connected with the end parts of the two sliding barrels 25, the push rod 23 is connected with a vertical mounting rod of the mounting base 1, the inner side wall of the sliding barrel 25 is in sliding connection with the side wall of the push rod, two ends of the spring 24 are respectively connected with the inner barrel bottom of the sliding barrel 25 and the push rod 23, the opening device is arranged at one side of the slag containing barrel, when the slag containing barrel 17 falls, the sliding plate 18 is contacted with the roll surface of the roll shaft 26, the coaming 20 and the bottom plate 19 continue to descend, the sliding plate 18 is not moved, the slag in the slag containing barrel 17 slides down along the bottom plate 19, when the limit protrusion 21 slides to the upper end of the limit chute 22, the spring 24 is compressed, the slide plate 18 moves down, the roller shaft 26 rolls, when the slide 18 is separated from the roller shaft 26, the lower end of the slide 18 is again in contact with the bottom plate 19, opening the device to facilitate the dumping of the slag.

Example 3

As shown in fig. 1, fig. 3, fig. 4 and fig. 5, a low energy consumption fiber yarn production process comprises the following steps: s1: soaking the pulp with sodium hydroxide water solution and curing agent to convert cellulose into alkali cellulose, and dissolving out hemicellulose;

s2: the alkali cellulose is squeezed to be converted into blocky alkali cellulose;

s3: crushing the blocky alkali cellulose on a crusher to form loose floccules;

s4: placing flocculent alkali cellulose in oxygen to cause oxidative cracking of the flocculent alkali cellulose and reduce the average polymerization degree;

s5: reacting the alkali cellulose in the S4 with carbon disulfide to generate cellulose xanthate;

s6: dissolving cellulose xanthate in dilute sodium hydroxide solution to obtain viscose;

s7: placing the viscose at 75 ℃ to gradually hydrolyze and saponify the sodium cellulose xanthate in the viscose, and simultaneously filtering and defoaming to remove bubbles and impurities;

s8: and (3) allowing the viscose in the S7 to pass through a spinneret orifice to form a trickle and enter an acid-containing coagulating bath, neutralizing alkali in the viscose, coagulating the trickle into a filament, and decomposing the cellulose xanthate to regenerate the hydrated cellulose.

Controlling the negative pressure of the boiler furnace outlet to be 0-50Pa, and controlling the boiler operation oxygen amount to be 2%.

The slag discharging device consists of a rotating device, a connecting device, a driving device, six slag containing barrels 17 and an opening device, and the lower end of the slag discharging device is provided with a mounting base;

the driving device consists of a supporting rod 2, two first gears 5, a first chain 4 and a motor 3, wherein the lower end of the supporting rod 2 is connected with the mounting base 1, the first gears 5 are rotatably connected with the supporting rod 4, the shell of the motor 3 is connected with the supporting rod 2, the output shaft of the motor 3 is connected with the first gears 5, the motor 3 drives the first gears 5 to rotate, the first gears 5 are meshed with the annular first chain 4, and the two first gears 5 are positioned on the same vertical plane;

the rotating device consists of a fixed plate 6, two second gears 7, a second chain 8 and two fixed rods 9, wherein two ends of each fixed rod 9 are respectively connected with the corresponding supporting rod 2 and the corresponding fixed plate 6, the fixed rods 9 penetrate through inner annular holes of the annular first chains 4, the second gears 7 are rotatably connected with the fixed plates 6, the second gears 7 are meshed with the annular second chains 8, and the two second gears 7 are positioned on the same vertical plane;

the connecting device comprises a first connecting piece 10, a second connecting piece 16, a first connecting rod 11, a second connecting rod 13, a third connecting rod 15, a first connecting block 12 and a second connecting block 14, one end of the first connecting piece 10 is connected with the annular end surface of the first chain 4, the other end of the first connecting piece 10 is rotatably connected with one end of the first connecting rod 11, the other end of the first connecting rod 11 is rotatably connected with the upper end of one side surface of the first connecting block 12, the lower end of the other side surface of the first connecting block 12 is connected with one end of the second connecting rod 13, the other end of the second connecting rod 13 is rotatably connected with the upper end of one side surface of the second connecting block 14, the lower end of the other side surface of the second connecting block 14 is connected with one end of the third connecting rod 15, one end of the second connecting piece 16 is connected with the annular end surface of the second chain 8, the other end of the second connecting piece 16 is rotatably connected with the third connecting rod 15, the other end of the third connecting rod 15 is connected with the side wall of the slag containing barrel 17, and the connecting device is convenient for the driving device to drive the rotating device to transport the boiler residues.

All be equipped with three protruding end on first connecting piece 10 and the second connecting piece 16, three protruding end all is equipped with mounting hole 29, and two mounting holes 29 that are nearest meet with first chain 4 and second chain 8, remaining mounting hole with respectively with head rod 11 and third connecting rod 15 rotate be connected, first connecting piece 10 and second connecting piece 16 are convenient for first chain 4 and second chain 8 to be connected with head rod 11 and third connecting rod 15 respectively.

The mounting base 1 is provided with a reinforcing plate 27, the fixing rod 9 penetrates through the reinforcing plate 27, the reinforcing plate 27 is provided with an annular hole 28 for the second connecting rod 13 to slide, the second connecting rod 13 is connected with the annular hole 28 in a sliding mode, and the reinforcing plate 27 is convenient for the connecting device to be stably connected.

The slag containing barrel 17 consists of a bottom plate 19, three enclosing plates 20 and a sliding plate 18, the enclosing plate 20 adjacent to the sliding plate 18 is connected with a third connecting rod 15, the lower end of the enclosing plate 20 is connected with the upper end edge of the bottom plate 19, the sliding plate 18 is in sliding connection with the enclosing plates 20, the two sides of the sliding plate 18 are provided with limiting bulges 21, the edge of the enclosing plate 20 is provided with a limiting sliding groove 22 matched with the limiting bulges 21, the limiting bulges 21 are in sliding connection with the groove bottom of the limiting sliding groove 22, and the limiting bulges 21 and the limiting sliding groove 22 are convenient for the sliding plate 18 to stably slide and prevent the sliding plate 18 from separating from the enclosing plates 20; the bottom plate 19 and the horizontal plane form an included angle of 30 degrees, the sliding plate 18 and the horizontal plane form an included angle of 80 degrees, and the sliding plate 18 is arranged above the lower end of the bottom plate 19.

The opening device is arranged at one side of the falling of the slag containing barrel 17, the opening device consists of a push rod 23, two sliding barrels 25, a spring 24 and a roll shaft 26, two ends of the roll shaft 26 are respectively and rotatably connected with the end parts of the two sliding barrels 25, the push rod 23 is connected with a vertical mounting rod of the mounting base 1, the inner side wall of the sliding barrel 25 is in sliding connection with the side wall of the push rod, two ends of the spring 24 are respectively connected with the inner barrel bottom of the sliding barrel 25 and the push rod 23, the opening device is arranged at one side of the slag containing barrel, when the slag containing barrel 17 falls, the sliding plate 18 is contacted with the roll surface of the roll shaft 26, the coaming 20 and the bottom plate 19 continue to descend, the sliding plate 18 is not moved, the slag in the slag containing barrel 17 slides down along the bottom plate 19, when the limit protrusion 21 slides to the upper end of the limit chute 22, the spring 24 is compressed, the slide plate 18 moves down, the roller shaft 26 rolls, when the slide 18 is separated from the roller shaft 26, the lower end of the slide 18 is again in contact with the bottom plate 19, opening the device to facilitate the dumping of the slag.

The working mode of the invention is as follows: boiler slag materials are loaded into the slag containing barrel 17 at the ascending end of the slag containing barrel 17, after slag is loaded, the driving device drives the rotating device to rotate through the connecting device, the rotating device can convey the slag materials to a high place to be discharged, the opening device is arranged at one side of the falling of the slag containing barrel 17, when the slag containing barrel 17 falls, the sliding plate 18 is in contact with the roller surface of the roller shaft 26, the enclosing plate 20 and the bottom plate 19 continue to fall, the sliding plate 18 is not moved, the slag materials in the slag containing barrel 17 slide down along the bottom plate 19, when the limiting bulge 21 slides to the upper end of the limiting sliding chute 22, the spring 24 is compressed, the sliding plate 18 moves downwards, the roller shaft 26 rolls, when the sliding plate 18 is separated from the roller shaft 26, the lower end of the sliding plate 18 is in contact with the bottom plate 19 again, and the opening device is convenient for dumping the slag materials; the negative pressure of the boiler furnace outlet and the running oxygen amount of the boiler are controlled, so that the power consumption of equipment can be reduced, and the production cost is reduced; arrange the residue device and be convenient for splendid attire and the residue in the transportation boiler, and dress sediment bucket 17 evenly sets up along second chain 8, when having dress sediment bucket 17 to rise, has dress sediment bucket 17 to descend, guarantees that motor 3 only does work to the transportation of residue, reduces the power consumption of motor 3.

Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

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