阅读说明：本技术 一种平抑血糖的罗汉果复配甜味剂及其制备方法 (A kind of Siraitia grosvenorii compound sweetener and preparation method thereof for stabilizing blood glucose ) 是由 李伟 黄华学 赵冠宇 刘永胜 叶桂芳 陈江林 黄�俊 贺进军 于 2019-09-24 设计创作，主要内容包括：一种平抑血糖的罗汉果复配甜味剂及其制备方法。本发明复配甜味剂包括罗汉果提取物、赤藓糖醇、桑叶DNJ、葫芦巴皂苷、茶多酚、酵母抽提物、柚皮苷和三氯蔗糖。本发明制备方法为：(1)将赤藓糖醇外的原料溶于热水中,过滤,将滤液真空减压浓缩,保温,得粘合剂；(2)将赤藓糖醇投入沸腾制粒机的流化床中,开启风机,并加热；(3)将粘合剂间歇喷入所述流化床,并保持所述流化床内物料沸腾,混合均匀；(4)喷入粘合剂结束后,保温干燥,静置冷却,得复配甜味剂。本发明的罗汉果复配甜味剂,除了复配甜味剂自身的优点外,还具有平抑血糖等有益的生理作用。本发明制备方法工艺稳定,设备简单,环保安全,无污染,适合大规模生产。(A kind of Siraitia grosvenorii compound sweetener and preparation method thereof for stabilizing blood glucose.Compound sweetener of the present invention includes Fructus Monordicae extract, antierythrite, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols, yeast extract, aurantiin and Sucralose.The preparation method comprises the following steps: the raw material outside antierythrite is dissolved in hot water by (1), filter vacuum is concentrated under reduced pressure the present invention for filtering, keeps the temperature, obtains adhesive；(2) by the fluidized bed of antierythrite investment fluid bed granulator, blower is opened, and heat；(3) adhesive interval is sprayed into the fluidized bed, and material in the fluidized bed is kept to boil, be uniformly mixed；(4) after spraying into adhesive, heat preservation and dryness stands cooling, obtains compound sweetener.Siraitia grosvenorii compound sweetener of the invention, in addition to the compound sweetener itself the advantages of other than, also have and stabilize the beneficial physiological action such as blood glucose.Preparation method process stabilizing of the present invention, equipment is simple, Environmental Safety, pollution-free, is suitble to large-scale production.)

1. a kind of Siraitia grosvenorii compound sweetener for stabilizing blood glucose, which is characterized in that including following components: Fructus Monordicae extract, red Moss sugar alcohol, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols, yeast extract, aurantiin and Sucralose.

2. having the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect according to claim 1, which is characterized in that by weight Meter, including following components: 0.1~11 part of Fructus Monordicae extract, 10~95 parts of antierythrite, 0.01~10 part of mulberry leaf DNJ, calabash 0.01~10 part of reed bar saponin(e, 0.01~10 part of tea polyphenols, 0.01~10 part of yeast extract, 0.01~10 part of aurantiin and three 0.01~10 part of chlorine sucrose.

3. according to claim 1 or claim 2 have the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect, which is characterized in that by weight Meter, including following components: 2~20 parts of Fructus Monordicae extract, 10~95 parts of antierythrite, 0.1~0.2 part of mulberry leaf DNJ, calabash 0.1~0.5 part of reed bar saponin(e, 0.1~0.5 part of tea polyphenols, 0.01~10 part of yeast extract, 0.01~10 part of aurantiin, three 0.01~10 part of chlorine sucrose.

4. having the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect described in -3 any one according to claim 1, which is characterized in that By weight, including following components: 2~20 parts of Fructus Monordicae extract, 60~90 parts of antierythrite, mulberry leaf DNJ 0.1~0.2 Part, 0.1~0.5 part of faenum graecum saponin(e, 0.1~0.5 part of tea polyphenols, 0.02~0.1 part of yeast extract, aurantiin 0.02~ 0.1 part, 0.05~4 part of Sucralose；Preferably, the glycosides V content in the Fructus Monordicae extract is 1.0~90.0%, the mulberry The content of leaf DNJ is 0.5~50%, and the content of the faenum graecum saponin(e is 10~50%；Preferably, the content of the tea polyphenols is 40~99%, the content of the aurantiin is 95~99%, and the content of the Sucralose is 98~100%.

5. there is the preparation method for the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect described in claim any one of 1-4, it is special Sign is, comprising the following steps:

(1) preparation of adhesive: by Fructus Monordicae extract, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols, yeast extract, shaddock ped Glycosides and Sucralose mixing, obtain mixed material, and after then mixed material is dissolved in hot water, filtering is depressurized filter vacuum dense Contracting, heat preservation, obtains adhesive；

(2) it preheats: by the fluidized bed of antierythrite investment fluid bed granulator, opening blower, and heat；

(3) it sprays into adhesive: the interval of adhesive obtained by step (1) being sprayed into the fluidized bed, and keeps object in the fluidized bed Material boiling, is uniformly mixed；

(4) dry and cooling: after having sprayed adhesive, heat preservation and dryness shuts down and stands cooling, obtains Siraitia grosvenorii compound sweetener.

6. having the preparation method for the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect according to claim 5, feature exists In in step (1), the dosage of the hot water is 10~20 times of mixed material gross mass；Preferably, the temperature of the hot water is 60~70 DEG C；Preferably, the filtering uses ceramic membrane filter, and the aperture of ceramic membrane is 0.05~0.5 μm.

7. having the preparation method for the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect, feature according to claim 5 or 6 Be, the condition of the vacuum-concentrcted is: temperature is 60~80 DEG C, and vacuum degree is -0.06~-0.08MPa, is concentrated into solid Until shape object content is 20~55%.

8. there is the preparation method for the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect according to claim any one of 5-7, It is characterized in that, the temperature of the heat preservation is 90~100 DEG C in step (1), the time is 1~2 hour.

9. there is the preparation method for the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect according to claim any one of 5-8, It is characterized in that, the temperature of the heating is 100~120 DEG C in step (2).

10. there is the preparation method for the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect according to claim any one of 5-8, It is characterized in that, described adhesive is divided into be sprayed into three times in step (3), the 40~50% of adhesive total amount is sprayed into for the first time, is mixed Close 8~10min；The 20~30% of second of penetrating adhesive total amount, mix 5~10min；Third time is whole by remaining adhesive It sprays into, mixes 10~20min.

Technical field

The present invention relates to Siraitia grosvenorii compound sweeteners and preparation method thereof, and in particular to a kind of Siraitia grosvenorii for stabilizing blood glucose is multiple With sweetener and preparation method thereof.

Background technique

Compound sweetener, refer to two or more natural or synthetic sweetener is compound, to reach comprehensive Close a kind of sweetener of sweetening effects.This compounding does not instead of simply mix various sweetener monomers, in conjunction with The technology compounding that the physilogical characteristics of synergistic effect and the sense of taste between various sweeteners carry out.

Since the sweetener of all kinds of single components cannot all meet safety, mouthfeel, technique, four Xiang Yaoqiu of cost simultaneously, all There are different aspect, in varying degrees the shortcomings that, but by compounding, mutual disadvantage can be made up, play mutual advantage. In addition, compounding between various sweeteners, there is likely to be synergistic effects, further promote the quality of sweetener.Therefore multiple An important development direction of sweetener exploitation, application will be become with sweetener.

But current compound sweetener production cost, flavour mouthfeel, health-care effect and in terms of all still In the presence of there are segmental defects.Such as:

CN102084982A discloses a kind of sweetener composition, and the composition contains Fructus Monordicae extract, STEVIA REBAUDIANA mentions Take object, neohesperidin dihydrochalcone and auxiliary material.The inventive method causes the composition to have due to having used qualities of stevia extract There is the defect in terms of the flavours such as rear bitter taste, metallic taste, and the composition is without nutrition health-care functions.

CN105338827A discloses a kind of composition and food, includes mogroside and antierythrite and rebaudioside A, rebaudioside B, rebaudioside C, Stevia rebaudiana D, rebaudioside E, rebaudioside M, sucrose, monatin, Talin, not in At least one of woods, Bu Laqiyin, l-Alanine, glycine, D-Psicose, hernandulcin, leaf stripe, trilobatin at Point.The compound sweetener complex process, it is with high costs, it is not suitable for industrialized production.

CN103906437A discloses a kind of sweetener composition, and for mitigating diabetes, the sweetener composition contains There are slowly digestible polysaccharide or anti-digestion polysaccharide as active constituent, further includes high intensity sweetner.Slowly digestible polysaccharide or The anti-digestion polysaccharide includes selecting from the group being made of isomaltulose, trehalose, anti-digestion maltodextrin and oligosaccharides At least one polysaccharide；High intensity sweetner includes from by steviol glycoside, Sucralose, aspartame, Fructus Monordicae extract, sweet At least one high intensity sweetner selected in the group that careless extract, Talin and American aloe syrup are constituted.The sweetener Composition heat is higher, is not suitable for diabetes patient's long-term consumption.

CN104996970A discloses a kind of compounding crystallization sweetener and preparation method thereof, and this method is successively by 0.8 weight 100-500 parts by weight water is added in part mogroside, 32-48 parts by weight antierythrite, 32-48 parts by weight isomalt In, it mixes, filtering, obtains compound sweetener solution, then program cooling, make compound sweetener solution sufficient crystallising, finally filter, Vacuum drying obtains compounding crystallization sweetener.The inventive method is adhered to mogroside on crystal by crystallization, there is knot Crystalline substance must generate mother liquor, there is mother liquor inherently shrink goals ingredient, and therefore, this method is to mogroside and other auxiliary materials Utilization rate is lower, and complex process, high production cost.

Summary of the invention

The technical problem to be solved by the present invention is to provide a kind of tool to overcome the above problem of the existing technology There is the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect.

The present invention is further the technical problem to be solved is that, provide a kind of with the Siraitia grosvenorii compounding for stabilizing blood glucose effect The preparation method of sweetener.Preparation method of the present invention is easy to operate, and used equipment is simple, is suitble to large-scale production.

The technical solution used to solve the technical problems of the present invention is that

It is a kind of with the Siraitia grosvenorii compound sweetener for stabilizing blood glucose effect, including following components: Fructus Monordicae extract, red moss Sugar alcohol, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols, yeast extract, aurantiin, Sucralose.

In the present invention, Fructus Monordicae extract derives from medicinal and edible plant --- Siraitia grosvenorii, has sugariness multiple height, zero Heat does not improve the advantages that blood glucose level.

In the present invention, antierythrite has the spies such as sugariness is low, stability is high, heat of solution is high, solubility is high, hygroscopicity is low Point, main function are to dilute the sugariness of the high Fructus Monordicae extract of sugariness multiple, and heat is almost nil, cool taste.

In the present invention, mulberry leaf DNJ, i.e. 1-DNJ are a kind of natural alkaloids derived from mulberry leaf, have and prolong Slow polysaccharide degradation process reduces Postprandial peak glucose, stablizes the physiological actions such as fasting blood-glucose.DNJ has other hypoglycemic products Incomparable advantage.

In the present invention, faenum graecum saponin(e derives from medicinal and edible plant --- faenum graecum, equally has hypoglycemic work With, in addition there are Adjust-blood lipid, weight-reducing the effect of.

In the present invention, tea polyphenols have blood pressure lowering, anticoagulation, reducing blood lipid obesity, prevent and treat artery sclerosis, is hypoglycemic, anti- The effects of controlling diabetes, sterilizing and anti-virus.

In the present invention, yeast extract has the function of fresh adding savoury, balance peculiar smell.

In the present invention, aurantiin has anti-inflammatory, antiviral, anticancer, antimutation, antiallergy, antiulcer, analgesia, drop blood The effects of pressure activity, energy hypercholesterolemia, the formation for reducing thrombus, improvement local microcirculation and nutrition supply.

In the present invention, Sucralose has the characteristics that empty calory, sugariness are high, sweet taste is pure, safe, to it is puckery, bitter etc. no Happy taste has cover effect.

In the present invention, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols synergistic effect have the function of stabilizing blood glucose.

In the present invention, faenum graecum saponin(e, tea polyphenols, yeast extract, aurantiin, Sucralose synergistic effect have and change The effect of the rear sweet taste of kind mogroside, can make the mouthfeel of compound sweetener identical with sucrose.

Including following components preferably, by weight: 0.1~11 part of Fructus Monordicae extract, 10~95 parts of antierythrite, 0.01~10 part of mulberry leaf DNJ, 0.01~10 part of faenum graecum saponin(e, 0.01~10 part of tea polyphenols, yeast extract 0.01~10 Part, 0.01~10 part of aurantiin, 0.01~10 part of Sucralose.

Preferably, by weight, including following components: 2~20 parts of Fructus Monordicae extract, 10~95 parts of antierythrite, mulberry 0.1~0.2 part of leaf DNJ, 0.1~0.5 part of faenum graecum saponin(e, 0.1~0.5 part of tea polyphenols, 0.01~10 part of yeast extract, 0.01~10 part of aurantiin, 0.01~10 part of Sucralose.

Preferably, by weight, including following components: 2~20 parts of Fructus Monordicae extract, 60~90 parts of antierythrite, mulberry 0.1~0.2 part of leaf DNJ, 0.1~0.5 part of faenum graecum saponin(e, 0.1~0.5 part of tea polyphenols, 0.02~0.1 part of yeast extract, 0.02~0.1 part of aurantiin, 0.05~4 part of Sucralose.

Preferably, the glycosides V content in the Fructus Monordicae extract is 1.0~90.0%, and the content of the mulberry leaf DNJ is 0.5~50%, the content of the faenum graecum saponin(e is 10~50%.

Preferably, the content of the tea polyphenols is 40~99%, and the content of the aurantiin is 95~99%, the trichlorine The content of sucrose is 98~100%

The present invention further solves its technical problem the technical scheme adopted is that a kind of with sieve for stabilizing blood glucose effect The preparation method of Chinese fruit compound sweetener, comprising the following steps:

(1) preparation of adhesive: by Fructus Monordicae extract, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols, yeast extract, Aurantiin and Sucralose mixing, obtain mixed material, and after then mixed material is dissolved in hot water, filter vacuum is depressurized in filtering Concentration, heat preservation, obtains adhesive；

(2) it preheats: by the fluidized bed of antierythrite investment fluid bed granulator, opening blower, and heat；

(3) it sprays into adhesive: the adhesive interval in step (1) being sprayed into the fluidized bed, and keeps the fluidized bed Interior material boiling, is uniformly mixed；

(4) dry and cooling: after having sprayed adhesive, heat preservation and dryness shuts down and stands cooling, obtains Siraitia grosvenorii compound sweetener.

Further, in step (1), the dosage of the hot water is 10~20 times of mixed material gross mass；The hot water Temperature is 60~70 DEG C.

Further, in step (1), the filtering uses ceramic membrane filter, and the aperture of ceramic membrane is 0.05~0.5 μm.

Further, in step (1), the condition of the vacuum-concentrcted is: temperature be 60~80 DEG C, vacuum degree be- 0.06~-0.08MPa, be concentrated into solid content be 20~55% until.

Further, in step (1), the temperature of the heat preservation is 90~100 DEG C, and the time is 1~2 hour.

In the present invention, the first purpose of soak is to make to interact between each ingredient, to play its collaboration Effect；The second purpose is sterilizing.

Further, in step (2), the temperature of the heating is 100~120 DEG C.

Further, in step (3), described adhesive is divided into be sprayed into three times, for the first time spray into adhesive total amount 40~ 50%, mix 8~10min；The 20~30% of second of penetrating adhesive total amount, mix 5~10min；Third time is viscous by residue Mixture all sprays into, and mixes 10~20min.

In the present invention, heat preservation and dryness, standing cooling can be realized by fluid bed granulator.

Compared with prior art, the invention has the following advantages: in (1) sweetener of the present invention, mulberry leaf DNJ, cucurbit Bar saponin(e and tea polyphenols compounding have synergistic effect to blood glucose is stabilized, under lower content, still stabilize blood glucose with excellent Effect can be used as the sucrose that sweetener substitution heat is high, sugar content is high and add in daily bread or functional health-care food, with It is edible for diabetic population and obese people；(2) raw material that sweetener of the present invention is selected is green, environmentally friendly, safe, and nontoxic pair is made With, alternative sucrose, and the adverse consequences such as blood glucose rise, obesity, saprodontia because of caused by sucrose will not be brought；

(3) preparation method Fructus Monordicae extract of the present invention, mulberry leaf DNJ, faenum graecum saponin(e, tea polyphenols, yeast extract, shaddock The concentrate of the hydrothermal solution of skin glycosides and Sucralose is adhesive, so that each raw material is easier to be uniformly mixed；Further, also right Adhesive has carried out continuing to keep the temperature, it has been investigated that, this insulating process also further promoted mulberry leaf DNJ, faenum graecum saponin(e and Tea polyphenols three to stabilize blood glucose synergistic effect；

(4) process stabilizing of preparation method of the present invention, required equipment is simple, and Environmental Safety is pollution-free, is suitble to extensive raw It produces.

Specific embodiment

The present invention will be described in detail by the following examples.In following embodiment, ceramic membrane is purchased from Nanjing forint moral Environmental Protection Technology Co., Ltd；

Fluid bed granulator is purchased from Changzhou drying equipment Co., Ltd step by step；

Glycosides V content in Fructus Monordicae extract is measured by high performance liquid chromatography (HPLC) external standard method method；

Fructus Monordicae extract is purchased from Hunan Hua Cheng living resources limited liability company, and the form of Fructus Monordicae extract is concentration Liquid or dry powder, wherein the content of glycosides V is 3.52% in Fructus Monordicae extract concentrate, and glycosides V's contains in Fructus Monordicae extract dry powder Amount is 51.02%；

In case of no particular description, other materials is all made of ordinary commercial products.Wherein, the content of antierythrite It is 98.25%, the content of mulberry leaf DNJ is 25.30%, and the content of faenum graecum saponin(e is 15.06%, and the content of tea polyphenols is 60.52%, the content of aurantiin is 98.72%, and the content of Sucralose is 99.96%.