Stirring type fluorination electrolytic tank

文档序号:1517012 发布日期:2020-02-11 浏览:29次 中文

阅读说明:本技术 一种搅拌式氟化电解槽 (Stirring type fluorination electrolytic tank ) 是由 陈雨 于 2019-12-03 设计创作,主要内容包括:本发明公开了一种搅拌式氟化电解槽,属于电解槽技术领域,包括电解桶、支撑架、搅拌组件、电解组件、过渣组件和进料组件,所述支撑架呈竖直设置,所述电解桶呈竖直设置在支撑架的顶部,所述搅拌组件设置在电解桶上,所述搅拌组件与电解桶转动配合,所述电解组件的一端设置在电解桶内,所述电解组件的另一端设置在电解桶的顶部,所述过渣组件设置在电解桶的底部且与电解桶相连通,所述进料组件设置在电解桶的顶部,所述进料组件与电解桶相连通。本发明通过刮料板转动对电解桶内壁上电解所产的结合物和粘附在内壁上的电解质进行刮除,防止在进行电解的过程中,有粘附物在电解桶1的内壁上,影响电解的进程和电解的效果。(The invention discloses an agitation type fluorination electrolytic cell, which belongs to the technical field of electrolytic cells and comprises an electrolytic barrel, a support frame, an agitation component, an electrolytic component, a slag passing component and a feeding component, wherein the support frame is vertically arranged, the electrolytic barrel is vertically arranged at the top of the support frame, the agitation component is arranged on the electrolytic barrel, the agitation component is in rotating fit with the electrolytic barrel, one end of the electrolytic component is arranged in the electrolytic barrel, the other end of the electrolytic component is arranged at the top of the electrolytic barrel, the slag passing component is arranged at the bottom of the electrolytic barrel and communicated with the electrolytic barrel, the feeding component is arranged at the top of the electrolytic barrel, and the feeding component is communicated with the electrolytic barrel. The invention scrapes the combination produced by electrolysis on the inner wall of the electrolytic barrel and the electrolyte adhered on the inner wall through the rotation of the scraper plate, thereby preventing the adhered substances on the inner wall of the electrolytic barrel 1 from influencing the electrolysis process and the electrolysis effect in the process of electrolysis.)

1. An agitated fluorination cell, comprising: comprises an electrolytic barrel (1), a supporting frame (2), a stirring component (3), an electrolytic component (4), a slag passing component (5) and a feeding component (6), the supporting frame (2) is vertically arranged, the electrolytic barrel (1) is vertically arranged at the top of the supporting frame (2), the stirring component (3) is arranged on the electrolytic barrel (1), the stirring component (3) is in running fit with the electrolytic barrel (1), one end of the electrolytic component (4) is arranged in the electrolytic barrel (1), the other end of the electrolytic component (4) is arranged at the top of the electrolytic barrel (1), the slag passing component (5) is arranged at the bottom of the electrolytic barrel (1) and is communicated with the electrolytic barrel (1), the slag passing assembly (5) is in sliding fit with the electrolytic barrel (1), the feeding assembly (6) is arranged at the top of the electrolytic barrel (1), and the feeding assembly (6) is communicated with the electrolytic barrel (1).

2. An agitated fluorination cell as claimed in claim 1 in which: stirring subassembly (3) include agitator motor (31), (mixing) shaft (32), solid fixed ring (33) and a plurality of puddler (34), agitator motor (31) set up the top at electrolysis bucket (1) through solid fixed ring (33), the vertical downward setting of output shaft of agitator motor (31), agitator shaft (32) set up in electrolysis bucket (1) and the top of (mixing) shaft (32) and the output shaft fixed connection of agitator motor (31), and is a plurality of puddler (34) are the circumference and set up on agitator shaft (32).

3. An agitated fluorination cell as claimed in claim 2 in which: stirring subassembly (3) still include stirring board (35), scrape flitch (36) and two flexible connecting rod (37), stirring board (35) set up in the bottom of (mixing) shaft (32) and the one end and (mixing) shaft (32) fixed connection of stirring board (35), two flexible connecting rod (37) symmetry sets up the one end at stirring board (35), scrape flitch (36) and be vertical setting in electrolytic tank (1) and scrape the bottom and two flexible connecting rod (37) fixed connection of flitch (36), scrape the inner wall sliding fit of flitch (36) and electrolytic tank (1), scrape flitch (36) and make for flexible material with electrolytic tank (1) sliding fit's one side.

4. An agitated fluorination cell as claimed in claim 1 in which: electrolytic component (4) are including install bin (41), positive pole electric post (42) and negative pole electric post (43), install bin (41) set up the top at electrolysis bucket (1), install bin (41) are network structure, positive pole electric post (42) set up in install bin (41), the top of positive pole electric post (42) is located the top of electrolysis bucket (1), negative pole electric post (43) set up in install bin (41) and are located the side of positive pole electric post (42), the top of negative pole electric post (43) is located the top of electrolysis bucket (1).

5. An agitated fluorination cell as claimed in claim 1 in which: the slag passing assembly (5) comprises a collecting cover (51), a driving motor (52), a driving disc (53), a driving rod (54), a connecting block (55) and a grid disc (56), wherein the collecting cover (51) is arranged at the bottom of the electrolytic barrel (1) and communicated with the electrolytic barrel (1), the grid disc (56) is horizontally arranged in the collecting cover (51), an installation circular groove (16) is formed in the side wall of the electrolytic barrel (1), a plurality of vibration springs (57) distributed in the circumferential direction are arranged at the top and the bottom of the grid disc (56), one end of the connecting block (55) is fixedly connected with the grid disc (56), a sliding groove (15) in sliding fit with the connecting block (55) is formed in the side wall of the electrolytic barrel (1), the driving motor (52) is arranged on the side wall of the electrolytic barrel (1), the driving disc (53) is arranged on an output shaft of the driving motor (52), and two ends of the driving rod (54) are respectively and rotatably connected with the driving disc (53) and the connecting block (55).

6. An agitated fluorination cell as claimed in claim 1 in which: feeding subassembly (6) are including rotating motor (61), storage box (62), first dwang (63), second dwang (64), closing plate (65) and play feed cylinder (66), storage box (62) set up the top in electrolysis bucket (1), go out feed cylinder (66) both ends and be linked together with storage box (62) and electrolysis bucket (1) respectively, closing plate (65) set up on going out feed cylinder (66) and with play feed cylinder (66) sliding fit, rotation motor (61) set up at the top of electrolysis bucket (1) and the vertical upwards setting of the output shaft of rotation motor (61), the one end setting of first dwang (63) is on the output shaft of rotation motor (61), the both ends of second dwang (64) are connected with first dwang (63) and closing plate (65) swivelling joint respectively.

7. An agitated fluorination cell as claimed in claim 1 in which: the top of electrolysis bucket (1) is equipped with inlet pipe (11) rather than being linked together, the bottom of collecting cover (51) is equipped with discharging pipe (12) rather than being linked together, be equipped with the solenoid valve on discharging pipe (12), the top of electrolysis bucket (1) is equipped with outlet duct (13) rather than being linked together.

8. An agitated fluorination cell as claimed in claim 1 in which: the side wall of the electrolytic barrel (1) is provided with a plurality of refrigeration pipes (14) which are distributed at equal intervals.

Technical Field

The invention relates to the technical field of electrolytic cells, in particular to a stirring type fluorination electrolytic cell.

Background

Fluorine-containing organic compounds are few in nature, and introduction of fluorine into organic compounds is a problem which needs to be solved urgently, and the preparation of organic fluorides can be directly fluorinated by F2 or indirectly fluorinated by a fluorinating reagent such as XeF2, hypofluoric acid, high-valence metal fluoride, N2F compounds and the like. The chemical fluorination methods have complex reaction and operation and harsh equipment; the fluorinating agents used are highly toxic or extremely unsafe, some being very expensive; furthermore, it is difficult to control the amount of fluorine added, and it is difficult to obtain the desired product. Therefore, other methods have to be sought.

For example, the patent with the publication number of CN103243341A relates to a stirring type fluorination electrolytic tank, which consists of a motor, a shaft coupling, a stirring shaft, a shaft seal, an electrode column, an electrode bundle, an electrolytic tank cover plate, an electrolytic tank jacket, a shaft sleeve, a blind plate, a guide cylinder, a stirring paddle and an insulating washer, the stirring type fluorination electrolytic tank provided by the invention ensures that the materials are dissolved and dispersed more uniformly in the whole system, and simultaneously, the fluorination reaction is carried out in the electrolytic tank, so that the reaction induction period is reduced, the reaction induction period is reduced from 3-5 days to one day, the phenomenon of tank death is basically avoided, the number of tank cleaning due to the treatment of the tank death is reduced, the tank death is not caused 3-4 times per year before the stirring type tank is adopted, the phenomenon of tank death is reduced by more than 20 percent, the yield of a single tank is improved by 30 percent, and the polymers generated in the electrolytic tank are reduced, the time for cleaning the groove is doubled, and the labor intensity of manual groove cleaning is reduced.

However, the above-mentioned devices also have the following problems in use: firstly, when carrying out electrolysis, can not separate the deposit in the electrolytic solution, cause the deposit accumulation easily, influence the effect of electrolysis, and secondly, when carrying out electrolysis, can not clear up the deposit of adhesion on the electrolysis trough inner wall, accumulate for a long time and influence the electrolysis effect of electrolysis trough.

Disclosure of Invention

The invention aims to provide a stirring type fluorination electrolytic tank to solve the technical problems that precipitates in an electrolytic solution cannot be separated, the precipitates are easy to accumulate and attachments adhered to the inner wall of the electrolytic tank cannot be cleaned in the prior art.

In order to solve the technical problems, the invention provides the following technical scheme: the utility model provides an electrolytic bath is fluoridized to stirring formula, includes electrolysis bucket, support frame, stirring subassembly, electrolysis subassembly, crosses sediment subassembly and feeding component, the support frame is vertical setting, the electrolysis bucket is vertical setting at the top of support frame, the stirring subassembly sets up on the electrolysis bucket, stirring subassembly and electrolysis bucket normal running fit, the one end setting of electrolysis subassembly is in the electrolysis bucket, the other end setting of electrolysis subassembly is at the top of electrolysis bucket, it sets up in the bottom of electrolysis bucket and is linked together with the electrolysis bucket to cross the sediment subassembly, cross sediment subassembly and electrolysis bucket sliding fit, the feeding component sets up the top at the electrolysis bucket, the feeding component is linked together with the electrolysis bucket.

Further, the stirring subassembly includes agitator motor, (mixing) shaft, solid fixed ring and a plurality of puddler, agitator motor sets up the top at the electrolysis bucket through solid fixed ring, agitator motor's the vertical downward setting of output shaft, the (mixing) shaft setting is in the electrolysis bucket and the top of (mixing) shaft and agitator motor's output shaft fixed connection, and is a plurality of the puddler is the circumference and sets up on the (mixing) shaft.

Further, the stirring subassembly still includes the stirring board, scrapes flitch and two flexible connecting rods, the stirring board sets up in the bottom of (mixing) shaft and the one end and the (mixing) shaft fixed connection of stirring board, two the flexible connecting rod symmetry sets up the one end at the stirring board, it is vertical setting and scrapes the bottom and two flexible connecting rod fixed connection of flitch in the electrolysis barrel to scrape the flitch, scrape the inner wall sliding fit of flitch and electrolysis barrel, it makes for flexible material with electrolysis barrel sliding fit's one side to scrape the flitch.

Further, the electrolysis subassembly includes install bin, positive pole electric post and negative pole electric post, the install bin sets up the top at the electrolysis bucket, the install bin is network structure, positive pole electric post sets up in the install bin, the top of positive pole electric post is located the top of electrolysis bucket, negative pole electric post sets up in the install bin and is located the side of positive pole electric post, the top of negative pole electric post is located the top of electrolysis bucket.

Further, it is including collecting cover, driving motor, driving-disc, actuating lever, connecting block and net disc to cross the sediment subassembly, it sets up in the bottom of electrolysis bucket and is linked together with the electrolysis bucket to collect the cover, the net disc is the level and sets up in collecting the cover, be equipped with the installation circular slot on the lateral wall of electrolysis bucket, the top and the bottom of net disc all are equipped with a plurality of vibrations springs that are the circumference and distribute, the one end and the net disc fixed connection of connecting block, be equipped with on the lateral wall of electrolysis bucket with connecting block sliding fit's sliding tray, driving motor sets up on the lateral wall of electrolysis bucket, the driving-disc sets up on driving motor's output shaft, the both ends of actuating lever rotate with driving-disc and connecting block respectively and are connected.

Further, the feeding subassembly is including rotating motor, storage tank, first dwang, second dwang, closing plate and play feed cylinder, the storage tank sets up the top at the electrolysis bucket, it is linked together with storage tank and electrolysis bucket respectively to go out the feed cylinder both ends, the closing plate setting on going out the feed cylinder and with play feed cylinder sliding fit, the vertical upwards setting of the output shaft that the motor set up at the top of electrolysis bucket and rotate the motor rotates, the one end setting of first dwang is on the output shaft that rotates the motor, the both ends of second dwang rotate with first dwang and closing plate respectively and are connected.

Furthermore, the top of the electrolytic barrel is provided with a feeding pipe communicated with the electrolytic barrel, the bottom of the collecting cover is provided with a discharging pipe communicated with the collecting cover, the discharging pipe is provided with an electromagnetic valve, and the top of the electrolytic barrel is provided with an air outlet pipe communicated with the electrolytic barrel.

Furthermore, a plurality of refrigeration pipes which are distributed at equal intervals are arranged on the side wall of the electrolytic barrel.

Compared with the prior art, the invention has the beneficial effects that:

firstly, the stirring shaft rotates to drive the stirring plate to rotate while stirring, the stirring plate rotates two flexible connecting rods, the two flexible connecting rods rotate to drive the scraper plate to rotate, and the scraper plate rotates to scrape a combination produced by electrolysis on the inner wall of the electrolytic tank 1 and electrolyte adhered to the inner wall, so that the phenomenon that the electrolytic process and the electrolytic effect are influenced by adhesive on the inner wall of the electrolytic tank in the process of electrolysis is prevented.

Secondly, after the electrolysis, the precipitates generated by the electrolysis can be accumulated in the electrolytic solution, when the electrolytic solution is discharged outwards, the mesh circular plate can be blocked due to the accumulation of the precipitates, the driving motor works to drive the driving disc to rotate, the driving disc rotates to drive the driving rod to rotate, the driving rod rotates to drive the connecting block to move on the sliding groove on the electrolytic barrel, the connecting block moves to drive the mesh circular plate to vibrate on the installation circular groove through a plurality of vibration springs, the precipitates on the mesh circular plate are vibrated down, and the mesh circular plate is prevented from being blocked, so that the filtering of the precipitates in the electrolytic solution is influenced.

Thirdly, in the process of electrolysis, the concentration of the electrolytic solution can be reduced, the electrolysis effect can be influenced after the reduction, the rotating motor works to drive the first rotating rod to rotate, the second rotating rod rotates to drive the second rotating rod to rotate, the second rotating rod rotates to drive the closing plate to move on the discharging barrel to control the on-off of the discharging barrel, the electrolytic solution in the storage box is conveyed into the electrolytic barrel, the concentration of the electrolytic solution in the electrolytic barrel is ensured, and the electrolysis effect cannot be influenced in the electrolysis process due to dilution of the concentration of the electrolyte.

Fourthly, the refrigerating pipes are arranged, the refrigerating pipes can cool the electrolytic solution, and the electrolytic solution is discharged after being cooled.

Drawings

FIG. 1 is a schematic perspective view of the present invention;

FIG. 2 is a top view of the present invention;

FIG. 3 is a cross-sectional view taken along line A-A of FIG. 2;

FIG. 4 is a schematic perspective view of the feed assembly of the present invention;

FIG. 5 is a perspective view of the slag passing assembly of the present invention;

fig. 6 is a schematic perspective view of the stirring assembly of the present invention.

The reference numbers in the figures are: the device comprises an electrolytic tank 1, a feeding pipe 11, a discharging pipe 12, an air outlet pipe 13, a refrigerating pipe 14, a sliding groove 15, a mounting circular groove 16, a support frame 2, a stirring assembly 3, a stirring motor 31, a stirring shaft 32, a fixing ring 33, a stirring rod 34, a stirring plate 35, a scraping plate 36, a flexible connecting rod 37, an electrolytic assembly 4, a mounting box 41, an anode electric pole 42, a cathode electric pole 43, a slag passing assembly 5, a collecting cover 51, a driving motor 52, a driving disc 53, a driving rod 54, a connecting block 55, a grid disc 56, a vibrating spring 57, a feeding assembly 6, a rotating motor 61, a storage box 62, a first rotating rod 63, a second rotating rod 64, a closing plate 65 and a discharging cylinder 66.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.

In the description of the present invention, it is to be understood that the terms "longitudinal", "lateral", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on those shown in the drawings, are merely for convenience of description of the present invention, and do not indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be construed as limiting the present invention.

Referring to fig. 1 to 6, the invention provides an agitation type fluorination electrolytic cell, which comprises an electrolytic barrel 1, a support frame 2, an agitation assembly 3, an electrolytic assembly 4, a slag passing assembly 5 and a feeding assembly 6, wherein the support frame 2 is vertically arranged, the electrolytic barrel 1 is vertically arranged at the top of the support frame 2, the agitation assembly 3 is arranged on the electrolytic barrel 1, the agitation assembly 3 is rotatably matched with the electrolytic barrel 1, one end of the electrolytic assembly 4 is arranged in the electrolytic barrel 1, the other end of the electrolytic assembly 4 is arranged at the top of the electrolytic barrel 1, the slag passing assembly 5 is arranged at the bottom of the electrolytic barrel 1 and communicated with the electrolytic barrel 1, the slag passing assembly 5 is slidably matched with the electrolytic barrel 1, the feeding assembly 6 is arranged at the top of the electrolytic barrel 1, and the feeding assembly 6 is communicated with the electrolytic barrel 1; when carrying out the point and solving, stirring subassembly 3 work drives the electrolytic solution in the electrolytic tank 1 and rotates, carry out abundant mixed operation with the electrolytic solution in the electrolytic tank 1, after stirring, electrolytic component 4 carries out the point and solves the operation to the electrolytic solution, at the in-process of electrolysis, feeding subassembly 6 work can carry electrolytic solution to electrolytic tank 1 in, prevent that the purity of electrolytic solution is not enough at the volume in-process of electrolysis, influence electrolysis operation, it can filter the solution after the electrolysis is accomplished to cross sediment subassembly 5, filter out the precipitate that generates in the electrolytic solution, carry out timely recovery to the precipitate.

The stirring assembly 3 comprises a stirring motor 31, a stirring shaft 32, a fixing ring 33 and a plurality of stirring rods 34, wherein the stirring motor 31 is arranged at the top of the electrolytic tank 1 through the fixing ring 33, an output shaft of the stirring motor 31 is vertically arranged downwards, the stirring shaft 32 is arranged in the electrolytic tank 1, the top of the stirring shaft 32 is fixedly connected with the output shaft of the stirring motor 31, and the stirring rods 34 are circumferentially arranged on the stirring shaft 32; the fixing ring 33 is used for fixing and installing stirring electrolysis, when stirring, the stirring motor 31 works to drive the stirring shaft 32 to rotate, the rotating shaft rotates to drive the stirring rods 34 to rotate, and the electrolytic solution in the electrolytic barrel 1 is fully stirred, so that the electrolytic solution is fully electrolyzed.

The stirring assembly 3 further comprises a stirring plate 35, a scraping plate 36 and two flexible connecting rods 37, the stirring plate 35 is arranged at the bottom of the stirring shaft 32, one end of the stirring plate 35 is fixedly connected with the stirring shaft 32, the two flexible connecting rods 37 are symmetrically arranged at one end of the stirring plate 35, the scraping plate 36 is vertically arranged in the electrolytic tank 1, the bottom of the scraping plate 36 is fixedly connected with the two flexible connecting rods 37, the scraping plate 36 is in sliding fit with the inner wall of the electrolytic tank 1, and one side of the scraping plate 36 in sliding fit with the electrolytic tank 1 is made of a flexible material; when stirring, stirring shaft 32 rotates and drives stirring board 35 and rotate, and stirring board 35 rotates two flexible connecting rods 37 and rotates, and two flexible connecting rods 37 rotate and drive scraping plate 36 and rotate, and scraping plate 36 rotates and strikes off the combination that the electrolysis produced on the inner wall of electrolytic tank 1 and the electrolyte of adhesion on the inner wall, prevents to carry out the in-process of electrolysis, has the adhesion thing on electrolytic tank 1's inner wall, influences electrolytic process and electrolytic effect.

The electrolytic component 4 comprises an installation box 41, an anode electric pole 42 and a cathode electric pole 43, the installation box 41 is arranged at the top of the electrolytic barrel 1, the installation box 41 is of a net structure, the anode electric pole 42 is arranged in the installation box 41, the top of the anode electric pole 42 is positioned at the top of the electrolytic barrel 1, the cathode electric pole 43 is arranged in the installation box 41 and positioned at the side of the anode electric pole 42, and the top of the cathode electric pole 43 is positioned at the top of the electrolytic barrel 1; an external power supply is connected to the anode electric pole 42 and the cathode electric pole 43, and the anode electric pole 42 and the cathode electric pole 43 perform electrolysis operation on the electrolyte in the installation box 41.

The slag passing assembly 5 comprises a collecting cover 51, a driving motor 52, a driving disc 53, a driving rod 54, a connecting block 55 and a grid disc 56, wherein the collecting cover 51 is arranged at the bottom of the electrolytic barrel 1 and communicated with the electrolytic barrel 1, the grid disc 56 is horizontally arranged in the collecting cover 51, a mounting circular groove 16 is arranged on the side wall of the electrolytic barrel 1, a plurality of vibration springs 57 which are distributed circumferentially are arranged at the top and the bottom of the grid disc 56, one end of the connecting block 55 is fixedly connected with the grid disc 56, a sliding groove 15 which is in sliding fit with the connecting block 55 is arranged on the side wall of the electrolytic barrel 1, the driving motor 52 is arranged on the side wall of the electrolytic barrel 1, the driving disc 53 is arranged on an output shaft of the driving motor 52, and two ends of the driving rod 54 are respectively in rotating connection with the driving disc 53 and the connecting block; after electrolysis, the precipitate generated by electrolysis can be accumulated in the electrolytic solution, when the electrolytic solution is discharged outwards, the precipitate accumulation can cause the grid disc 56 to be blocked, the driving motor 52 works to drive the driving disc 53 to rotate, the driving disc 53 rotates to drive the driving rod 54 to rotate, the driving rod 54 rotates to drive the connecting block 55 to move on the chute on the electrolytic barrel 1, the connecting block 55 moves to drive the grid disc to vibrate on the installation circular groove 16 through a plurality of vibration springs 57, the precipitate on the grid disc 56 is vibrated down, the grid disc 56 is prevented from being blocked, and the filtering of the precipitate in the electrolytic solution is influenced.

The feeding assembly 6 comprises a rotating motor 61, a storage box 62, a first rotating rod 63, a second rotating rod 64, a closing plate 65 and a discharging barrel 66, the storage box 62 is arranged at the top of the electrolytic barrel 1, two ends of the discharging barrel 66 are respectively communicated with the storage box 62 and the electrolytic barrel 1, the closing plate 65 is arranged on the discharging barrel 66 and is in sliding fit with the discharging barrel 66, the rotating motor 61 is arranged at the top of the electrolytic barrel 1 and is vertically upwards arranged on an output shaft of the rotating motor 61, one end of the first rotating rod 63 is arranged on the output shaft of the rotating motor 61, and two ends of the second rotating rod 64 are respectively in rotating connection with the first rotating rod 63 and the closing plate 65; the storage box 62 is used for depositing the electrolytic solution that needs to add, at the in-process that carries out the electrolysis, electrolytic solution's concentration can reduce, can influence electrolytic effect after reducing, the work of rotation motor 61 drives first dwang 63 and rotates, second dwang 64 rotates and drives second dwang 64 and rotate, second dwang 64 rotates and drives the break-make that closing plate 65 removed control play feed cylinder 66 on going out feed cylinder 66, carry the electrolytic solution in the storage box 62 to the electrolysis bucket 1 in, guarantee electrolytic solution's in the electrolysis bucket 1 concentration, can not lead to the electrolytic effect of influence among the electrolysis-process because electrolyte concentration dilutes.

The top of the electrolytic barrel 1 is provided with a feeding pipe 11 communicated with the electrolytic barrel, the bottom of the collecting cover 51 is provided with a discharging pipe 12 communicated with the collecting cover, the discharging pipe 12 is provided with an electromagnetic valve, and the top of the electrolytic barrel 1 is provided with an air outlet pipe 13 communicated with the electrolytic barrel; the feeding pipe 11 is used for conveying required electrolytic solution to the electrolytic barrel 1, the discharging pipe 12 is used for discharging the electrolytic solution, the electromagnetic valve is used for controlling the on-off of the discharging pipe 12, and the gas outlet pipe 13 is used for discharging waste gas generated by electrolysis.

A plurality of refrigeration pipes 14 which are distributed at equal intervals are arranged on the side wall of the electrolytic barrel 1; the cooling pipes 14 can cool the electrolytic solution, and the electrolytic solution is discharged after cooling.

The working principle of the invention is as follows: when the invention is used, the feeding pipe 11 is used for conveying the required electrolytic solution into the electrolytic barrel 1, when stirring, the stirring motor 31 works to drive the stirring shaft 32 to rotate, the rotating shaft rotates to drive the stirring rods 34 to rotate, so as to fully stir the electrolytic solution in the electrolytic barrel 1 and fully electrolyze the electrolytic solution, when stirring, the stirring shaft 32 rotates to drive the stirring plate 35 to rotate, the stirring plate 35 rotates two flexible connecting rods 37 to rotate, the two flexible connecting rods 37 rotate to drive the scraper 36 to rotate, the scraper 36 rotates to scrape the combination produced by electrolysis on the inner wall of the electrolytic barrel 1 and the electrolyte adhered on the inner wall, so that the phenomenon that the adhesion matters are on the inner wall of the electrolytic barrel 1 to influence the electrolytic process and the electrolytic effect is prevented during the electrolysis, the external power supply is connected to the anode electric column 42 and the cathode electric column 43, the anode electric pole 42 and the cathode electric pole 43 perform electrolysis operation on the electrolyte in the installation box 41, after electrolysis, the deposit generated by electrolysis will accumulate in the electrolytic solution, when the electrolytic solution is discharged outwards, the deposit accumulation will cause the grid disc 56 to block, the driving motor 52 works to drive the driving disc 53 to rotate, the driving disc 53 rotates to drive the driving rod 54 to rotate, the driving rod 54 rotates to drive the connecting block 55 to move on the chute on the electrolytic barrel 1, the connecting block 55 moves to drive the grid disc to vibrate on the installation circular groove 16 through a plurality of vibrating springs 57, the deposit on the grid disc 56 is vibrated down to prevent the grid disc 56 from blocking, during the electrolysis, the concentration of the electrolytic solution will decrease, after the decrease, the electrolysis effect will be affected, the rotating motor 61 works to drive the first rotating rod 63 to rotate, the second rotating rod 64 rotates to drive the second rotating rod 64 to rotate, second dwang 64 rotates and drives closure plate 65 and remove the break-make that comes control play feed cylinder 66 on play feed cylinder 66, carry the electrolytic solution in the storage box 62 to electrolytic tank 1 in, guarantee the concentration of the electrolytic solution in electrolytic tank 1, can not lead to the effect of electrolysis in-process influence electrolysis because electrolyte concentration dilutes, after the electrolysis is accomplished, need outwards discharge electrolytic solution, a plurality of refrigeration pipes 14 move and to cool down electrolytic solution, be favorable to discharging electrolytic solution after the cooling, discharging pipe 12 is used for discharging electrolytic solution after the cooling, the solenoid valve is used for controlling the break-make of discharging pipe 12, outlet duct 13 discharges the waste gas that the electrolysis produced.

Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.

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