阅读说明：本技术 一种青柠薄荷香型烟用爆珠的制备及其方法 (Preparation method and method of lemon mint flavor type blasting bead for cigarettes ) 是由 尹团章 陈浩 张敦铁 邵兴伟 张磊 于 2019-09-25 设计创作，主要内容包括：本发明公开了一种青柠薄荷香型烟用爆珠的制备及其方法,该种方法通过乳化、滴制成型、水洗、交联和干燥等一系列烟用爆珠制备工艺,从而制得青柠薄荷香型烟用爆珠,该爆珠能较好地包裹青柠薄荷香精,生产过程较简单,质量稳定性好,也能满足生产的要求；在制备过程中避免机械切割成型的使用,采用液体乳化交联滴制成型的方式,避免了偏芯珠、实心珠、气泡珠等现象的发生,有效提高了产品的成品率和质量；同时,通过本发明制成的成型液和乳化液,得到的爆珠的芯液和外包胶液有效适配,避免了包覆破漏的现象发生。(The invention discloses a preparation method of a lemon mint flavor type bead blasting for cigarettes and a preparation method thereof, wherein the method prepares the lemon mint flavor type bead blasting for cigarettes through a series of bead blasting preparation processes of emulsification, drip molding, washing, crosslinking, drying and the like, and the bead blasting can better wrap lemon mint essence, has a simpler production process and good quality stability and can also meet the production requirement; the use of mechanical cutting molding is avoided in the preparation process, and the liquid emulsifying, crosslinking and dripping molding mode is adopted, so that the phenomena of eccentric beads, solid beads, bubble beads and the like are avoided, and the yield and the quality of products are effectively improved; meanwhile, the core liquid of the obtained blasting bead is effectively matched with the outer coating glue liquid through the molding liquid and the emulsion prepared by the invention, so that the phenomenon of coating and leakage is avoided.)

1. A lime mint flavor type blasting bead for cigarettes is characterized in that: the coating comprises the following components in parts by mass:

14-70 parts of deionized water phase;

28-280 parts of essence oil phase;

100 portions of molding liquid

100 portions and 220 portions of crosslinking liquid.

2. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 1, wherein: the deionized water phase comprises deionized water, 1-2wt% of sodium alginate and 1-2wt% of emulsifier.

3. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 2, wherein: the emulsifier is Tween 80.

4. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 1, wherein: the essence oil phase comprises a green lemon mint essence and an oily solvent, and the mixing mass ratio of the green lemon mint essence to the oily solvent is 1: 8-10.

5. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 4, wherein: the oily solvent is one or a mixture of ODO solvent and olive oil.

6. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 5, wherein: the ODO solvent and the olive oil are mixed according to the mass ratio of 4-8: 1-5.

7. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 1, wherein: the molding liquid contains deionized water and 1-2wt% of CaCl in deionized water₂And span 20 with the weight of 3-5 per mill of deionized water.

8. The popping bead for the green lemon mint flavor type cigarette as claimed in claim 1, wherein: the cross-linking solution is 0.5-1.0% chitosan solution or 4-5% potassium persulfate solution.

9. The method for preparing the bead blasting for the green lemon mint type cigarette according to any one of claims 1 to 8, comprising the following steps:

s1, preparing deionized water phase solution: adding 1.0-2.0% of sodium alginate and 1.0-2.0% of Tween80 into deionized water, and fully and uniformly stirring to obtain a deionized water phase for later use;

s2, preparing an essence oil phase solution: adding the green lemon mint essence and one or two of ODO solvent or olive oil according to the weight ratio of 1: 8-10, uniformly stirring, and filtering by a 0.8nm ceramic membrane to obtain an essence oil phase for later use;

s3, emulsification: adding the essence oil phase solution and the deionized water phase solution according to the weight ratio of 2-4: 1, homogenizing at a high speed of 8000-11000 rpm for 5-10 min, and preparing into an emulsion;

s4, preparation of a molding liquid: adding CaCl according to 4-8% of the weight of the deionized water₂Adding span 20 in an amount which is 3-5 per mill of the weight of the deionized water, and fully and uniformly stirring to obtain a forming solution;

s5, dropping and forming: dripping the emulsion into the forming liquid at the speed of 3.0-6.0 ML/min by a plunger pump, and reacting for 6-15 minutes to prepare young pills;

s6, washing: putting the prepared young green lemon mint essence pills into deionized water, and washing off forming liquid on the surfaces of the young green lemon mint essence pills;

s7, crosslinking: putting the washed young pills into 0.5-1.0% chitosan solution or 4-5% potassium persulfate solution, and crosslinking for 20-40 minutes;

s8, drying: and (3) drying the crosslinked young pills in a roller to obtain the finished products of the green lemon mint flavor type popping pills.

10. The method for preparing the bead for the green lemon mint type cigarette according to claim 9, wherein the method comprises the following steps: the drying temperature in the step 8 is 20-28 ℃, the drying humidity is 20-40% RH, and the drying time is 1-2 h.

Technical Field

The invention relates to the technical field of bead blasting for cigarettes, in particular to a preparation method and a method of bead blasting for cigarettes with green lemon mint flavor.

Background

At present, in the dropping forming process of the bead blasting for the cigarettes, a gravity cutting forming process and a pulse cutting forming process are common. The bead blasting and dripping forming process generally adopts a two-channel approach of concentric circles of core liquid and glue liquid to carry out dripping, and the forming process can have the phenomena of eccentric beads, solid beads, bubble beads and the like, and even has the problem that essence and essential oil cannot be wrapped. The phenomena of eccentric beads, solid beads, bubble beads and the like can be solved by optimizing process parameters, and the difficult problem that the core liquid cannot be wrapped is caused by the improper matching of the core liquid and the glue liquid. The optimization of the formula of the glue solution is a relatively complex and huge technical working process.

The production system (application No. 201510944973.5) of the hollow alginate capsule for the cigarette adopts CaCl containing essential oil₂The emulsion is dripped into the sodium alginate solution to generate bead blasting, the capsule for the cigarette prepared by the patent technology gradually consumes the amount of the sodium alginate in the forming solution, the pressure born by the finished capsule produced subsequently is gradually reduced, and the quality stability of the capsule for the cigarette is required to be improved.

Disclosure of Invention

The invention aims to provide a preparation method of the flavor type lemon mint popping bead for cigarettes and a preparation method thereof aiming at the defects of the prior art, and the bead popping prepared by the method has good quality stability and can meet the requirement of production capacity.

The invention provides a lemon mint flavor type bead for cigarettes, which comprises the following components in parts by mass:

14-70 parts of deionized water phase;

28-280 parts of essence oil phase;

100 portions of molding liquid

100 portions and 220 portions of crosslinking liquid.

Further, the deionized water phase comprises deionized water, 1-2wt% of sodium alginate and 1-2wt% of emulsifier.

Further, the emulsifier is tween 80.

Further, the essence oil phase comprises the green lemon mint essence and an oily solvent, and the mixing mass ratio of the green lemon mint essence to the oily solvent is 1: 8-10.

Further, the oily solvent is one or a mixture of ODO solvent and olive oil.

Further, the ODO solvent and the olive oil are mixed in a mass ratio of 4-8: 1-5.

Further, the forming liquid contains deionized water and 1-2wt% of CaCl in the deionized water₂And span 20 with the weight of 3-5 per mill of deionized water.

Further, the crosslinking solution is 0.5-1.0% of chitosan solution or 4-5% of potassium persulfate solution.

A preparation method of the lemon mint flavor type blasting bead for cigarettes comprises the following steps:

s1, preparing deionized water phase solution: adding 1.0-2.0% of sodium alginate and 1.0-2.0% of Tween80 into deionized water, and fully and uniformly stirring to obtain a deionized water phase for later use;

s2, preparing an essence oil phase solution: adding the green lemon mint essence and one or two of ODO solvent or olive oil according to the proportion of 1: 8-10, uniformly stirring, and filtering by a 0.8nm ceramic membrane to obtain an essence oil phase for later use;

s3, emulsification: adding the essence oil phase solution and the deionized water phase solution according to the weight ratio of 2-4: 1, homogenizing at a high speed of 8000-11000 rpm for 5-10 min, and preparing into an emulsion;

s4, preparation of a molding liquid: adding CaCl according to 4-8% of the weight of the deionized water₂Adding span 20 in an amount which is 3-5 per mill of the weight of the deionized water, and fully and uniformly stirring to obtain a forming solution;

s5, dropping and forming: dripping the emulsion into the forming liquid at the speed of 3.0-6.0 ML/min by a plunger pump, and reacting for 6-15 minutes to prepare young pills;

s6, washing: putting the prepared young green lemon mint essence pills into deionized water, and washing off forming liquid on the surfaces of the young green lemon mint essence pills;

s7, crosslinking: putting the washed young pills into 0.5-1.0% chitosan solution or 4-5% potassium persulfate solution, and crosslinking for 20-40 minutes;

s8, drying: and (3) drying the crosslinked young pills in a roller to obtain the finished products of the green lemon mint flavor type popping pills.

Further, the drying temperature in the step 8 is 20-28 ℃, the drying humidity is 20-40% RH, and the drying time is 1-2 h.

According to the preparation method of the lemon mint flavor type bead blasting for the cigarettes and the preparation method thereof, the lemon mint flavor type bead blasting for the cigarettes is prepared through a series of bead blasting preparation processes of emulsification, dropping forming, washing, crosslinking, drying and the like, and the lemon mint flavor type bead blasting for the cigarettes can well wrap the lemon mint essence, is simple in production process and good in quality stability, and can meet the production requirements; the use of mechanical cutting molding is avoided in the preparation process, and the liquid emulsifying, crosslinking and dripping molding mode is adopted, so that the phenomena of eccentric beads, solid beads, bubble beads and the like are avoided, and the yield and the quality of products are effectively improved; meanwhile, the core liquid of the obtained blasting bead is effectively matched with the outer coating glue liquid through the molding liquid and the emulsion prepared by the invention, so that the phenomenon of coating and leakage is avoided.

Detailed Description

The invention will be further illustrated below with reference to specific examples. It should be understood that these examples are for illustrative purposes only and are not intended to limit the scope of the present invention. Furthermore, various changes or modifications of the present invention may be made by those skilled in the art, and equivalents may fall within the scope of the claims of the present application. The proportions in the examples of the invention are by weight.