阅读说明：本技术 一种油包水包油霜的制备方法 (A kind of preparation method of Water-In-Oil packet bloom ) 是由 黄战捷 冷军程 蔡波 于 2019-09-19 设计创作，主要内容包括：本发明提供一种油包水包油霜的制备方法,其制备步骤包括：将所述水相升温至80-90℃,搅拌均匀至无颗粒物；将所述第一油相加入所述水相中,开启均质3-5分钟后,降温至40-45℃,得到水包油相；将所述水包油相分多次缓慢加入所述第二油相中,并进行低速搅拌,待所述水包油相剩下重量百分比为15%-25%时,将剩下的所述水包油相全部加入,同时进行中速搅拌,使所述水包油相全部被所述第二油相全部包住,得到油包水包油相；将所述助剂加入所述油包水包油相,同时进行低速搅拌均匀后,再进行高速搅拌或低速均质,在温度为20-40℃下调整粘稠度至80000 mPa.s以上,得到油包水包油霜,所得油包水包油霜具有良好肤感且不油腻。(The present invention provides a kind of preparation method of Water-In-Oil packet bloom, and preparation step includes: that the water phase is warming up to 80-90 DEG C, is evenly stirred until no particulate matter；First oil is added in the water phase, after opening homogeneous 3-5 minutes, 40-45 DEG C is cooled to, obtains oil-in-water phase；The oil-in-water is mutually slowly added to several times in the described second oily phase, and it is stirred at low speed, when it is 15%-25% that the oil-in-water, which is mutually left weight percent, the remaining oil-in-water is mutually all added, moderate-speed mixer is carried out simultaneously, it encases the oil-in-water mutually all mutually all by second oil, obtains Water-In-Oil packet oil phase；The Water-In-Oil packet oil phase is added in the auxiliary agent, after being stirred at low speed simultaneously, then high-speed stirred or low speed homogeneous are carried out, adjusts viscosity to 80000 mPa.s or more at being 20-40 DEG C in temperature, Water-In-Oil packet bloom is obtained, gained Water-In-Oil packet bloom has good skin sense and non-greasy.)

1. a kind of preparation method of Water-In-Oil packet bloom, which is characterized in that its raw material is in parts by weight are as follows: 72-88 parts of water phase, One oily 3.7-6.8 parts of phase, the second oily 7.5-9.8 parts and 1-2 parts of auxiliary agent of phase, preparation step is as follows:

Water phase preparation step: the water phase is warming up to 80-90 DEG C, is evenly stirred until no particulate matter；

Oil-in-water phase preparation step: first oil is added in the water phase, after opening homogeneous 3-5 minutes, is cooled to 40- 45 DEG C, obtain oil-in-water phase；

Water-In-Oil packet oil phase preparation step: the oil-in-water is mutually slowly added in the described second oily phase several times, and carried out low The remaining oil-in-water is mutually all added when it is 15%-25% that the oil-in-water, which is mutually left weight percent, for speed stirring, Moderate-speed mixer is carried out simultaneously, the oil-in-water is encased mutually all mutually all by second oil, obtains Water-In-Oil packet oil phase；

Finished product preparation step: being added the Water-In-Oil packet oil phase for the auxiliary agent, while after being stirred at low speed, then carries out High-speed stirred or low speed homogeneous, adjustment viscosity obtains Water-In-Oil packet to 80000 mPa.s or more at being 20-40 DEG C in temperature Bloom.

2. the preparation method of Water-In-Oil packet bloom as described in claim 1, which is characterized in that the water phase includes deionization Water, EDETATE SODIUM, glycerol, propylene glycol, xanthan gum, Sodium Hyaluronate, magnesium sulfate and sodium chloride, first oil mutually includes laurel Alcohol polyethers -7, citrate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, dimethyl silicone polymer, isononyl isononanoate, the described second oily phase Including ring five dimethyl silicone polymer, dimethyl silicone polymer, silica, cetyl PEG/PPG-10/1 polydimethylsiloxanes Alkane, PEG-10 dimethyl silicone polymer.

3. the preparation method of Water-In-Oil packet bloom as claimed in claim 2, which is characterized in that the dimethyl silicone polymer can Ring five dimethyl silicone polymer is replaced with, the octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester can be replaced saualane or isomery hexadecane, described Ring five dimethyl silicone polymer shell can be replaced C9-11 isoparaffin or C10-13 isoparaffin, and the auxiliary agent is preservative, perfume (or spice) One or both of essence is mixed with arbitrary proportion.

4. the preparation method of Water-In-Oil packet bloom as claimed in claim 2, which is characterized in that all components are in parts by weight Are as follows: water phase: 36-52 parts of deionized water, 0.01-0.02 parts of EDETATE SODIUM, 10-15 parts of glycerol, 25-30 parts of propylene glycol, xanthan gum 0.1-0.2 parts, 0.02-0.05 parts of Sodium Hyaluronate, 0.2-0.5 parts of magnesium sulfate, 0.2-0.5 parts of sodium chloride；First oily phase: laurel 0.7-0.8 parts of -7 citrate of alcohol polyethers, octanoic acid/1-2 parts of certain herbaceous plants with big flowers acid glycerol three ester, 1-2 parts of dimethyl silicone polymer, isononanoic acid 1-2 parts of different nonyl ester；

Second oily phase: five 3-4 parts of dimethyl silicone polymers, 3-4 parts of dimethyl silicone polymer, 0.1-0.2 parts of silica, cetyl 0.7-0.8 parts of PEG/PPG-10/1 dimethyl silicone polymer, 0.7-0.8 parts of PEG-10 dimethyl silicone polymer.

5. the preparation method of Water-In-Oil packet bloom as described in claim 1, which is characterized in that mutually prepare step in the oil-in-water It further include after mutually having weighed first oil, the step of being warming up to 75-85 DEG C, be evenly stirred until no particulate matter before rapid.

6. the preparation method of Water-In-Oil packet bloom as described in claim 1, which is characterized in that mutually made in the Water-In-Oil packet oil Before standby step, further include the steps that mutually mixing is uniformly dispersed at normal temperature by second oil.

7. the preparation method of Water-In-Oil packet bloom as described in claim 1, which is characterized in that the Water-In-Oil packet oil is mutually prepared In step, the mixing speed stirred at low speed is 50-200rpm, and the mixing speed of the moderate-speed mixer is 200-500rpm.

8. the preparation method of Water-In-Oil packet bloom as described in claim 1, which is characterized in that in the finished product preparation step, The mixing speed stirred at low speed is 50-200rpm, and the mixing speed of the high-speed stirred or low speed homogeneous is 500- 1000rpm。

9. the preparation method of Water-In-Oil packet bloom as described in claim 1, which is characterized in that the Water-In-Oil packet oil is mutually prepared In step, the oil-in-water, which mutually at least divides 4 times, to be added in the described second oily phase, and the oil-in-water phase is added every time and stirs to it Another oil-in-water phase is added after being completely encased.

Technical field

The invention belongs to cosmetic fields, and the present invention relates to a kind of preparation methods of Water-In-Oil packet bloom.

Background technique

The more water contents of water-in-oil type oil content are fewer, and oil components coat water composition, and foreign minister is mostly oil mutually frost Shape, when smearing feel to compare stiff, and closure is stronger, can lock moisture and not be lost.On the market in skin care item title band " frost ", Printed words such as " cream " are mostly Water-In-Oil quality.Be conducive to water lock, moisturizing, tough skin barrier, resist extraneous infringement, protects on the market What the skin name of an article claimed the printed words such as middle band " frost ", " cream " is mostly Water-In-Oil quality, is conducive to water lock, moisturizing, tough skin barrier is resisted External world's infringement.Oil-in-water type is usually that water content is relatively high and oil content is relatively low, and aqueous component coats oil component, Wai Xiangwei Aqueous phase liquid is in the majority, uses and feels more salubrious, on the market the band printed words such as " cream ", " dew ", " honey " in skin care item title Mostly oil-in-water quality, quality is relatively slim and graceful salubriouser, is translucent, and the ratio of water is bigger than oil.

With the improvement of living standards, the requirement to skin care item is also higher and higher, simple water-in-oil type or oil-in-water type Skin care item are not able to satisfy all consumer demands, and many consumers intentionally get skin sense non-greasy and the strong skin care of humidity-preserving type Product substitute existing " cream " or " frost " class skin care item.

Summary of the invention

For the shortcomings of the prior art, the present invention provides a kind of preparation method of Water-In-Oil packet bloom, It is achieved through the following technical solutions:

A kind of preparation method of Water-In-Oil packet bloom, raw material are 72-88 parts of water phase, the first oily phase 3.7- in parts by weight 6.8 parts, the second oily 7.5-9.8 parts and 1-2 parts of auxiliary agent of phase, preparation step is as follows:

Water phase preparation step: the water phase is warming up to 80-90 DEG C, is evenly stirred until no particulate matter.

Oil-in-water phase preparation step: first oil is added in the water phase, after opening homogeneous 3-5 minutes, cooling To 40-45 DEG C, oil-in-water phase is obtained.

Water-In-Oil packet oil phase preparation step: the oil-in-water is mutually slowly added in the described second oily phase several times, is gone forward side by side It is capable to stir at low speed, when it is 15%-25% that the oil-in-water, which is mutually left weight percent, the remaining oil-in-water is mutually all added Enter, while carrying out moderate-speed mixer, encases the oil-in-water mutually all mutually all by second oil, obtain Water-In-Oil packet oil Phase.

Finished product preparation step: being added the Water-In-Oil packet oil phase for the auxiliary agent, while after being stirred at low speed, then High-speed stirred or low speed homogeneous are carried out, viscosity is adjusted when temperature is 20-40 DEG C to 80000 mPa.s or more, obtains oily packet Oil-in-water frost.

It is warming up to 80-90 ° after water phase has been weighed, for stirring and dissolving uniformly to no particulate matter, it is to allow water phase group that this, which is walked, Divide and be adequately swollen at a suitable temperature, is completely dispersed and is dissolved in water.First oil is added to during water phase adds, is opened Homogeneous, homogeneous 3-5min keep water phase fully emulsified in the first oily phase, form the oil-in-water phase of emulsion form, then cool the temperature to 40-45 DEG C, reduce temperature be in order in the step of next step Water-In-Oil oil phase, be ensured of carry out at a lower temperature it is cold Packet.Water-In-Oil packet oil phase preparation step makes the second oil mutually slowly sufficiently encase oil-in-water phase at the beginning using stirring at low speed.It helps Agent is added and is then turned on high-speed stirred or low speed homogeneous after mixing evenly, its viscosity is made to increase, when temperature is 20-40 DEG C Stop stirring when having detected viscosity more than or equal to 80000mPas, viscosity setting value is to allow the product knot of water-in-oil system It is complexed more stable between structure, is firm, to reach guarantee product stability, extending the effect of shelf time, qualification to be detected (up to standard, fragrance of viscosity etc. meets the requirements) can discharge afterwards, can obtain this product.

Further, the water phase include deionized water, EDETATE SODIUM, glycerol, propylene glycol, xanthan gum, Sodium Hyaluronate, Magnesium sulfate and sodium chloride, first oil mutually includes laureth -7, citrate, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, poly- diformazan Radical siloxane, isononyl isononanoate, it is described second oil mutually include ring five dimethyl silicone polymer, dimethyl silicone polymer, silica, Cetyl PEG/PPG-10/1 dimethyl silicone polymer, PEG-10 dimethyl silicone polymer.

Further, the dimethyl silicone polymer can be replaced ring five dimethyl silicone polymer, and the octanoic acid/certain herbaceous plants with big flowers acid is sweet Oily three esters can be replaced saualane or isomery hexadecane, and the ring five dimethyl silicone polymer can be replaced C9-11 isoparaffin Or C10-13 isoparaffin, the auxiliary agent are that one or both of preservative, essence are mixed with arbitrary proportion.

Further, all components are in parts by weight are as follows: water phase: 36-52 parts of deionized water, EDETATE SODIUM 0.01-0.02 Part, 10-15 parts of glycerol, 25-30 parts of propylene glycol, 0.1-0.2 parts of xanthan gum, 0.02-0.05 parts of Sodium Hyaluronate, magnesium sulfate 0.2- 0.5 part, 0.2-0.5 parts of sodium chloride；First oily phase: 0.7-0.8 parts of -7 citrate of laureth, octanoic acid/certain herbaceous plants with big flowers acid glycerol three 1-2 parts of ester, 1-2 parts of dimethyl silicone polymer, 1-2 parts of isononyl isononanoate；Second oily phase: five 3-4 parts of dimethyl silicone polymers, 3-4 parts of dimethyl silicone polymer, 0.1-0.2 parts of silica, cetyl PEG/PPG-10/1 dimethyl silicone polymer 0.7-0.8 Part, 0.7-0.8 parts of PEG-10 dimethyl silicone polymer.

It further, further include heating after mutually having weighed first oil before the oil-in-water phase preparation step To 75-85 DEG C, the step of being evenly stirred until no particulate matter.

The temperature of first oily heat phase is unsuitable excessively high, excessively high to make caprylic/capric triglyceride in oil phase component, poly- diformazan Radical siloxane volatilizees at too high a temperature, generates bad grease smell, too low, the dissolution that is unable to fully with water phase, liquid Change.

Further, before the Water-In-Oil packet oil phase preparation step, further include by it is described second oil mutually at normal temperature The step of mixing is uniformly dispersed.

Second oily phase is sufficiently mixed at normal temperature, without heating, preferably uses high speed homogenization to carry out uniformly mixed, Be no longer heat up, then in the preparation step that Water-In-Oil packet oil is thought before do not need to be cooled down again, it is time saving and energy saving.

Further, in the Water-In-Oil packet oil phase preparation step, the mixing speed stirred at low speed is 50- 200rpm, the mixing speed of the moderate-speed mixer are 200-500rpm.

Further, in the finished product preparation step, the mixing speed stirred at low speed is 50-200rpm, the height The mixing speed of speed stirring or low speed homogeneous is 500-1000rpm.

Further, in the Water-In-Oil packet oil phase preparation step, the oil-in-water, which mutually at least divides 4 times, is added described second In oily phase, be added every time the oil-in-water phase and stir be completely encased to it after add another oil-in-water phase.Point At least 4 times additions could preferably make the second oil mutually adequately encase water phase, and product is more stable.

The utility model has the advantages that Water-In-Oil packet bloom moistening effect prepared by preparation method of the present invention is good and non-greasy, existing frost class The high moistening effect of product, and have the salubrious sense of type of latex type product, consumer's usage experience is good.This preparation method strict control is each Mixing speed and temperature in step, structure of title compound is more stable, homogeneous and free from extraneous odour.

Specific embodiment