阅读说明：本技术 含有6-糠氨基嘌呤和赤霉酸ga4+7可溶液剂及其制备方法 (Soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 and its prepn process ) 是由 朱朝印 包来仓 陈剑钊 韩建征 王建伟 *** 方业忠 于 2019-08-30 设计创作，主要内容包括：本发明涉及一种含有6-糠氨基嘌呤和赤霉酸GA4+7可溶液剂及其制备方法,该可溶液剂包括6-糠氨基嘌呤、赤霉酸GA4+7、表面活性剂和溶剂,各个成分的重量百分比为：6-糠氨基嘌呤1％～7％、赤霉酸GA4+71％～2％、表面活性剂1％～2％,余量为溶剂；所述表面活性剂取自十二烷基苯磺酸钠、硬脂酸、卵磷脂、脂肪酸甘油酯、聚山梨酯中的至少一种；溶剂取自可溶解6-糠氨基嘌呤的甲酸、苯甲酸、乙酸、丙酸、丁酸、碳酸、硬脂酸、二甲基甲酰胺、二甲基亚砜中的至少一种以及可溶解赤霉酸GA4+7的甲醇、乙醇中的至少一种。实现6-糠氨基嘌呤和赤霉酸GA4+7的合理配伍。避免了将6-糠氨基嘌呤和赤霉酸GA4+7制备成可湿粉剂导致的环境污染以及利用率低的问题。(The invention relates to a soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 and a preparation method thereof, wherein the soluble solution comprises 6-furfurylaminopurine, gibberellic acid GA4+7, a surfactant and a solvent, and the weight percentages of all the components are as follows: 1-7% of 6-furfuryl aminopurine, 1-2% of gibberellic acid GA4+ 71%, 1-2% of surfactant and the balance of solvent; the surfactant is at least one selected from sodium dodecyl benzene sulfonate, stearic acid, lecithin, fatty glyceride and polysorbate; the solvent is selected from at least one of formic acid, benzoic acid, acetic acid, propionic acid, butyric acid, carbonic acid, stearic acid, dimethyl formamide, and dimethyl sulfoxide capable of dissolving 6-furfuryl aminopurine, and at least one of methanol and ethanol capable of dissolving gibberellic acid GA4+ 7. Realizes the reasonable compatibility of the 6-furfuryl aminopurine and the gibberellic acid GA4+ 7. The problems of environmental pollution and low utilization rate caused by preparing the 6-furfurylaminopurine and the gibberellic acid GA4+7 into wettable powder are solved.)

1. A soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 is characterized by comprising 6-furfurylaminopurine, gibberellic acid GA4+7, a surfactant and a solvent, wherein the weight percentages of the components are as follows: 1-7% of 6-furfuryl aminopurine, 1-2% of gibberellic acid GA4+ 71%, 1-2% of surfactant and the balance of solvent; the surfactant is at least one selected from sodium dodecyl benzene sulfonate, stearic acid, lecithin, fatty glyceride and polysorbate; the solvent is selected from at least one of formic acid, benzoic acid, acetic acid, propionic acid, butyric acid, carbonic acid, stearic acid, dimethyl formamide, and dimethyl sulfoxide capable of dissolving 6-furfuryl aminopurine, and at least one of methanol and ethanol capable of dissolving gibberellic acid GA4+ 7.

2. The soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 as claimed in claim 1, wherein 6-furfurylaminopurine is 3.5%, gibberellic acid GA4+ 71.5%, surfactant 1.5%, and the balance is solvent.

3. A method for preparing a soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 according to claim 1, comprising the steps of:

(1) respectively weighing 6-furfuryl aminopurine and at least one of formic acid, benzoic acid, acetic acid, propionic acid, butyric acid, carbonic acid, stearic acid, dimethylformamide and dimethyl sulfoxide to completely dissolve the 6-furfuryl aminopurine in the solvent;

(2) weighing gibberellic acid GA4+7 and at least one of methanol and ethanol to completely dissolve the gibberellic acid GA4+7 in the solvent;

(3) uniformly mixing the two solutions in the steps (1) and (2), adding a surfactant, and finally adding ethanol or methanol to supplement the preparation amount;

(4) and (5) packaging the finished product after sampling inspection is qualified.

Technical Field

The invention relates to a soluble agent containing 6-furfuryl aminopurine and gibberellic acid GA4+7 and a preparation method thereof.

Background

Disclosure of Invention

The invention aims to provide a soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7, which aims to solve the problems of environmental pollution and low utilization rate of effective components caused by the fact that 6-furfurylaminopurine and gibberellic acid GA4+7 are adopted to prepare wettable powder in the prior art.

In order to achieve the purpose, the soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 adopts the following technical scheme:

a soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 comprises 6-furfurylaminopurine, gibberellic acid GA4+7, a surfactant and a solvent, wherein the weight percentages of the components are as follows: 1-7% of 6-furfuryl aminopurine, 1-2% of gibberellic acid GA4+ 71%, 1-2% of surfactant and the balance of solvent; the surfactant is at least one selected from sodium dodecyl benzene sulfonate, stearic acid, lecithin, fatty glyceride and polysorbate; the solvent is selected from at least one of formic acid, benzoic acid, acetic acid, propionic acid, butyric acid, carbonic acid, stearic acid, dimethyl formamide, and dimethyl sulfoxide capable of dissolving 6-furfuryl aminopurine, and at least one of methanol and ethanol capable of dissolving gibberellic acid GA4+ 7.

Further, 3.5% of 6-furfuryl aminopurine, 71.5% of gibberellic acid GA4, 1.5% of a surfactant and the balance of a solvent.

The preparation method of the soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 adopts the following technical scheme:

the preparation method of soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 comprises the following steps:

(1) respectively weighing 6-furfuryl aminopurine and at least one of formic acid, benzoic acid, acetic acid, propionic acid, butyric acid, carbonic acid, stearic acid, dimethylformamide and dimethyl sulfoxide to completely dissolve the 6-furfuryl aminopurine in the solvent;

(2) weighing gibberellic acid GA4+7 and at least one of methanol and ethanol to completely dissolve the gibberellic acid GA4+7 in the solvent;

(3) uniformly mixing the two solutions in the steps (1) and (2), adding a surfactant, and finally adding ethanol or methanol to supplement the preparation amount;

(4) and (5) packaging the finished product after sampling inspection is qualified.

The invention has the following beneficial effects: compared with the prior art, the soluble solution containing 6-furfurylaminopurine and gibberellic acid GA4+7 is prepared by designing the combination of 6-furfurylaminopurine, gibberellic acid GA4+7, a surfactant and a solvent in percentage by weight, and the corresponding solvent is prepared into the soluble solution, so that the problems of environmental pollution and low utilization rate caused by preparing the 6-furfurylaminopurine and the gibberellic acid GA4+7 into wettable powder are solved. Promoting flower bud differentiation and fruit enlargement.

Because the gibberellic acid GA4+7 original drug is insoluble in water and soluble in organic solvents such as alcohols, the preparation is easy to process into missible oil and soluble agent formulations; the 6-furfurylaminopurine is insoluble in water, alcohol, ether and acetone, so that the soluble solvent is prepared by dissolving two raw materials into different solvents respectively and then mixing the two raw materials together in the actual preparation process. Screening out proper solvent to realize reasonable compatibility of 6-furfuryl aminopurine and gibberellic acid GA4+ 7.

Detailed Description

In order to make the technical purpose, technical solutions and advantageous effects of the present invention more clear, the technical solutions of the present invention are further described below with reference to specific embodiments.

The soluble solvent containing 6-furfuryl aminopurine and gibberellic acid GA4+7 comprises 6-furfuryl aminopurine, gibberellic acid GA4+7, a surfactant and a solvent, wherein the solvent is at least one of formic acid, benzoic acid, acetic acid, propionic acid, butyric acid, carbonic acid, stearic acid, dimethylformamide and dimethyl sulfoxide capable of dissolving 6-furfuryl aminopurine, and at least one of methanol and ethanol capable of dissolving gibberellic acid GA4+7 is selected. Of course, in this example, ethanol is preferred to dissolve gibberellic acid GA4+ 7.