阅读说明：本技术 一种预防肠炎的茶油及其制备方法 (Tea oil for preventing enteritis and preparation method thereof ) 是由 管敏 管天球 管斌 管晖 于 2020-12-10 设计创作，主要内容包括：本发明公开的一种预防肠炎的茶油,涉及生物医药和食品加工技术领域,是由包括以下重量份的原料制备而成：茶油80-90、中药叶粉2-5、中药花粉2-7、水果粉4-10、中药皮粉2-5、添加剂1-3；其制备过程如下：⑴、备料；⑵、混合一；⑶、混合二；⑷、混合三；⑸、混合四；⑹、总混合；⑺、精滤。具有营养价值较高、能够预防肠炎等特点,适合于各个年龄层次的人们食用。(The invention discloses tea oil for preventing enteritis, which relates to the technical field of biological medicine and food processing and is prepared from the following raw materials in parts by weight: 80-90 parts of tea oil, 2-5 parts of traditional Chinese medicine leaf powder, 2-7 parts of traditional Chinese medicine pollen, 4-10 parts of fruit powder, 2-5 parts of traditional Chinese medicine peel powder and 1-3 parts of additive; the preparation process comprises the following steps: preparing materials; the first step is mixing; performing mixing; fourthly, mixing the materials; fifthly, mixing; sixthly, totally mixing; and (4) calming and fine filtering. Has high nutritive value, can prevent enteritis, and is suitable for people of all ages.)

1. The tea oil for preventing enteritis is characterized by being prepared from the following raw materials in parts by weight:

tea oil 80-90 Chinese medicinal leaf powder 2-5 Chinese medicinal pollen 2-7

Fruit powder 4-10, Chinese medicinal peel powder 2-5, additive 1-3;

the traditional Chinese medicine leaf powder comprises one or more of rosemary leaf powder, roxburgh rose leaf powder, buckwheat leaf powder and bamboo leaf powder which are mixed with livestock and poultry blood powder, garlic leaf powder and dandelion leaf powder according to the equal weight proportion, and the weight ratio of the traditional Chinese medicine leaf powder to the livestock and poultry blood powder is 5-6.5: 1: 0.1-0.35: 0.4-0.6 by weight ratio;

the Chinese medicinal pollen comprises one or more of tea tree pollen, gardenia bud powder and peony pollen mixed according to equal weight proportion, and is mixed with breviscapine pollen, momordica grosvenori pollen, salvia miltiorrhiza pollen and substitutional pollen according to the weight proportion of 0.2-0.35:1:0.5-0.6:0.45: 0.1;

the fruit powder comprises one or more of apple powder and mangosteen powder mixed according to equal weight proportion, and garlic root hair powder, bone soup powder and fish skin powder mixed according to weight proportion of 2-3.3:0.1:1.5-2: 0.4;

the traditional Chinese medicine peel powder comprises one or more of white fresh peel powder, ash peel powder and asparagus lettuce peel powder which are mixed according to equal weight proportion, and is mixed with grape peel powder, orange peel powder and sugarcane peel powder according to the weight proportion of 0.3-0.45:2-3:0.2: 1;

the additive is prepared from dietary fiber, riboflavin and nicotinic acid according to the weight ratio of 1.2-2.0: 0.1-0.25: 0.05-0.12 weight ratio.

2. The tea oil for preventing enteritis according to claim 1, wherein the traditional Chinese medicine leaf powder is prepared by the following method:

the method comprises the following steps of:

preparing rosemary leaf powder: pulverizing distilled rosemary leaves into rosemary leaf coarse powder of 8-15 meshes, then putting the coarse powder into a low-polarity organic solvent with the weight being 2-4 times that of the coarse powder, soaking the coarse powder at normal temperature until the solid content in the solvent is 0.8-1.4mg/ml, filtering the solution, and collecting rosemary leaf solvent liquid; mixing the rosemary leaf solvent solution with a decolorizing agent accounting for 5-8% of the weight of the rosemary coarse powder, sealing and stirring at 35-45 ℃ for 30-60min, transferring to a concentrator, concentrating under vacuum to 40-50% of the original volume of the rosemary leaf solvent solution, filtering while hot, and collecting the rosemary leaf decolorizing solvent solution; adding pure water with the same weight into the rosemary leaf decolorization solvent liquid, stirring uniformly, transferring to a refrigeration house, refrigerating for 15-20h at 0-10 ℃, then extracting the organic solvent in the rosemary leaf decolorization solvent liquid, filtering the rest liquid and precipitate, and collecting rosemary leaf extract precipitate; washing the rosemary leaf extract precipitate with boiling water for 2-3 times, drying and crushing the washed rosemary leaf extract precipitate to obtain rosemary leaf powder, and preserving at 10-24 ℃ for later use;

② preparation of roxburgh rose leaf powder: mixing the roxburgh rose leaves with an inorganic salt solution with the same weight and the mass fraction of 3.5-5.5% to prepare coarse roxburgh rose leaf slurry of 10-20 meshes, adjusting the pH value of the slurry to be neutral by using an alkaline water solution with the mass fraction of 0.8-1.5%, filtering, and collecting roxburgh rose leaf filter residues; adding the roxburgh rose leaf filter residue into ethanol solution with the same weight and volume concentration of more than 80%, soaking until the solid content in the ethanol is 0.3-0.55mg/ml, filtering, and collecting roxburgh rose leaf ethanol solution; concentrating the ethanol solution of folium Rosae Normalis until the solid content is 5.6-7.5mg/ml, transferring into a refrigerator, refrigerating at 0-10 deg.C to remove precipitate, and collecting the liquid to obtain folium Rosae Normalis precipitate; washing the Rosa roxburghii leaf precipitate with 0.1-0.25% sodium bicarbonate water solution for 2-3 times, and washing with boiling water for 2-3 times to obtain Rosa roxburghii leaf washing precipitate; washing the roxburgh rose leaf, drying and crushing to obtain roxburgh rose leaf powder, and preserving at 10-24 ℃ for later use;

preparing buckwheat leaf powder: cleaning fresh semen Fagopyri Esculenti, transferring to microwave dryer, treating at 35-48 deg.C for 50-70min, spreading inorganic salt solution with mass fraction of 0.5-0.75% onto folium Fagopyri Esculenti surface every 10-15min, each time the amount is 5.0-9.0% of folium Fagopyri Esculenti weight, to obtain treated folium Fagopyri Esculenti; adding the treated folium Fagopyri Esculenti into a cooking pot filled with 2-3 times of clear water, cooking with slow fire until the solid content of the water solution is 0.2-1.2mg/ml, and filtering to obtain folium Fagopyri Esculenti water solution; adding decolorizer 1.2-1.8 wt% of the folium Fagopyri Esculenti water solution, stirring at 35-40 deg.C for 30-40min, and filtering to obtain decolorized folium Fagopyri Esculenti water solution; concentrating, drying, and pulverizing the decolorized buckwheat leaf water solution to obtain buckwheat leaf powder, and preserving at 10-24 deg.C;

fourthly, preparing the bamboo leaf powder: cleaning folium Bambusae, adding into ethanol solution with weight 2-4 times and volume concentration of above 70%, soaking at 45-55 deg.C until the solid content in ethanol is 1.55-2.25mg/ml, filtering, and collecting folium Bambusae ethanol solution; diluting the folium Bambusae ethanol solution with 0.3-0.45% sodium carbonate water solution to obtain diluted folium Bambusae ethanol solution with solid content of 0.7-1.0mg/ml and pH value of 7.5-8.5; adding low-polarity organic solvent with the same volume into diluted bamboo leaf ethanol solution, stirring at normal temperature for 10-18min, standing, layering, and collecting supernatant; concentrating the supernatant under vacuum until no alcohol exists to obtain concentrated bamboo leaf extract; adjusting pH of the concentrated folium Bambusae extract to 6-6.5 with 1.6-3.2 wt% inorganic acid solution, transferring into a refrigerator, refrigerating for 10-15 hr, filtering, and collecting folium Bambusae extract precipitate; drying and pulverizing the bamboo leaf extract precipitate to obtain bamboo leaf powder, and preserving at 10-24 deg.C;

fifth, preparing the livestock and poultry blood powder: preheating fresh livestock and fowl blood to 50-60 deg.C, adding 3.5-4.5 wt% of inorganic saline solution with concentration of 0.5-0.9% and 0.5-1.2% of dispersant, stirring, treating at constant temperature for 20-35min, filtering with 10-20 μm filter membrane device, collecting filtered livestock and fowl blood water solution, introducing into adsorption column at addition rate of 15-24L/h, standing for 5-8h after the livestock and fowl blood water solution is completely added, heating blood in the adsorption column to 50-60 deg.C with jacket, controlling flow rate at 30-45ml/min, collecting effluent livestock and fowl blood water solution, concentrating at 70-80 deg.C under pressure of 5-10KPa to solid content of 28.5-32.5mg/ml, obtaining concentrated livestock and fowl blood water solution, and adding edible ethanol while hot, adjusting the alcohol degree to 60%, stirring for 10-15min, transferring to a cold storage, standing at-4-0 deg.C for 4-7h, adding inorganic salt 0.5-1.2% of the weight of the livestock blood, stirring, standing for 2-3h, filtering, collecting the upper clear ethanol solution of livestock blood, concentrating at 60-75 deg.C under 5-10KPa to obtain a concentrated livestock blood solution with a solid content of 12.5-15.5mg/ml, adding organic solvent with the same volume, stirring and extracting at room temperature for 10-15min, standing, layering, collecting the organic solvent extractive solution, concentrating, drying, and pulverizing to obtain livestock blood powder;

sixthly, preparing the garlic leaf powder: naturally drying fresh garlic leaves until the garlic leaves turn yellow, then crushing the garlic leaves into fine powder with the particle size of more than 60 meshes, transferring the fine powder into boiling water with the weight of 2-4 times of the garlic leaves, carrying out heat preservation and stirring treatment until the solid content in water liquid is 0.7-1.9mg/ml and the carotene content is higher than 0.05mg/ml, filtering, and collecting water extract of the garlic leaves; concentrating, drying and pulverizing the water extractive solution of Bulbus Allii leaf to obtain Bulbus Allii leaf powder, and preserving at 10-24 deg.C;

preparing dandelion leaf powder: selecting dandelion leaf powder which is extracted from dandelion leaves, has the phylloquinone content of more than 8.5 percent, the lutein content of more than 22.5 percent, the vitamin content of 1.5-3.2mg/10g and the residual amount of ethanol solvent of less than 3.5ppm, and preserving at 10-24 ℃ for later use;

the preparation method comprises the following steps: mixing one or more of the above herba Rosmarini officinalis leaf powder, folium Rosae Normalis powder, folium Fagopyri Esculenti powder, and folium Bambusae powder with livestock and fowl blood powder, Bulbus Allii leaf powder, and herba Taraxaci leaf powder at corresponding weight ratio, and preserving at 10-24 deg.C.

3. The tea oil for preventing enteritis according to claim 1, wherein the traditional Chinese medicine pollen is prepared by the following method:

the method comprises the following steps of:

firstly, preparing tea tree pollen: taking fresh tea flowers, and separating tea petals from tea pistils; firstly, soaking tea tree petals in 5-8.5% of vinegar solution for 8-15min, then washing with clear water for 2-3 times, then transferring to a drying oven, and drying at 60-70 ℃ until the water content is less than 5% to obtain dried tea tree petals; putting tea plant pistils into a distiller, simultaneously adding pure water which accounts for 8-12 times of the weight of the tea plant pistils into the distiller, uniformly stirring, distilling until the water volume is reduced by 40-45%, and collecting tea plant pistils distillate; mixing dried tea petal with tea stamen distillate, boiling for 20-32min, filtering, and collecting tea flower water solution; then, concentrating, drying and crushing the tea flower water solution to obtain tea flower pollen for later use;

② preparing gardenia bud powder: grinding the prepared gardenia buds into gardenia bud coarse powder with the particle size of more than 10 meshes, then dripping ammonia water with the mass concentration of 3.5-5.5% according to the proportion of 6-8 drops/20 g, uniformly stirring, transferring into a microwave dryer, and treating at the temperature of 45-50 ℃ for 22-28min to obtain microwave-treated gardenia bud coarse powder; transferring the microwave-treated fructus Gardeniae bud coarse powder into 1.5-3.5 wt% sodium hydrogen phosphate solution, stirring at 40-52 deg.C for 5-15min, and filtering to obtain treated fructus Gardeniae bud powder; adding the treated fructus Gardeniae bud powder into 1-3 times of pure water, steaming with 50-55 deg.C slow fire until pH value of the water solution is 4.8-5.5, and filtering to obtain fructus Gardeniae bud powder water solution; concentrating, drying and pulverizing the water solution of the gardenia bud powder to obtain gardenia bud powder for later use;

③ preparing peony pollen: soaking flos Paeoniae in ethanol solution with volume concentration of 50% or more and weight of 1.5-3.0 times of the flos Paeoniae at 50-65 deg.C until the solid content in the ethanol solution is 3.2-4.2mg/ml to obtain flos Paeoniae ethanol soaking solution; adding decolorizing agent 1.2-1.5% of the original weight of flos Paeoniae into the flos Paeoniae ethanol soaking solution, stirring at 40-50 deg.C for 30-45min, filtering, and collecting decolorized flos Paeoniae ethanol solution; concentrating, drying and crushing the decolorized peony flower ethanol solution to obtain peony flower powder for later use;

preparing erigeron breviscapus pollen: firstly, putting the erigeron breviscapus into 0.3-0.5% sodium bicarbonate aqueous solution with the weight of 1-2.5 times of that of the erigeron breviscapus, soaking for 25-40min at normal temperature, and filtering to obtain the treated erigeron breviscapus; then the treated erigeron breviscapus is transferred into boiling water with the same weight, and is stirred back and forth for 8-12min, and is filtered to obtain the erigeron breviscapus treated by the boiling water; adding boiling water-treated flos Hibisci into edible ethanol solution with weight 2-3 times and volume concentration above 35%, soaking at 50-65 deg.C until erigeron content in the ethanol solution is 0.11-0.18mg/ml, and filtering to obtain flos Hibisci ethanol soaking solution; vacuum concentrating the ethanol soaking solution at low temperature until the content of erigeron breviscapus glycoside is 0.8-1.25mg/ml to obtain erigeron breviscapus ethanol concentrated solution; transferring the concentrated solution into a refrigerator, refrigerating at 4-8 deg.C until no precipitate is separated out, filtering, and collecting the upper layer of herba Erigerontis liquid; spray drying the erigeron breviscapus liquid to obtain erigeron breviscapus powder for later use;

fifthly, preparing momordica grosvenori pollen: cleaning flos Momordicae, soaking in 30-45% ethanol solution at 45-55 deg.C until the content of saccharide in the ethanol solution reaches 0.03-0.1mg/ml, and filtering to obtain flos Momordicae ethanol soaking solution; adding a decolorizing agent accounting for 0.3-0.6% of the weight of the original momordica grosvenori flower into the momordica grosvenori flower ethanol soaking solution, stirring for 10-15min, filtering by a 0.5 micron filter membrane device, and collecting momordica grosvenori flower ethanol soaking filtrate; soaking the momordica grosvenori flower in ethanol, concentrating and drying the filtrate to obtain momordica grosvenori pollen for later use;

sixthly, preparing salvia miltiorrhiza pollen: soaking Salvia miltiorrhiza flower in ethanol solution with 1.5-3.0 times weight and volume concentration of more than 50% at 50-65 deg.C until the solid content in ethanol solution is 0.8-1.35mg/ml to obtain Salvia miltiorrhiza flower ethanol soaking solution; adding a decolorizing agent accounting for 0.5-0.75% of the original weight of the salvia miltiorrhiza flower into the salvia miltiorrhiza flower ethanol soaking solution, stirring at 40-50 ℃ for 10-15min, filtering, and collecting the salvia miltiorrhiza flower ethanol soaking decolorizing solution; then the ethanol-soaked destaining solution of the salvia miltiorrhiza flowers is concentrated, dried and crushed to obtain salvia miltiorrhiza pollen for later use;

and seventhly, preparing substitute pollen: firstly, mixing the seville orange flower with pure water of which the weight is 4-6 times that of the seville orange flower, putting the mixture into a distillation container, carrying out distillation treatment for 1.0-1.5h at the temperature of 100 ℃ and 110 ℃, taking out and draining to obtain the distilled seville orange flower; drying and crushing the distilled bitter orange to obtain bitter orange powder for later use;

the preparation method comprises the following steps: mixing one or more of the above prepared tea tree pollen, fructus Gardeniae bud powder, and radix Paeoniae pollen with breviscapine pollen, fructus Siraitiae Grosvenorii pollen, Saviae Miltiorrhizae radix pollen, and substitute pollen at corresponding weight ratio to obtain traditional Chinese medicine pollen.

4. The tea oil for preventing enteritis according to claim 1, wherein the fruit powder is prepared by the following method:

the method comprises the following steps of:

firstly, preparing apple powder: mixing fresh, cleaned and peeled apple pulp with sodium citrate solution with the same weight and mass fraction of 1.2-2.5%, and processing into 10-40 mesh apple pulp coarse slurry by a beater; preheating the apple pulp coarse slurry to 60-70 deg.C, placing in a wide-mouth bottle, stirring until no oxidation phenomenon occurs in the slurry, adding decolorizer 2.5-3.2 wt%, stirring at constant temperature for 10-20min, filtering, and collecting the filtered apple pulp water solution; adding 0.01-0.08 wt% of antiseptic, stirring, sealing, and transferring to shade place for 1-2 days; concentrating, drying, pulverizing to obtain apple powder, and refrigerating at 0-4 deg.C;

preparing mangosteen powder: adding fresh mangosteen pulp into boiling water with the same weight, preserving heat until the solid content in the water solution is 1.2-3.2mg/ml, filtering to obtain mangosteen pulp water solution, concentrating, drying, pulverizing to obtain mangosteen powder, and refrigerating at 0-4 deg.C for use;

preparing the garlic root hair powder: cleaning Bulbus Allii root, soaking in 8-12 wt% vinegar solution at room temperature for 30-40min, and filtering to obtain vinegar-processed Bulbus Allii root; drying the garlic root treated with vinegar in the shade until the water content is less than 7.5%, and pulverizing into fine powder of garlic root hair of more than 40 meshes; adding the fine powder into 1.5-2.5 times of boiling water, boiling for 20-25min, stopping heating, cooling to 40-52 deg.C, filtering, and collecting water solution of Bulbus Allii root hair; spray drying the garlic root hair aqueous solution to obtain garlic root powder for later use;

fourthly, preparing bone soup powder: cleaning livestock and fowl bones, and pulverizing into bone granules with diameter less than 0.5 cm; soaking the bone granules in 6-9 wt% vinegar at 45-62 deg.C for 3.5-5.0 hr, and filtering to obtain livestock and fowl bone vinegar soaking solution and soaked bone granules; pulverizing the soaked bone particles into 80 mesh above bone powder, adding 5.5-7.0 wt% of Bulbus Allii seed, 1.2-3.0 wt% of fructus Piperis powder, and 7.0-9.0 wt% of radix Raphani slice, and stirring to obtain mixture; putting the mixture into a cooking pot, simultaneously adding clear water which accounts for 2-3.5 times of the weight of the mixture, cooking for 8.0-12h, turning off a heat source, adding proteolytic enzyme which accounts for 1.5-3.0% of the weight of the mixture and inorganic salt which accounts for 1.2-2.0% of the weight of the mixture into the cooking pot when the temperature in the cooking pot is reduced to 36-45 ℃, stirring uniformly, preserving heat for 3.5-5.0h, filtering, and collecting bone granule enzymolysis water liquid; mixing the bone granule enzymolysis water solution and livestock and fowl bone edible vinegar soaking solution to obtain livestock and fowl bone extractive solution, decocting with slow fire until the solid content in the solution is 3.5-6.5mg/ml, filtering with filter membrane device with pore diameter of 15 μm, and collecting livestock and fowl bone extractive filtrate; drying and crushing the livestock and poultry bone extract filtrate to obtain bone soup powder for later use;

preparing the fish skin powder: cleaning fresh fish skin, spreading on the surface of silica gel particles, transferring into a closed box, controlling the vacuum degree in the closed box at 5-9KPa and the temperature at 35-45 deg.C, and processing until the water content in the fish skin is less than 8% to obtain dried fish skin; pulverizing dried fish skin into fine powder of more than 100 meshes to obtain fish skin powder for later use;

the preparation method comprises the following steps: and uniformly mixing one or more of the prepared apple powder and the mangosteen powder in equal weight proportion with the garlic root hair powder, the bone soup powder and the fish skin powder in corresponding weight proportion to obtain the fruit powder.

5. The tea oil for preventing enteritis according to claim 1, wherein the traditional Chinese medicine peel powder is prepared by the following method:

the method comprises the following steps of:

preparing the cortex dictamni powder: selecting cortex Dictamni Radicis powder which is prepared by extracting cortex Dictamni Radicis, has trigonelline content of 70-82%, phellodendron lactone content of 6-10%, limonin content of 1-2.5%, other components content of less than 1.5%, and solvent residue of less than 5ppm, and keeping;

② preparing the ash bark powder, cleaning the ash bark, cutting into ash bark slices with uniform width, adding edible ethanol with the same weight and volume concentration of more than 80%, soaking at normal temperature until the content of aesculin in the ethanol is higher than 0.15mg/ml, filtering to obtain the ash bark ethanol soaking solution; preheating the cortex Fraxini ethanol soak solution to 46-58 deg.C, simultaneously diluting with 0.3-0.6% buffer salt solution at the same temperature until ethanol concentration is reduced to 40-48%, and stirring at constant temperature for 15-30 min; then diluting with 0.2-0.5% edible vinegar solution until ethanol concentration is reduced to 25%, stirring, standing until solution temperature is reduced to 20-24 deg.C, filtering, and collecting cortex Fraxini extract precipitate; washing the ash bark extract precipitate with clear water for 2-3 times to obtain washed ash bark extract precipitate; drying and pulverizing the washed ash bark extract precipitate to obtain ash bark powder for later use;

preparing asparagus lettuce skin powder: cleaning fresh asparagus lettuce, peeling the skin of the asparagus lettuce carrying the asparagus lettuce with the thickness less than 0.2cm, mixing the skin with warm water with the same weight and the temperature of 60-72 ℃, and processing the mixture into 10-mesh asparagus lettuce skin slurry by a grinding machine; filtering the asparagus lettuce epidermis slurry through a filter membrane device with the aperture of 30 microns, and collecting the filtrate of the asparagus lettuce epidermis slurry; concentrating, drying and crushing the asparagus lettuce epidermis slurry filtrate to obtain asparagus lettuce epidermis powder for later use;

preparing grape skin powder: selecting grape skin powder which is extracted from grape skin, contains 40-48% of anthocyanin, 45-60% of resveratrol, less than 1.2% of tannin and less than 50ppm of ethanol solvent residual quantity for later use;

preparing orange peel powder: putting fresh orange peel and clean water with the same weight into a distiller, boiling and distilling until the volume of water liquid is reduced by 40-45%, and filtering to obtain distilled orange peel; drying the distilled orange peel until the water content is less than 12%, grinding the dried orange peel into 20-40 meshes of orange peel coarse powder, soaking the orange peel coarse powder in ethanol with the weight being 2-3 times and the volume concentration being 70% for 4-7h, and filtering to obtain orange peel ethanol soaking liquid; concentrating, drying and crushing the orange peel ethanol soaking solution to obtain orange peel powder for later use;

sixthly, sugarcane peel powder: putting the cleaned and peeled sugarcane peel into a microwave vacuum drier, and drying for 10-16min at the vacuum degree of 4-8KPa to obtain dried sugarcane peel; micronizing the dried sugarcane peel into dry sugarcane peel fine powder of more than 200 meshes, and uniformly mixing the dry sugarcane peel fine powder with bentonite of 100 meshes according to equal weight proportion to obtain mixed sugarcane peel fine powder; adding 2-3 times of boiling water into the mixed sugarcane peel fine powder, uniformly stirring, sealing, standing until the water temperature is reduced to room temperature, filtering, and collecting a mixed sugarcane peel fine powder water solution; spray drying the mixed sugarcane peel fine powder water solution to obtain sugarcane peel powder for later use;

the preparation method comprises the following steps: and uniformly mixing one or more of the prepared white delicate hide powder, ash bark powder and asparagus lettuce bark powder in equal weight proportion with grape bark powder, orange bark powder and sugarcane bark powder in corresponding weight proportion to obtain the traditional Chinese medicine bark powder.

6. A method for preparing the tea oil for preventing enteritis according to any one of claims 1 to 5, which comprises the following steps:

preparing materials: according to the weight ratio, respectively taking tea oil, traditional Chinese medicine peel powder, traditional Chinese medicine pollen, fruit powder, traditional Chinese medicine leaf powder and additives for later use;

secondly, mix: firstly, uniformly mixing fruit powder and edible surfactant which accounts for 0.3-1.2% of the weight of the fruit powder to obtain mixed fruit powder; preheating 1/5 of the tea oil to above 120 deg.C, slowly adding mixed fruit powder into hot tea oil under stirring, treating at constant temperature for 30-45min, and filtering with 300 mesh sieve to obtain primary mixed tea oil; transferring the primary mixed tea oil to a refrigeration house, refrigerating at 0-10 deg.C for 5-7h, and filtering with 300 mesh screen to obtain mixed tea oil I;

the third step of mixing: mixing traditional Chinese medicine pollen and traditional Chinese medicine leaf powder to obtain traditional Chinese medicine mixed powder, adding N503 solvent 1.5-3.0 times of the weight of the traditional Chinese medicine mixed powder and ammonium salt solution 1.2-3.5% of the weight of the traditional Chinese medicine mixed powder and 4-6.5% of the mass fraction, mixing, stirring at 30-45 deg.C for 2.5-3.5h, standing, layering, filtering, and collecting N503 solvent solution; then transferring the N503 solvent liquid into edible ethanol with the weight of 2-3 times and the volume concentration of more than 80%, rolling and stirring for 1.0-1.5h, then adding a sodium salt solution with the mass fraction of 10-15% into the edible ethanol, mixing and stirring for 10-30min, standing, layering, filtering, and collecting the traditional Chinese medicine mixed powder ethanol extraction solution; vacuum concentrating the ethanol extract solution of the Chinese medicinal mixed powder at low temperature until the solid content is 15.5-21.0mg/ml to obtain ethanol extract concentrated material of the Chinese medicinal mixed powder; preheating 2/5 of the tea oil to more than 150 ℃, slowly adding the ethanol-extracted concentrated material of the traditional Chinese medicine mixed powder into the hot tea oil while stirring, after the tea oil is completely added, stirring at constant temperature for 30-45min, then closing a heat source, adding pure water accounting for 20-35% of the weight of the tea oil when the tea oil is naturally cooled to 70-80 ℃, stirring for 10-20min, then, continuously naturally cooling to room temperature, filtering, and collecting filtered tea oil to obtain a second mixed tea oil for later use;

fourthly, mixing three: mixing the Chinese medicinal peel powder with edible surfactant 1.0-2.4% of the weight of the Chinese medicinal peel powder, and stirring to obtain mixed Chinese medicinal peel powder; preheating 1/5 of the tea oil to 80 deg.C, slowly adding the mixed Chinese medicinal peel powder into the tea oil under stirring, and treating at constant temperature for 30-45min to obtain mixed tea oil III;

fifthly, mixing: preheating the rest 1/5 of the tea oil to 120 deg.C, slowly adding the additive into the tea oil while stirring, and filtering after dissolving to obtain mixed tea oil IV;

sixthly, total mixing: putting the mixed tea oil I, the mixed tea oil II, the mixed tea oil III and the mixed tea oil IV into a mixing container, uniformly stirring, heating to 160-200 ℃ at a heating rate of 10-15 ℃/min, and stirring at a constant temperature for 1.5-2.5h to obtain total mixed tea oil; adding a decolorizing agent accounting for 2.5-4.5% of the total weight of the mixed tea oil, stirring for decolorizing for 30-40min, filtering, and collecting decolorized mixed tea oil for later use;

training, fine filtering: subjecting the decolorized mixed tea oil to supercritical fine filtration or nano-membrane device fine filtration to obtain tea oil for preventing enteritis.

Technical Field

The invention relates to the technical field of biological medicine and food processing, in particular to tea oil for preventing enteritis and a preparation method thereof.

Background

Enteritis is caused by bacteria, viruses, fungi and parasites. The clinical manifestations mainly include abdominal pain, diarrhea, watery stool or mucous bloody stool. Some patients may have fever and tenesmus, so they are also called infectious diarrhea. Enteritis is classified into acute and chronic types according to the length of the disease course. The course of chronic enteritis is generally more than two months, and chronic bacillary dysentery, chronic amebic dysentery, schistosomiasis, nonspecific ulcerative colitis, limited enteritis and the like are common clinically. With the accelerated pace of life, most people have disorderly life rules and eating rules, often accompanied by symptoms such as abdominal pain and diarrhea, and become potential patients of enteritis.

Tea oil (Camellia oleifera Abel) is edible vegetable oil which is peculiar to China, contains more monounsaturated fatty acid and unsaturated fatty acid, is rich in vitamin E, especially contains squalene and flavonoid substances which have excellent anti-inflammatory effect, does not contain cholesterol, aflatoxin and additives, and is not polluted by any pesticide and chemical fertilizer; meanwhile, the product has unique fragrance and taste. At present, most of tea oil produced by domestic oil enterprises is only simply refined, deep processing is not carried out on the tea oil, and the tea oil is not applied to health care aspects such as enteritis prevention and the like through the deep processing.

Chinese patent (patent application No. 201510262939.X) discloses a camellia oil liquid preparation with gastrointestinal health care function, which mainly comprises camellia oil and malt flour, and can also comprise one or more of the following raw materials: hericium erinaceus, hawthorn, pseudo-ginseng, codonopsis pilosula, poria cocos, lily, dried orange peel, cabbage and fried bighead atractylodes rhizome. The camellia oil liquid preparation has good prevention and treatment and health care effects on gastrointestinal diseases, and can be used as a gastrointestinal health care product.

Another chinese patent (patent application No. 201610722300.X) "a stomach nourishing tea oil and its preparation method", the tea oil is mainly prepared from oil tea seed, black soybean, oil mushroom, millet, rhizoma Zingiberis recens, Poria, fructus Amomi, fructus crataegi, semen Ziziphi Spinosae, rhizoma Polygonati, radix Acanthopanacis Senticosi, radix Ginseng, rhizoma Gastrodiae, radix Isatidis, bupleuri radix, semen Maydis and Ginseng radix. The tea oil is suitable for people with bad intestines and stomach.

Also, Chinese patent (patent application No. 201710757274.9) discloses a camellia oil for promoting health of intestine and stomach and its preparation method, which comprises camellia oil, tea polyphenols, extractive solution A, extractive solution B, extractive solution C, rice oil of sorghum, rice oil of old storehouse, and oleum Ricini. Wherein the extract A is prepared from fructus Jujubae, fructus crataegi, pericarpium Citri Tangerinae, flos Caryophylli, fructus Amomi rotundus, fructus Amomi, and cortex Magnolia officinalis, and the extract B is prepared from semen Raphani, radix Cynanchi auriculati, Atractylodis rhizoma, flos lablab album, fructus Cari Carvi, fructus Perillae Frutescentis, and semen Platycladi; the extract C is prepared from radix Adenophorae, rhizoma Polygonati Odorati, herba Dendrobii, Trichosanthis radix, radix Codonopsis, etc. The invention also provides a preparation method of the camellia oil for intestine and stomach health care. The camellia oil for gastrointestinal health care has a protection effect on gastrointestinal mucosa, has a good repairing effect on gastritis and ulcer, can deeply moisten the gastrointestinal mucosa, has long lasting action time, and has better prevention and health care effects on gastrointestinal diseases.

Also disclosed in Chinese patent application No. 201711013829.5 is a camellia oil for promoting health of intestine and stomach and its preparation method, which comprises (by weight parts) camellia oil 800-1200 parts, radish seed oil 15-35 parts, rice oil 20-45 parts, haw 30-40 parts, red date 20-50 parts, lotus seed 30-40 parts, lotus leaf 10-30 parts, radix cynanchi bungei 18-35 parts, and root of straight ladybell 20-40 parts. The invention also provides a preparation method of the health-care camellia oil beneficial to intestines and stomach. The health-care camellia oil beneficial to intestines and stomach has a protection effect on gastrointestinal tract mucosa, has a good repairing effect on gastritis and ulcer, can deeply moisten the gastrointestinal tract mucosa, has long lasting action time, and has better prevention and health-care effects on gastrointestinal tract diseases.

Disclosure of Invention

The invention aims to provide tea oil which has high nutritive value and can prevent enteritis, and a preparation method matched with the tea oil.

In order to achieve the purpose, the technical measure adopted by the invention is to invent the tea oil for preventing enteritis, which is prepared from the following raw materials in parts by weight:

tea oil 80-90 Chinese medicinal leaf powder 2-5 Chinese medicinal pollen 2-7

Fruit powder 4-10, Chinese medicinal peel powder 2-5, additive 1-3;

the traditional Chinese medicine leaf powder comprises one or more of rosemary leaf powder, roxburgh rose leaf powder, buckwheat leaf powder and bamboo leaf powder which are mixed with livestock and poultry blood powder, garlic leaf powder and dandelion leaves according to the equal weight proportion, and the weight ratio of the traditional Chinese medicine leaf powder to the livestock and poultry blood powder is 5-6.5: 1: 0.1-0.35: 0.4-0.6 by weight ratio;

the Chinese medicinal pollen comprises one or more of tea tree pollen, gardenia bud powder and peony pollen mixed according to equal weight proportion, and is mixed with breviscapine pollen, momordica grosvenori pollen, salvia miltiorrhiza pollen and substitutional pollen according to the weight proportion of 0.2-0.35:1:0.5-0.6:0.45: 0.1;

the fruit powder comprises one or more of apple powder and mangosteen powder mixed according to equal weight proportion, and garlic root hair powder, bone soup powder and fish skin powder mixed according to weight proportion of 2-3.3:0.1:1.5-2: 0.4;

the traditional Chinese medicine peel powder comprises one or more of white fresh peel powder, ash peel powder and asparagus lettuce peel powder which are mixed according to equal weight proportion, and is mixed with grape peel powder, orange peel powder and sugarcane peel powder according to the weight proportion of 0.3-0.45:2-3:0.2: 1;

the additive is prepared from dietary fiber, riboflavin and nicotinic acid according to the proportion of 1.2-2.0: 0.1-0.25: 0.05-0.12 weight ratio.

The traditional Chinese medicine leaf powder is prepared by the following method:

the method comprises the following steps of:

preparing rosemary leaf powder: pulverizing distilled rosemary leaf into coarse powder of 8-15 meshes, adding 2-4 times of low-polarity organic solvent (such as ethyl acetate, petroleum ether, etc.), soaking at room temperature until the solid content in the solvent is 0.8-1.4mg/ml, filtering, and collecting rosemary leaf solvent solution; mixing the rosemary leaf solvent solution with a decolorizing agent (prepared by mixing activated carbon and diatomite according to the weight ratio of 2-3.2: 1) accounting for 5-8% of the weight of the rosemary coarse powder, sealing and stirring at 35-45 ℃ for 30-60min, transferring to a concentrator, concentrating under vacuum to 40-50% of the original volume of the rosemary leaf solvent solution, filtering while hot, and collecting the rosemary leaf decolorizing solvent solution; adding pure water with the same weight into the rosemary leaf decolorization solvent liquid, stirring uniformly, transferring to a refrigeration house, refrigerating for 15-20h at 0-10 ℃, then extracting the organic solvent in the rosemary leaf decolorization solvent liquid, filtering the rest liquid and precipitate, and collecting rosemary leaf extract precipitate; washing the rosemary leaf extract precipitate with boiling water for 2-3 times, drying and crushing the washed rosemary leaf extract precipitate to obtain rosemary leaf powder, and preserving at 10-24 ℃ for later use;

② preparation of roxburgh rose leaf powder: mixing folium Rosae Normalis with 3.5-5.5 wt% inorganic salt (such as hydrochloride and carbonate) solution to obtain 10-20 mesh coarse pulp, adjusting pH to neutral with 0.8-1.5 wt% aqueous solution of alkali (such as sodium hydroxide and sodium bicarbonate), filtering, and collecting folium Rosae Normalis residue; adding the roxburgh rose leaf filter residue into ethanol solution with the same weight and volume concentration of more than 80%, soaking until the solid content in the ethanol is 0.3-0.55mg/ml, filtering, and collecting roxburgh rose leaf ethanol solution; concentrating the ethanol solution of folium Rosae Normalis until the solid content is 5.6-7.5mg/ml, transferring into a refrigerator, refrigerating at 0-10 deg.C to remove precipitate, and collecting the liquid to obtain folium Rosae Normalis precipitate; washing the Rosa roxburghii leaf precipitate with 0.1-0.25% sodium bicarbonate water solution for 2-3 times, and washing with boiling water for 2-3 times to obtain Rosa roxburghii leaf washing precipitate; washing the Rosa roxburghii leaf, precipitating, drying, pulverizing to obtain Rosa roxburghii leaf powder (containing Rosa roxburghii glycoside 50-60%, daucosterol 4-7.5%, physcion less than 0.5%, and sitosterol 1.2-1.8%), and preserving at 10-24 deg.C;

preparing buckwheat leaf powder: cleaning fresh semen Fagopyri Esculenti, transferring to microwave dryer, treating at 35-48 deg.C for 50-70min, spreading 0.5-0.75 wt% inorganic salt (prepared by mixing one or more of sodium sulfate, magnesium sulfate, ammonium chloride, sodium chloride, and sodium hydrogen phosphate at equal weight ratio) solution every 10-15min to obtain treated folium Fagopyri Esculenti leaf, wherein the amount of each time is 5.0-9.0 wt% of folium Fagopyri Esculenti leaf; adding the treated folium Fagopyri Esculenti into a cooking pot filled with 2-3 times of clear water, cooking with slow fire until the solid content of the water solution is 0.2-1.2mg/ml, and filtering to obtain folium Fagopyri Esculenti water solution; adding decolorizing agent (prepared by mixing neutral aluminum oxide, bentonite, and quartz sand powder of above 300 meshes at weight ratio of 3-4: 0.2: 0.5-1.0) 1.2-1.8% into the folium Fagopyri Esculenti water solution, stirring at 35-40 deg.C for 30-40min, and filtering to obtain decolorized folium Fagopyri Esculenti water solution; concentrating, drying, and pulverizing the decolorized buckwheat leaf water solution to obtain buckwheat leaf powder, and preserving at 10-24 deg.C;

fourthly, preparing the bamboo leaf powder: cleaning folium Bambusae, adding into ethanol solution with weight 2-4 times and volume concentration of above 70%, soaking at 45-55 deg.C until the solid content in ethanol is 1.55-2.25mg/ml, filtering, and collecting folium Bambusae ethanol solution; diluting the folium Bambusae ethanol solution with 0.3-0.45% sodium carbonate water solution to obtain diluted folium Bambusae ethanol solution with solid content of 0.7-1.0mg/ml and pH value of 7.5-8.5; adding low-polarity organic solvent (such as ethyl acetate and petroleum ether) with same volume into diluted folium Bambusae ethanol solution, stirring at room temperature for 10-18min, standing, layering, and collecting supernatant; concentrating the supernatant under vacuum until no alcohol exists to obtain concentrated bamboo leaf extract; adjusting pH of the concentrated folium Bambusae extract to 6-6.5 with 1.6-3.2 wt% inorganic acid (such as hydrochloric acid, phosphoric acid, etc.), transferring into a refrigerator, refrigerating for 10-15 hr, filtering, and collecting folium Bambusae extract precipitate; drying and pulverizing the bamboo leaf extract precipitate to obtain bamboo leaf powder, and preserving at 10-24 deg.C;

fifth, preparing the livestock and poultry blood powder: preheating fresh livestock and fowl blood (chicken blood or pig blood or duck blood or rabbit blood or donkey blood) to 50-60 deg.C, adding inorganic salt (such as sodium chloride, sodium sulfate, calcium chloride, sodium phosphate, etc.) aqueous solution with concentration of 0.5-0.9% and 3.5-4.5% of its weight, and 0.5-1.2% dispersant (polyethylene glycol 200 or polyethylene glycol 400 or polyethylene glycol 800, etc.), stirring, treating at constant temperature for 20-35min, filtering with 10-20 μm filter membrane device, collecting filtered livestock and fowl blood water solution, introducing into adsorption column (prepared by mixing one or more of vermiculite, dolomite, zeolite, and feldspar at equal weight ratio and pulverizing to particle size of less than 0.5 mm) at addition rate of 15-24L/h, standing for 5-8h after all livestock and fowl blood water solution is added, heating the blood in the adsorption column to 50-60 deg.C by jacket, controlling the flow rate at 30-45ml/min, collecting effluent column-passing livestock and poultry blood water solution, concentrating at 70-80 deg.C under 5-10KPa until the solid content is 28.5-32.5mg/ml, adding edible ethanol while hot, adjusting its alcoholicity to 60%, stirring for 10-15min, transferring to a refrigerator, standing at-4-0 deg.C for 4-7 hr, adding inorganic salt (such as sodium chloride, sodium sulfate, calcium chloride, and sodium phosphate) 0.5-1.2% of its weight, standing for 2-3 hr after stirring, filtering, collecting upper clear livestock and poultry blood ethanol solution, concentrating at 60-75 deg.C under 5-10KPa until the solid content is 12.5-15.5mg/ml to obtain concentrated livestock and poultry blood water solution, adding organic solvent (such as dichloromethane, ethyl acetate, etc.) with the same volume, stirring and extracting at room temperature for 10-15min, standing, layering, collecting organic solvent extract, concentrating, drying, and pulverizing to obtain livestock and fowl blood powder;

sixthly, preparing the garlic leaf powder: naturally drying fresh garlic leaves until the garlic leaves turn yellow, then crushing the garlic leaves into fine powder with the particle size of more than 60 meshes, transferring the fine powder into boiling water with the weight of 2-4 times of the garlic leaves, carrying out heat preservation and stirring treatment until the solid content in water liquid is 0.7-1.9mg/ml and the carotene content is higher than 0.05mg/ml, filtering, and collecting water extract of the garlic leaves; concentrating, drying and pulverizing the water extractive solution of Bulbus Allii leaf to obtain Bulbus Allii leaf powder, and preserving at 10-24 deg.C;

preparing dandelion leaf powder: selecting dandelion leaf powder which is extracted from dandelion leaves, has the phylloquinone content of more than 8.5 percent, the lutein content of more than 22.5 percent, the vitamin content of 1.5-3.2mg/10g and the residual amount of ethanol solvent of less than 3.5ppm, and preserving at 10-24 ℃ for later use;

the preparation method comprises the following steps: mixing one or more of the above herba Rosmarini officinalis leaf powder, folium Rosae Normalis powder, folium Fagopyri Esculenti powder, and folium Bambusae powder with livestock and fowl blood powder, Bulbus Allii leaf powder, and herba Taraxaci leaf powder at corresponding weight ratio, and preserving at 10-24 deg.C.

The traditional Chinese medicine pollen is prepared by the following method:

the method comprises the following steps of:

firstly, preparing tea tree pollen: taking fresh tea flowers, and separating tea petals from tea pistils; firstly, soaking tea tree petals in 5-8.5% of vinegar solution for 8-15min, then washing with clear water for 2-3 times, then transferring to a drying oven, and drying at 60-70 ℃ until the water content is less than 5% to obtain dried tea tree petals; putting tea plant pistils into a distiller, simultaneously adding pure water which accounts for 8-12 times of the weight of the tea plant pistils into the distiller, uniformly stirring, distilling until the water volume is reduced by 40-45%, and collecting tea plant pistils distillate; mixing dried tea petal with tea stamen distillate, boiling for 20-32min, filtering, and collecting tea flower water solution; then, concentrating, drying and crushing the tea flower water solution to obtain tea flower pollen for later use;

② preparing gardenia bud powder: grinding the prepared gardenia buds into gardenia bud coarse powder with the particle size of more than 10 meshes, then dripping ammonia water with the mass concentration of 3.5-5.5% according to the proportion of 6-8 drops/20 g, uniformly stirring, transferring into a microwave dryer, and treating at the temperature of 45-50 ℃ for 22-28min to obtain microwave-treated gardenia bud coarse powder; transferring the microwave-treated fructus Gardeniae bud coarse powder into 1.5-3.5 wt% sodium hydrogen phosphate solution, stirring at 40-52 deg.C for 5-15min, and filtering to obtain treated fructus Gardeniae bud powder; adding the treated fructus Gardeniae bud powder into 1-3 times of pure water, steaming with 50-55 deg.C slow fire until pH value of the water solution is 4.8-5.5, and filtering to obtain fructus Gardeniae bud powder water solution; concentrating, drying and pulverizing the water solution of the gardenia bud powder to obtain gardenia bud powder for later use;

③ preparing peony pollen: soaking flos Paeoniae in ethanol solution with volume concentration of 50% or more and weight of 1.5-3.0 times of the flos Paeoniae at 50-65 deg.C until the solid content in the ethanol solution is 3.2-4.2mg/ml to obtain flos Paeoniae ethanol soaking solution; adding decolorizing agent (prepared by mixing neutral aluminum oxide, ammonium chloride, and quartz sand powder of 300 meshes at weight ratio of 3-4: 0.2: 0.5-1.0) 1.2-1.5% of the original weight of flos Paeoniae into the flos Paeoniae ethanol soaking solution, stirring at 40-50 deg.C for 30-45min, filtering, and collecting decolorized flos Paeoniae ethanol solution; concentrating, drying and crushing the decolorized peony flower ethanol solution to obtain peony flower powder for later use;

preparing erigeron breviscapus pollen: firstly, putting the erigeron breviscapus into 0.3-0.5% sodium bicarbonate aqueous solution with the weight of 1-2.5 times of that of the erigeron breviscapus, soaking for 25-40min at normal temperature, and filtering to obtain the treated erigeron breviscapus; then the treated erigeron breviscapus is transferred into boiling water with the same weight, and is stirred back and forth for 8-12min, and is filtered to obtain the erigeron breviscapus treated by the boiling water; adding boiling water-treated flos Hibisci into edible ethanol solution with weight 2-3 times and volume concentration above 35%, soaking at 50-65 deg.C until erigeron content in the ethanol solution is 0.11-0.18mg/ml, and filtering to obtain flos Hibisci ethanol soaking solution; vacuum concentrating the ethanol soaking solution at low temperature until the content of erigeron breviscapus glycoside is 0.8-1.25mg/ml to obtain erigeron breviscapus ethanol concentrated solution; transferring the concentrated solution into a refrigerator, refrigerating at 4-8 deg.C until no precipitate is separated out, filtering, and collecting the upper layer of herba Erigerontis liquid; spray drying the erigeron breviscapus liquid to obtain erigeron breviscapus powder for later use;

fifthly, preparing momordica grosvenori pollen: cleaning flos Momordicae, soaking in 30-45% ethanol solution at 45-55 deg.C until the content of saccharide in the ethanol solution reaches 0.03-0.1mg/ml, and filtering to obtain flos Momordicae ethanol soaking solution; adding a decolorizing agent (prepared by mixing 100-mesh zeolite powder, sodium bicarbonate and bentonite at a weight ratio of 1:0.04: 1.5) 0.3-0.6% of the original flos Momordicae into the ethanol soaking solution of flos Momordicae, stirring for 10-15min, filtering with 0.5 micrometer filter membrane device, and collecting the ethanol soaking filtrate of flos Momordicae; soaking the momordica grosvenori flower in ethanol, concentrating and drying the filtrate to obtain momordica grosvenori pollen for later use;

sixthly, preparing salvia miltiorrhiza pollen: soaking Salvia miltiorrhiza flower in ethanol solution with 1.5-3.0 times weight and volume concentration of more than 50% at 50-65 deg.C until the solid content in ethanol solution is 0.8-1.35mg/ml to obtain Salvia miltiorrhiza flower ethanol soaking solution; adding a decolorizing agent (prepared by mixing neutral aluminum oxide, ammonium chloride and quartz sand powder of more than 300 meshes in a weight ratio of 3-4: 0.2: 0.5-1.0) accounting for 0.5-0.75% of the weight of the original salvia flower into the salvia flower ethanol soaking solution, stirring at 40-50 ℃ for 10-15min, filtering, and collecting the salvia flower ethanol soaking decolorizing solution; then the ethanol-soaked destaining solution of the salvia miltiorrhiza flowers is concentrated, dried and crushed to obtain salvia miltiorrhiza pollen for later use;

and seventhly, preparing substitute pollen: firstly, mixing the seville orange flower with pure water of which the weight is 4-6 times that of the seville orange flower, putting the mixture into a distillation container, carrying out distillation treatment for 1.0-1.5h at the temperature of 100 ℃ and 110 ℃, taking out and draining to obtain the distilled seville orange flower; drying and crushing the distilled bitter orange to obtain bitter orange powder for later use;

the preparation method comprises the following steps: mixing one or more of the above prepared tea tree pollen, fructus Gardeniae bud powder, and radix Paeoniae pollen with breviscapine pollen, fructus Siraitiae Grosvenorii pollen, Saviae Miltiorrhizae radix pollen, and substitute pollen at corresponding weight ratio to obtain traditional Chinese medicine pollen.

The fruit powder is prepared by the following method:

the method comprises the following steps of:

firstly, preparing apple powder: mixing fresh, cleaned and peeled apple pulp with sodium citrate solution with the same weight and mass fraction of 1.2-2.5%, and processing into 10-40 mesh apple pulp coarse slurry by a beater; preheating the apple pulp coarse slurry to 60-70 deg.C, placing in a wide-mouth bottle, stirring until no oxidation phenomenon occurs in the slurry, adding decolorizing agent (prepared by mixing diatomite and 300 mesh feldspar powder at a weight ratio of 1.5-3.5: 1) 2.5-3.2% of the pulp, stirring at constant temperature for 10-20min, filtering, and collecting the filtered apple pulp water solution; adding 0.01-0.08 wt% of antiseptic (prepared from one or more of calcium propionate, natamycin, and potassium sorbate at equal weight ratio), stirring, sealing, and transferring to shade place for 1-2 days; concentrating, drying, pulverizing to obtain apple powder, and refrigerating at 0-4 deg.C;

preparing mangosteen powder: adding fresh mangosteen pulp into boiling water with the same weight, preserving heat until the solid content in the water solution is 1.2-3.2mg/ml, filtering to obtain mangosteen pulp water solution, concentrating, drying, pulverizing to obtain mangosteen powder, and refrigerating at 0-4 deg.C for use;

preparing the garlic root hair powder: cleaning Bulbus Allii root, soaking in 8-12 wt% vinegar solution at room temperature for 30-40min, and filtering to obtain vinegar-processed Bulbus Allii root; drying the garlic root treated with vinegar in the shade until the water content is less than 7.5%, and pulverizing into fine powder of garlic root hair of more than 40 meshes; adding the fine powder into 1.5-2.5 times of boiling water, boiling for 20-25min, stopping heating, cooling to 40-52 deg.C, filtering, and collecting water solution of Bulbus Allii root hair; spray drying the garlic root hair aqueous solution to obtain garlic root powder for later use;

fourthly, preparing bone soup powder: cleaning livestock and fowl bones (chicken bone or pig bone or duck bone or rabbit bone or donkey bone), and pulverizing into bone granules with diameter less than 0.5 cm; soaking the bone granules in 6-9 wt% vinegar at 45-62 deg.C for 3.5-5.0 hr, and filtering to obtain livestock and fowl bone vinegar soaking solution and soaked bone granules; pulverizing the soaked bone particles into 80 mesh above bone powder, adding 5.5-7.0 wt% of Bulbus Allii seed, 1.2-3.0 wt% of fructus Piperis powder, and 7.0-9.0 wt% of radix Raphani slice, and stirring to obtain mixture; putting the mixture into a cooking pot, simultaneously adding clear water which accounts for 2-3.5 times of the weight of the mixture, cooking for 8.0-12h, turning off a heat source, adding proteolytic enzyme which accounts for 1.5-3.0% of the weight of the mixture and inorganic salt (one or more of sodium sulfate, zinc sulfate, calcium chloride and sodium chloride which are mixed according to equal weight proportion) which accounts for 1.2-2.0% of the weight of the mixture into the cooking pot when the temperature in the cooking pot is reduced to 36-45 ℃, stirring uniformly, preserving heat for 3.5-5.0h, filtering, and collecting bone granule enzymolysis water liquid; mixing the bone granule enzymolysis water solution and livestock and fowl bone edible vinegar soaking solution to obtain livestock and fowl bone extractive solution, decocting with slow fire until the solid content in the solution is 3.5-6.5mg/ml, filtering with filter membrane device with pore diameter of 15 μm, and collecting livestock and fowl bone extractive filtrate; drying and crushing the livestock and poultry bone extract filtrate to obtain bone soup powder for later use;

preparing the fish skin powder: cleaning fresh fish skin (edible fresh water or seawater fish), spreading on the surface of silica gel particles, transferring into a closed box, controlling the vacuum degree in the closed box at 5-9KPa and 35-45 deg.C, and processing until the water content in the fish skin is less than 8% to obtain dried fish skin; pulverizing dried fish skin into fine powder of more than 100 meshes to obtain fish skin powder for later use;

the preparation method comprises the following steps: and uniformly mixing one or more of the prepared apple powder and the mangosteen powder in equal weight proportion with the garlic root hair powder, the bone soup powder and the fish skin powder in corresponding weight proportion to obtain the fruit powder.

The Chinese medicinal hide powder is prepared by the following method:

the method comprises the following steps of:

preparing the cortex dictamni powder: selecting cortex Dictamni Radicis powder which is prepared by extracting cortex Dictamni Radicis, has trigonelline content of 70-82%, phellodendron lactone content of 6-10%, limonin content of 1-2.5%, other components content of less than 1.5%, and solvent residue of less than 5ppm, and keeping;

② preparing the ash bark powder, cleaning the ash bark, cutting into ash bark slices with uniform width, adding edible ethanol with the same weight and volume concentration of more than 80%, soaking at normal temperature until the content of aesculin in the ethanol is higher than 0.15mg/ml, filtering to obtain the ash bark ethanol soaking solution; preheating the cortex Fraxini ethanol soak solution to 46-58 deg.C, simultaneously diluting with 0.3-0.6% buffer salt solution (composed of sodium phosphate and sodium hydrogen phosphate at equal weight ratio, or sodium sulfite and sodium bisulfite at equal weight ratio) at the same temperature until ethanol concentration is reduced to 40-48%, and stirring at constant temperature for 15-30 min; then diluting with 0.2-0.5% edible vinegar solution until ethanol concentration is reduced to 25%, stirring, standing until solution temperature is reduced to 20-24 deg.C, filtering, and collecting cortex Fraxini extract precipitate; washing the ash bark extract precipitate with clear water for 2-3 times to obtain washed ash bark extract precipitate; drying and pulverizing the washed ash bark extract precipitate to obtain ash bark powder for later use;

preparing asparagus lettuce skin powder: cleaning fresh asparagus lettuce, peeling the skin of the asparagus lettuce carrying the asparagus lettuce with the thickness less than 0.2cm, mixing the skin with warm water with the same weight and the temperature of 60-72 ℃, and processing the mixture into 10-mesh asparagus lettuce skin slurry by a grinding machine; filtering the asparagus lettuce epidermis slurry through a filter membrane device with the aperture of 30 microns, and collecting the filtrate of the asparagus lettuce epidermis slurry; concentrating, drying and crushing the asparagus lettuce epidermis slurry filtrate to obtain asparagus lettuce epidermis powder for later use;

preparing grape skin powder: selecting grape skin powder which is extracted from grape skin, contains 40-48% of anthocyanin, 45-60% of resveratrol, less than 1.2% of tannin and less than 50ppm of ethanol solvent residual quantity for later use;

preparing orange peel powder: putting fresh orange peel and clean water with the same weight into a distiller, boiling and distilling until the volume of water liquid is reduced by 40-45%, and filtering to obtain distilled orange peel; drying the distilled orange peel until the water content is less than 12%, grinding the dried orange peel into 20-40 meshes of orange peel coarse powder, soaking the orange peel coarse powder in ethanol with the weight being 2-3 times and the volume concentration being 70% for 4-7h, and filtering to obtain orange peel ethanol soaking liquid; concentrating, drying and crushing the orange peel ethanol soaking solution to obtain orange peel powder for later use;

sixthly, sugarcane peel powder: putting the peeled sugarcane peels into a microwave vacuum dryer, and drying for 10-16min at the frequency of 100-; micronizing the dried sugarcane peel into dry sugarcane peel fine powder of more than 200 meshes, and uniformly mixing the dry sugarcane peel fine powder with bentonite of 100 meshes according to equal weight proportion to obtain mixed sugarcane peel fine powder; adding 2-3 times of boiling water into the mixed sugarcane peel fine powder, uniformly stirring, sealing, standing until the water temperature is reduced to room temperature, filtering, and collecting a mixed sugarcane peel fine powder water solution; spray drying the mixed sugarcane peel fine powder water solution to obtain sugarcane peel powder for later use;

the preparation method comprises the following steps: and uniformly mixing one or more of the prepared white delicate hide powder, ash bark powder and asparagus lettuce bark powder in equal weight proportion with grape bark powder, orange bark powder and sugarcane bark powder in corresponding weight proportion to obtain the traditional Chinese medicine bark powder.

Meanwhile, a preparation method of the tea oil for preventing enteritis is also provided, and the preparation process is as follows:

preparing materials: according to the weight ratio, respectively taking tea oil, traditional Chinese medicine peel powder, traditional Chinese medicine pollen, fruit powder, traditional Chinese medicine leaf powder and additives for later use;

secondly, mix: firstly, uniformly mixing fruit powder and edible surfactant (such as lecithin, sucrose ester and the like) accounting for 0.3-1.2% of the weight of the fruit powder to obtain mixed fruit powder; preheating 1/5 of the tea oil to above 120 deg.C, slowly adding mixed fruit powder into hot tea oil under stirring at a rate of 40-60g/min, treating at constant temperature for 30-45min, and filtering with 300 mesh screen to obtain primarily mixed tea oil; transferring the primary mixed tea oil to a refrigeration house, refrigerating at 0-10 deg.C for 5-7h, and filtering with 300 mesh screen to obtain mixed tea oil I;

the third step of mixing: mixing traditional Chinese medicine pollen and traditional Chinese medicine leaf powder to obtain traditional Chinese medicine mixed powder, adding N503 solvent (extractant) 1.5-3.0 times of the weight of the traditional Chinese medicine mixed powder and ammonium salt (such as ammonium sulfate salt, ammonium carbonate salt, etc.) solution 1.2-3.5% of the weight of the traditional Chinese medicine mixed powder and 4-6.5% of the mass fraction, mixing, stirring at 30-45 deg.C for 2.5-3.5h, standing, layering, filtering, and collecting N503 solvent solution; then, the N503 solvent solution is transferred into edible ethanol with the weight of 2-3 times and the volume concentration of more than 80%, the rolling stirring treatment is carried out for 1.0-1.5h, then sodium salt (such as sodium chloride, sodium sulfate and the like) solution with the mass fraction of 10-15% is added into the edible ethanol, the adding amount of the sodium salt solution is 5-8% of the volume of the N503 solvent solution, the mixing and stirring are carried out for 10-30min, the standing, the layering and the filtering are carried out, and the ethanol extraction solution of the traditional Chinese medicine mixed powder is collected; vacuum concentrating the ethanol extract solution of the Chinese medicinal mixed powder at low temperature until the solid content is 15.5-21.0mg/ml to obtain ethanol extract concentrated material of the Chinese medicinal mixed powder; preheating 2/5 of the tea oil to more than 150 ℃, slowly adding the ethanol-extracted concentrated material of the traditional Chinese medicine mixed powder into the hot tea oil while stirring at the rate of 120 plus 140g/min, stirring at constant temperature for 30-45min after the tea oil is completely added, then closing a heat source, adding pure water accounting for 20-35% of the weight of the tea oil (namely 2/5 of the tea oil) when the tea oil is naturally cooled to 70-80 ℃, stirring for 10-20min, then, continuously naturally cooling to room temperature, filtering, and collecting filtered tea oil to obtain mixed tea oil II for later use;

fourthly, mixing three: mixing the Chinese medicinal peel powder with edible surfactant (such as lecithin and sucrose ester) 1.0-2.4 wt% of the Chinese medicinal peel powder, and stirring to obtain mixed Chinese medicinal peel powder; preheating 1/5 of the tea oil to 80 deg.C, slowly adding the mixed Chinese medicinal peel powder into the tea oil while stirring, controlling the adding rate at 60-70g/min, and treating at constant temperature for 30-45min after adding completely to obtain mixed tea oil III;

fifthly, mixing: preheating the rest 1/5 of the tea oil to 120 deg.C, slowly adding the additive into the tea oil while stirring, and filtering after dissolving to obtain mixed tea oil IV;

sixthly, total mixing: putting the mixed tea oil I, the mixed tea oil II, the mixed tea oil III and the mixed tea oil IV into a mixing container, uniformly stirring, heating to 160-200 ℃ at a heating rate of 10-15 ℃/min, and stirring at a constant temperature for 1.5-2.5h to obtain total mixed tea oil; then adding a decolorizing agent (prepared by mixing neutral activated carbon, 3A type molecular sieve, 300-mesh vermiculite powder and calcium chloride powder in a weight ratio of 2-4: 1: 0.4-0.8: 0.1-0.25) accounting for 2.5-4.5% of the total mixed tea oil weight, stirring for decolorizing for 30-40min, filtering, and collecting decolorized mixed tea oil for later use;

training, fine filtering: subjecting the decolorized mixed tea oil to supercritical fine filtration or nano-membrane device fine filtration to obtain tea oil for preventing enteritis.

The tea oil is edible tea oil which meets the national standard GB/T11765-2003.

The tea oil for preventing enteritis provided by the invention is prepared from main raw materials of tea oil, which comprise livestock and poultry blood powder, garlic leaf powder, dandelion leaf powder, erigeron breviscapus pollen, momordica grosvenori pollen, salvia miltiorrhiza pollen, substitute pollen, garlic root hair powder, bone soup powder, fishskin powder, grape skin powder, orange skin powder, sugarcane skin powder, dietary fibers, riboflavin, nicotinic acid, one or more of rosemary leaf powder, roxburgh rose leaf powder, buckwheat leaf powder and bamboo leaf powder, one or more of tea tree pollen, gardenia bud powder and peony pollen, one or more of apple powder and mangosteen powder, and one or more of dictamnus chinensis powder, ash bark powder and asparagus lettuce skin powder.

Tea oil (Camellia oleifera Abel) belongs to the Theaceae family, and is the main and unique woody edible oil in China. The tea oil has high comprehensive utilization value, contains rich bioactive substances such as unsaturated fatty acid, monounsaturated fatty acid, vitamin E, squalene, tea polyphenol and the like, and particularly has excellent effects of preventing cancers and resisting inflammation by squalene and flavonoid substances. The tea oil plays a specific role in the invention: one is vegetable oil dissolved as all prophylactic drugs; secondly, the tea oil has the functions of clearing away heat and toxic materials, resisting cancer and improving immunity; and thirdly, the tea oil has the effects of moistening intestines and promoting digestion and absorption and can promote the absorption of preventive medicaments.

The livestock blood powder plays a specific role in the invention: after being decomposed by gastric juice, the blood protein in the livestock blood can react with smoke dust and heavy metals invading human bodies, so that the chler's function of macrophages is promoted, and the detoxification function is realized.

The garlic leaf powder is prepared from garlic (Allium Sativum L.) leaves, and has the following specific functions: the garlic leaves are rich in various nutritional ingredients and have the effects of sterilizing, diminishing inflammation and promoting digestion.

The dandelion leaf powder is prepared from dandelion (Taraxacum mongolicum hand. -Mazz.) leaves, and the dandelion leaf powder plays a specific role in the invention: the dandelion leaf has the effects of diminishing inflammation, detoxifying and the like.

The Erigeron breviscapus powder is prepared from dried whole plant of Erigeron breviscapus (Vant.) Hand-Mazz of Compositae, and has the following specific functions: the erigeron breviscapus has the effects of promoting blood circulation, removing blood stasis, diminishing inflammation and the like.

The momordica grosvenori pollen is prepared from flowers of momordica grosvenori (Siraitia grosvenor (Swingle) C.Jeffrey ex Lu et Z.Y.Z) which is a perennial vine of Cucurbitaceae, and has the following specific functions: the fructus Siraitiae Grosvenorii flower contains multiple nutrients, and has effects of removing toxic substances, regulating blood pressure, and reducing blood lipid.

The Salvia miltiorrhiza pollen is prepared from Salvia miltiorrhiza (Salvia militaria Bunge) flowers, and the Salvia miltiorrhiza pollen plays a specific role in the invention: the red sage flower has the functions of dissipating blood stasis, nourishing heart, tranquilizing, etc.

The substitute pollen is prepared from Citrus aurantium L (Citrus aurantium L) belonging to Rutaceae, and has the following specific functions: the seville orange flower is rich in various glycosides and has the effects of resisting inflammation, resisting virus, regulating endocrine and the like.

The Garlic root hair powder is prepared from Garlic (Garlic) roots, and has the following specific functions in the invention: the scallion root has the effects of diminishing inflammation, sterilizing and the like.

The bone soup powder is prepared from livestock and poultry bones, and has the following specific functions: has the effects of promoting blood circulation, moistening the intestines and the like.

The fish skin powder is prepared from edible fish skin, and the fish skin powder plays a specific role in the invention: the fish skin contains multiple nutrients, such as leucocyte, and has antiinflammatory and anticancer effects.

The grape skin powder is prepared from grape (Vitis vinifera L.) pericarp, and the grape skin powder plays a specific role in the invention: the grape skin contains natural pigment, and can promote intestinal peristalsis.

The orange peel powder is prepared from Rutaceae plant orange (Citrus reticulata Blanco) and mature fruit peel of cultivated varieties thereof, and has the following specific functions: the orange peel has the effects of detoxifying, regulating intestines and stomach and the like.

The sugarcane peel powder is prepared from sugarcane (sugarcane peel), and the sugarcane peel powder plays a specific role in the invention: the sugarcane peel has effects of removing toxic substance and promoting digestion.

The dietary fiber plays a specific role in the invention: can promote intestinal peristalsis and digestion.

The riboflavin plays a particular role in the present invention: has effects of reducing pathogenic fire, clearing away heat, and preventing mucosal inflammation.

The nicotinic acid plays a specific role in the invention: promoting metabolism, and preventing dermatitis.

Tea tree pollen is prepared from flowers of tea trees [ Camellia sinensis (Linn.) O.Kuntze ], and plays a specific role in the invention: the tea flower contains multiple antioxidant substances, and can reduce oxidation reaction in vivo and prevent oxidation of the medicine in vivo.

The Gardenia bud powder is prepared from buds of Gardenia (scientific name: Gardenia jasminoides), and the Gardenia bud powder plays a specific role in the invention: the gardenia contains triterpene active substances, has the effects of clearing away lung-heat, resisting inflammation, moistening intestines and the like, and promotes the prevention effect and metabolism of the medicine.

The peony pollen is prepared from the flower of peony (academic name: Paeonia lactiflora Pall.), and the peony pollen plays specific roles in the invention: the peony flower has the effects of promoting blood circulation, protecting liver and the like, regulating human metabolism and promoting the metabolic absorption of preventive medicaments in vivo.

The apple powder is prepared from apples (Malus domestica), and the apple powder plays a specific role in the invention: has effects of moistening intestine, promoting toxic substances, etc.

The mangosteen powder is prepared from mangosteen (Garcinia mangostana L.), and the mangosteen powder plays a specific role in the invention: the mangosteen is rich in various vitamins, dietary fibers and other substances, and has the effects of resisting inflammation, detoxifying, regulating spleen and stomach and the like.

The Cortex dictamni powder is prepared from Cortex dictamni (Cortex Dictamni), and the Cortex dictamni powder plays a specific role in the invention: has antibacterial and toxic materials clearing away effects

The ash bark powder is prepared from ash bark (Cortex fraxini), and the ash bark powder plays a specific role in the invention: has antibacterial and antiviral effects.

The asparagus lettuce peel powder is prepared from asparagus lettuce (Lactuca sativa L.var. angustana Irish.) peel, and the specific function of the asparagus lettuce peel powder in the invention is as follows: has effects of promoting gastrointestinal digestion.

The tea oil for preventing enteritis, which is prepared from the raw materials, contains various glycosides, flavonoids and other substances and active substances beneficial to human bodies, so that enteritis diseases can be effectively prevented, and particularly, the tea oil has good inhibition and treatment effects on chronic enteritis.

The following table 1 is the data of the main effective ingredient test of the camellia oil for preventing enteritis of the invention:

TABLE 1 Main effective ingredient test Table (100g content)

The data in the table show that the tea oil for preventing enteritis contains not only abundant monounsaturated fatty acid and unsaturated fatty acid, but also more beneficial substances such as flavonoid, glycosides, polysaccharides, terpenes and the like.

The tea oil for preventing enteritis of the invention has been subjected to inhibition and treatment tests of chronic enteritis:

1. test subjects:

volunteers (age 20-60 years, total 46) with relatively close disease degree, life style, family life condition and working condition for chronic enteritis patients were selected and divided into test group and control group according to random principle, and the specific conditions are shown in the following table 2.

Table 2 test grouping table

Test group

23

Control group

23

2. Symptoms are:

abdominal pain, diarrhea, bloody purulent stool in stool.

3. The test method comprises the following steps:

firstly, a test group:

the tea oil for preventing enteritis, which is prepared from the following raw materials in parts by weight, is eaten (namely, the following example 3):

tea oil 85 Chinese medicinal leaf powder 3.5 Chinese medicinal pollen 4.5

Fruit powder 7 Chinese medicinal peel powder 3.5 additive 2.

The eating method comprises the following steps: during the test, the kinds and the amounts of the meals eaten were all the same as normal times, except that the tea oil for preventing enteritis according to the present invention was used for cooking.

The method comprises the following steps:

during the test control period, the types and the quantities of the eaten dishes are all the same according to the normal time, and the oil used for cooking is common tea oil.

3. And (3) evaluating the effect:

the method comprises the following steps: the symptoms and physical signs disappear, and no relapse occurs for more than 3 months.

The method has the advantages that: the symptoms and physical signs are relieved during the attack, and the attack frequency is reduced.

And thirdly, ineffective: there was no significant improvement in symptoms and signs.

The effective rate statistics comprises the obvious effect and the improvement.

4. The statistical basis is as follows:

taking the confirmed diagnosis report of the hospital above the county level as the statistical basis.

5. And (3) test results:

after one year of continuous testing, the test data were counted to form the following test results table (table 3):

TABLE 3 test results Table

The statistical data show that the effective rate of the test group taking the tea oil for preventing enteritis of the invention for inhibiting and treating chronic enteritis is 69.56%, while the effective rate of the control group taking common tea oil for inhibiting and treating chronic enteritis is 30.43%, and compared with the control group, the effective rate of the test group for inhibiting and treating chronic enteritis is improved by 39.13%.

Detailed Description

The present invention will be further described with reference to the following examples. The following description is given by way of example, and the scope of the invention is not limited thereto.

Example 1:

the tea oil for preventing enteritis of the embodiment is prepared by the following steps:

(1) and raw material pretreatment:

the preparation method comprises the following steps of:

preparing rosemary leaf powder: crushing distilled rosemary leaves into 10-mesh rosemary leaf coarse powder, then putting the coarse powder into ethyl acetate with the weight being 3 times that of the coarse powder, soaking the coarse powder at normal temperature until the solid content in a solvent is 1.1mg/ml, filtering the solution, and collecting rosemary leaf solvent liquid; then mixing the rosemary leaf solvent liquid with the rosemary coarse powder which accounts for 7 percent of the weight of the rosemary coarse powder, activated carbon and diatomite according to a proportion of 2.5: 1, mixing the decolorants mixed according to the weight ratio, sealing and stirring at 40 ℃ for 45min, transferring the mixture into a concentrator, concentrating the mixture in vacuum until the volume of the solvent solution is 45% of the original volume of the rosemary leaf, filtering the mixture while the mixture is hot, and collecting the rosemary leaf decoloration solvent solution; adding pure water with the same weight into the rosemary leaf decolorization solvent liquid, stirring uniformly, transferring to a refrigeration house, refrigerating at 4 ℃ for 18h, then extracting the organic solvent in the rosemary leaf decolorization solvent liquid, filtering the rest liquid and precipitate, and collecting rosemary leaf extract precipitate; washing the rosemary leaf extract precipitate with boiling water for 2-3 times, drying and crushing the washed rosemary leaf extract precipitate to obtain rosemary leaf powder, and preserving at 18 ℃ for later use;

② preparation of roxburgh rose leaf powder: mixing the roxburgh rose leaves with a sodium chloride solution with the same weight and the mass fraction of 4.5% to prepare coarse roxburgh rose leaf slurry of 15 meshes, adjusting the pH value of the slurry to be neutral by using a sodium hydroxide aqueous solution with the mass fraction of 1.2%, filtering, and collecting roxburgh rose leaf filter residues; adding the roxburgh rose leaf filter residue into ethanol solution with the same weight and volume concentration of more than 80%, soaking until the solid content in the ethanol is 0.45mg/ml, filtering, and collecting roxburgh rose leaf ethanol solution; concentrating the ethanol solution of the roxburgh rose leaves until the solid content is 6.5mg/ml, transferring the roxburgh rose leaves into a refrigeration house, refrigerating at 4 ℃ until no precipitate is separated out, and extracting liquid to obtain roxburgh rose leaf precipitate; washing the roxburgh rose leaf precipitate with 0.18% sodium bicarbonate water solution for 2-3 times, and washing with boiling water for 2-3 times to obtain roxburgh rose leaf washing precipitate; washing the Rosa roxburghii leaf, precipitating, drying, pulverizing to obtain Rosa roxburghii leaf powder (containing Rosa roxburghii glycoside 50-60%, daucosterol 4-7.5%, physcion less than 0.5%, and sitosterol 1.2-1.8%), and preserving at 18 deg.C;

preparing buckwheat leaf powder: cleaning fresh buckwheat, transferring to a microwave dryer, treating at 42 deg.C for 60min, and spreading 0.65 wt% inorganic salt solution prepared by mixing sodium sulfate, magnesium sulfate, ammonium chloride, sodium chloride and sodium hydrogen phosphate at equal weight ratio of 7% to obtain treated buckwheat leaf every 12 min; then putting the treated buckwheat leaves into a cooking pot filled with clear water with the weight 2.5 times that of the buckwheat leaves, cooking the buckwheat leaves with slow fire until the solid content of the water liquid is 0.7mg/ml, and filtering the buckwheat leaves to obtain a buckwheat leaf water liquid; then adding 1.5% by weight of neutral alumina, bentonite and quartz sand powder of more than 300 meshes into the buckwheat leaf water solution according to the weight ratio of 3.5: 0.2: 0.8, stirring at 38 deg.C for 35min, and filtering to obtain decolorized folium Fagopyri Esculenti water solution; concentrating, drying, and pulverizing the decolorized buckwheat leaf water solution to obtain buckwheat leaf powder, and preserving at 18 deg.C;

fourthly, preparing the bamboo leaf powder: cleaning folium Bambusae, adding into ethanol solution with weight 3 times and volume concentration of above 70%, soaking at 50 deg.C until the solid content in ethanol is 1.9mg/ml, filtering, and collecting folium Bambusae ethanol solution; diluting the bamboo leaf ethanol solution with 0.38% sodium carbonate aqueous solution by mass fraction to obtain diluted bamboo leaf ethanol solution with solid content of 0.85mg/ml and pH value of 8.0; adding ethyl acetate with the same volume into the diluted bamboo leaf ethanol solution, stirring at normal temperature for 15min, standing, layering, and collecting supernatant; concentrating the supernatant under vacuum until no alcohol exists to obtain concentrated bamboo leaf extract; adjusting pH of the concentrated solution to 6.2 with 2.4% phosphoric acid solution, transferring into a refrigerator, refrigerating for 12 hr, filtering, and collecting the precipitate; drying and pulverizing the bamboo leaf extract precipitate to obtain bamboo leaf powder, and preserving at 18 deg.C for use;

fifth, preparing the livestock and poultry blood powder: preheating fresh pig blood to 55 deg.C, adding sodium chloride water solution with concentration of 0.7% and 4% of its weight, 0.8% of polyethylene glycol 200 (dispersant), stirring, treating at constant temperature for 28min, filtering with filter membrane device with pore diameter of 15 μm, collecting filtered pig blood water solution, introducing into adsorption column prepared by mixing vermiculite, dolomite, zeolite, and feldspar in equal weight ratio at addition rate of 20L/h, pulverizing into particles with particle diameter less than 0.5mm, standing for 7h after pig blood water solution is completely added, heating blood in the adsorption column to 55 deg.C by jacket, controlling flow rate at 38ml/min, collecting pig blood water solution flowing out, concentrating at pressure of 8KPa and temperature of 75 deg.C to solid content of 30.5mg/ml to obtain concentrated pig blood water solution, adding edible ethanol, regulating its alcohol degree to 60%, stirring for 12min, transferring to a refrigerator, standing at-2 deg.C for 6h, adding 0.8% sodium chloride, stirring, standing for 3h, filtering, collecting supernatant ethanol solution of pig blood, concentrating at 68 deg.C under 8KPa until solid content is 14mg/ml to obtain concentrated pig blood water solution, adding dichloromethane with the same volume, stirring at room temperature for 12min, standing, layering, collecting organic solvent extract, concentrating, drying, and pulverizing to obtain pig blood powder;

sixthly, preparing the garlic leaf powder: naturally drying fresh garlic leaves until the garlic leaves turn yellow, then crushing the garlic leaves into fine powder with the particle size of more than 60 meshes, transferring the fine powder into boiling water with the weight of 3 times of the garlic leaves, carrying out heat preservation and stirring treatment until the solid content in water liquid is 1.2mg/ml and the carotene content is higher than 0.05mg/ml, filtering, and collecting water extract of the garlic leaves; concentrating, drying and pulverizing the water extract of garlic leaves to obtain garlic leaf powder, and preserving at 18 ℃ for later use;

preparing dandelion leaf powder: selecting dandelion leaf powder which is extracted from dandelion leaves, has the phylloquinone content of more than 8.5 percent, the lutein content of more than 22.5 percent, the vitamin content of 2.5mg/10g and the residual quantity of ethanol solvent of less than 3.5ppm, and preserving at 18 ℃ for later use;

and eighthly, mixing: mixing the prepared rosemary leaf powder, roxburgh rose leaf powder, buckwheat leaf powder and bamboo leaf powder in equal weight proportion, and mixing with livestock and poultry blood powder, garlic leaf powder and dandelion leaf powder according to a ratio of 6: 1: 0.25: 0.5 weight ratio to obtain the traditional Chinese medicine leaf powder, and preserving at 18 ℃.

Preparing traditional Chinese medicine pollen:

firstly, preparing tea tree pollen: taking fresh tea flowers, and separating tea petals from tea pistils; firstly, soaking tea tree petals in 7% of vinegar solution for 12min, then washing with clear water for 2-3 times, then transferring to a drying oven, and drying at 65 ℃ until the water content is less than 5% to obtain dried tea tree petals; putting the tea plant pistils into a distiller, simultaneously adding pure water which accounts for 10 times of the weight of the tea plant pistils into the distiller, uniformly stirring, distilling until the volume of water liquid is reduced by 42%, and collecting tea plant pistils distillate; mixing dried tea petal with tea stamen distillate, boiling for 25min, filtering, and collecting tea flower water solution; then, concentrating, drying and crushing the tea flower water solution to obtain tea flower pollen for later use;

② preparing gardenia bud powder: grinding the prepared gardenia buds into gardenia bud coarse powder with the particle size of more than 10 meshes, then dripping ammonia water with the mass concentration of 4.5% according to the proportion of 7 drops/20 g, uniformly stirring, transferring into a microwave dryer, and treating for 25min at the power of 650W and the temperature of 48 ℃ to obtain microwave-treated gardenia bud coarse powder; then transferring the microwave-treated gardenia bud coarse powder into a sodium hydrogen phosphate solution with the mass fraction of 2.5%, stirring at 45 ℃ for 10min, and filtering to obtain treated gardenia bud powder; adding the treated fructus Gardeniae bud powder into 2 times of pure water, steaming with 50-55 deg.C slow fire until pH value of the water solution is 5.1, and filtering to obtain fructus Gardeniae bud powder water solution; concentrating, drying and pulverizing the water solution of the gardenia bud powder to obtain gardenia bud powder for later use;

③ preparing peony pollen: soaking flos Paeoniae in ethanol solution with 2.5 times weight and volume concentration of above 50% at 58 deg.C until solid content in ethanol solution is 3.6mg/ml to obtain flos Paeoniae ethanol soaking solution; adding 1.4% of the original peony flower weight, neutral alumina, ammonium chloride and quartz sand powder of more than 300 meshes into the peony flower ethanol soaking solution according to the weight ratio of 3.5: 0.2: 0.8, stirring at 45 ℃ for 38min, filtering, and collecting decolorized ethanol solution of peony flower; concentrating, drying and crushing the decolorized peony flower ethanol solution to obtain peony flower powder for later use;

preparing erigeron breviscapus pollen: firstly, putting the erigeron breviscapus into a sodium bicarbonate aqueous solution with the weight 2 times that of the erigeron breviscapus and the mass fraction of 0.4%, soaking for 32min at normal temperature, and filtering to obtain the treated erigeron breviscapus; then the treated erigeron breviscapus is transferred into boiling water with the same weight, and is stirred back and forth for 10min, and is filtered to obtain the boiling water treated erigeron breviscapus; adding boiling water-treated flos Hibisci into edible ethanol solution with weight 2.5 times and volume concentration above 35%, soaking at 58 deg.C until erigeron content in the ethanol solution is 0.15mg/ml, and filtering to obtain flos Hibisci ethanol soaking solution; vacuum concentrating the ethanol soaking solution at low temperature until the content of erigeron breviscapus glycoside is 1mg/ml to obtain erigeron breviscapus ethanol concentrated solution; transferring the concentrated solution into a refrigeration house, refrigerating at 5 deg.C until no precipitate is separated out, filtering, and collecting the upper layer of herba Erigerontis liquid; spray drying the erigeron breviscapus liquid to obtain erigeron breviscapus powder for later use;

fifthly, preparing momordica grosvenori pollen: cleaning flos Momordicae, soaking in 38% ethanol solution at 50 deg.C until the content of saccharide in the ethanol solution reaches 0.06mg/ml, and filtering to obtain flos Momordicae ethanol soaking solution; adding a decolorizing agent which is 0.5 percent of the weight of the original momordica grosvenori flower and is formed by mixing 100-mesh zeolite powder, sodium bicarbonate and bentonite according to the weight ratio of 1:0.04:1.5 into the momordica grosvenori flower ethanol soaking solution, stirring for 12min, filtering by a 0.5-micron filter membrane device, and collecting momordica grosvenori flower ethanol soaking filtrate; soaking the momordica grosvenori flower in ethanol, concentrating and drying the filtrate to obtain momordica grosvenori pollen for later use;

sixthly, preparing salvia miltiorrhiza pollen: soaking Salvia miltiorrhiza flower in 2.2 times of ethanol solution with volume concentration of more than 50% at 58 deg.C until the solid content in the ethanol solution is 1.15mg/ml to obtain Salvia miltiorrhiza flower ethanol soaking solution; then adding the neutral alumina, the ammonium chloride and the quartz sand powder with the granularity of more than 300 meshes which account for 0.65 percent of the weight of the original salvia miltiorrhiza flower into the ethanol soaking solution of the salvia miltiorrhiza flower according to the weight ratio of 3.5: 0.2: 0.8, stirring at 45 ℃ for 12min, filtering, and collecting the salvia miltiorrhiza flower ethanol soaking decolorized solution; then the ethanol-soaked destaining solution of the salvia miltiorrhiza flowers is concentrated, dried and crushed to obtain salvia miltiorrhiza pollen for later use;

and seventhly, preparing substitute pollen: firstly, mixing the seville orange flower with pure water of which the weight is 5 times that of the seville orange flower, putting the mixture into a distillation container, carrying out distillation treatment at 105 ℃ for 1.2h, taking out the mixture, and draining to obtain distilled seville orange flower; drying and crushing the distilled bitter orange to obtain bitter orange powder for later use;

and eighthly, mixing: mixing the prepared tea tree pollen, gardenia bud powder and peony pollen according to equal weight proportion, and then uniformly mixing the mixed pollen with breviscapine pollen, momordica grosvenori pollen, salvia miltiorrhiza pollen and substitutional pollen according to the weight proportion of 0.28:1:0.55:0.45:0.1 to obtain the traditional Chinese medicine pollen.

Preparing the fruit powder:

firstly, preparing apple powder: mixing fresh, cleaned and peeled apple pulp with sodium citrate solution with the same weight and the mass fraction of 1.8%, and processing into coarse pulp of apple pulp of 25 meshes by a pulping machine; preheating the apple pulp coarse slurry to 65 ℃, placing the apple pulp coarse slurry into a wide-mouth bottle, stirring until no oxidation phenomenon is generated in the slurry, adding 2.8% of diatomite and 300-mesh feldspar powder by weight: 1, stirring at constant temperature for 15min, filtering, and collecting the filtered apple pulp water solution; adding 0.05 wt% of preservative prepared from calcium propionate, natamycin and potassium sorbate according to equal weight proportion, stirring, sealing and transferring to a shade place for treatment for 2 days; concentrating, drying, pulverizing to obtain apple powder, and refrigerating at 2 deg.C;

preparing mangosteen powder: adding fresh mangosteen pulp into boiling water with the same weight, preserving heat until the solid content in the water solution is 2.2mg/ml, filtering to obtain mangosteen pulp water solution, concentrating, drying, pulverizing to obtain mangosteen powder, and refrigerating at 2 deg.C for use;

preparing the garlic root hair powder: cleaning garlic root, adding into 10% edible vinegar solution with the same weight, soaking at normal temperature for 35min, and filtering to obtain edible vinegar-processed garlic root; drying the garlic root treated with vinegar in the shade until the water content is less than 7.5%, and pulverizing into fine powder of garlic root hair of more than 40 meshes; adding the fine powder of Bulbus Allii root hair into 2 times of boiling water, boiling for 22min, stopping heating, cooling to 45 deg.C, filtering, and collecting water solution of Bulbus Allii root hair; spray drying the garlic root hair aqueous solution to obtain garlic root powder for later use;

fourthly, preparing bone soup powder: cleaning pig bones, and pulverizing into bone granules with particle size less than 0.5 cm; soaking the bone granules in 8% vinegar at 55 deg.C for 4 hr, and filtering to obtain pig bone vinegar soaking solution and soaked bone granules; crushing the soaked bone particles into 80-mesh or more soaked bone fine powder, adding 6.5 wt% of garlic seeds, 2 wt% of pepper powder and 8 wt% of white radish slices, and stirring to obtain a mixture; putting the mixture into a cooking pot, simultaneously adding clear water which accounts for 3 times of the weight of the mixture, cooking for 10 hours, turning off a heat source, adding proteolytic enzyme which accounts for 2.2 percent of the weight of the mixture and inorganic salt which accounts for 1.6 percent of the weight of the mixture and is formed by mixing sodium sulfate, zinc sulfate, calcium chloride and sodium chloride according to equal weight proportion into the cooking pot when the temperature in the cooking pot is reduced to 40 ℃, uniformly stirring, preserving heat for 4.5 hours, filtering, and collecting bone particle enzymolysis water liquid; mixing the bone particle enzymolysis water solution and pig bone edible vinegar soak solution to obtain pig bone extract, decocting with slow fire until the solid content in the solution is 5mg/ml, filtering with a filter membrane device with pore diameter of 15 μm, and collecting pig bone extract filtrate; drying and crushing the pig bone extraction filtrate to obtain bone soup powder for later use;

preparing the fish skin powder: cleaning fresh and edible fresh water fish skin, spreading on the surface of silica gel particles, transferring into a closed box, controlling the vacuum degree in the closed box at 7KPa and the temperature at 40 ℃, and processing until the water content in the fish skin is less than 8% to obtain dry fish skin; pulverizing dried fish skin into fine powder of more than 100 meshes to obtain fish skin powder for later use;

and eighthly, mixing: mixing the prepared apple powder and mangosteen powder according to equal weight proportion, and then uniformly mixing the apple powder and mangosteen powder with garlic root hair powder, bone soup powder and fish skin powder according to the weight proportion of 2.6:0.1:1.8:0.4 to obtain the fruit powder.

Preparing traditional Chinese medicine leather powder:

preparing the cortex dictamni powder: selecting cortex Dictamni Radicis powder which is prepared by extracting cortex Dictamni Radicis, has trigonelline content of 70-82%, phellodendron lactone content of 6-10%, limonin content of 1-2.5%, other components content of less than 1.5%, and solvent residue of less than 5ppm, and keeping;

② preparing the ash bark powder, cleaning the ash bark, cutting into ash bark slices with uniform width, adding edible ethanol with the same weight and volume concentration of more than 80%, soaking at normal temperature until the content of aesculin in the ethanol is higher than 0.15mg/ml, filtering to obtain the ash bark ethanol soaking solution; preheating the cortex Fraxini ethanol soak solution to 52 deg.C, simultaneously diluting with 0.45% buffer salt solution composed of sodium phosphate and sodium hydrogen phosphate at the same weight ratio at the same temperature until ethanol concentration is reduced to 45%, and stirring at constant temperature for 20 min; then diluting with 0.35% edible vinegar solution until ethanol concentration is reduced to 25%, stirring, standing until solution temperature is reduced to 22 deg.C, filtering, and collecting cortex Fraxini extract precipitate; washing the ash bark extract precipitate with clear water for 2-3 times to obtain washed ash bark extract precipitate; drying and pulverizing the washed ash bark extract precipitate to obtain ash bark powder for later use;

preparing asparagus lettuce skin powder: cleaning fresh asparagus lettuce, peeling the skin of the asparagus lettuce carrying the asparagus lettuce with the thickness less than 0.2cm, mixing the skin with warm water with the same weight and at 65 ℃, and processing the mixture into 10-mesh asparagus lettuce skin slurry by a grinder; filtering the asparagus lettuce epidermis slurry through a filter membrane device with the aperture of 30 microns, and collecting the filtrate of the asparagus lettuce epidermis slurry; concentrating, drying and crushing the asparagus lettuce epidermis slurry filtrate to obtain asparagus lettuce epidermis powder for later use;

preparing grape skin powder: selecting grape skin powder which is extracted from grape skin, contains 40-48% of anthocyanin, 45-60% of resveratrol, less than 1.2% of tannin and less than 50ppm of ethanol solvent residual quantity for later use;

preparing orange peel powder: putting fresh orange peel and clean water with the same weight into a distiller, boiling and distilling until the volume of water liquid is reduced by 42%, and filtering to obtain distilled orange peel; drying the distilled orange peel until the water content is less than 12%, grinding the dried orange peel into 30-mesh orange peel coarse powder, soaking the orange peel coarse powder in ethanol with the weight being 2.5 times of that of the orange peel coarse powder and the volume concentration being 70% for 6 hours, and filtering the orange peel coarse powder to obtain orange peel ethanol soaking liquid; concentrating, drying and crushing the orange peel ethanol soaking solution to obtain orange peel powder for later use;

sixthly, sugarcane peel powder: putting the cleaned and peeled sugarcane peels into a microwave vacuum dryer, and drying for 14min at the frequency of 120Hz, the power of 80W and the vacuum degree of 6KPa to obtain dried sugarcane peels; micronizing the dried sugarcane peel into dry sugarcane peel fine powder of more than 200 meshes, and uniformly mixing the dry sugarcane peel fine powder with bentonite of 100 meshes according to equal weight proportion to obtain mixed sugarcane peel fine powder; adding 2.5 times of boiling water into the mixed sugarcane peel fine powder, stirring uniformly, sealing, standing until the water temperature is reduced to room temperature, filtering, and collecting a mixed sugarcane peel fine powder water solution; spray drying the mixed sugarcane peel fine powder water solution to obtain sugarcane peel powder for later use;

and (c) mixing: mixing the prepared cortex dictamni powder, ash bark powder and asparagus lettuce bark powder in equal weight proportion, and then uniformly mixing the mixture with grape bark powder, orange bark powder and sugarcane bark powder in a weight proportion of 0.8:2.5:0.2:1 to obtain the traditional Chinese medicine bark powder.

Preparing an additive:

mixing dietary fiber, riboflavin, nicotinic acid, and a mixture of 1.5: 0.18: 0.08, and mixing to obtain the additive.

(2) Preparing materials:

respectively taking 80 parts of tea oil (edible tea oil meeting GB/T11765-2003 national standard), 5 parts of traditional Chinese medicine leaf powder, 2 parts of traditional Chinese medicine pollen, 10 parts of fruit powder, 2 parts of traditional Chinese medicine peel powder and 3 parts of additive according to parts by weight for later use;

(3) and (3) preparation:

firstly, mixing: firstly, uniformly mixing fruit powder and lecithin (edible surfactant) accounting for 0.8 percent of the weight of the fruit powder to obtain mixed fruit powder; preheating 1/5 of the tea oil to above 120 deg.C, slowly adding mixed fruit powder into hot tea oil under stirring at a rate of 50g/min, treating at constant temperature for 38min, and filtering with 300 mesh sieve to obtain primary mixed tea oil; transferring the primary mixed tea oil to a refrigeration house, refrigerating for 6h at 4 ℃, and then filtering by a 300-mesh screen to obtain a mixed tea oil I for later use;

secondly, mixing: mixing traditional Chinese medicine pollen and traditional Chinese medicine leaf powder to obtain traditional Chinese medicine mixed powder, adding N503 solvent (extractant) 2.5 times of the weight of the traditional Chinese medicine mixed powder and ammonium sulfate solution 2.5% of the weight of the traditional Chinese medicine mixed powder and 5.5% of the mass fraction, mixing, stirring at 38 deg.C for 3h, standing, layering, filtering, and collecting N503 solvent solution; then transferring the N503 solvent liquid into edible ethanol with the weight of 2.5 times and the volume concentration of more than 80%, performing rolling stirring treatment for 1.2h, then adding a sodium chloride solution with the mass fraction of 12% into the edible ethanol, wherein the adding amount of the sodium salt solution is 6% of the volume of the N503 solvent liquid, mixing and stirring for 20min, standing, layering, filtering, and collecting the ethanol extraction solution of the traditional Chinese medicine mixed powder; vacuum concentrating the ethanol extract solution of the Chinese medicinal mixed powder at low temperature until the solid content is 18mg/ml to obtain ethanol extract concentrated material of the Chinese medicinal mixed powder; preheating 2/5 of the tea oil to more than 150 ℃, slowly adding the ethanol-extracted concentrated material of the traditional Chinese medicine mixed powder into the hot tea oil while stirring, wherein the adding speed is 130g/min, after the tea oil is completely added, stirring at constant temperature for 38min, then closing a heat source, adding pure water which accounts for 28 percent of the weight of the tea oil (namely 2/5 of the tea oil) when the tea oil is naturally cooled to 75 ℃, stirring for 15min, then, continuously naturally cooling to room temperature, filtering, and collecting filtered tea oil to obtain second mixed tea oil for later use;

thirdly, mixing: mixing the Chinese medicinal peel powder with lecithin (edible surfactant) 1.8 wt% of the Chinese medicinal peel powder to obtain mixed Chinese medicinal peel powder; preheating 1/5 of the tea oil to 80 ℃, slowly adding the mixed traditional Chinese medicine peel powder into the tea oil while stirring, controlling the adding rate at 65g/min, and after all the powder is added, carrying out constant temperature treatment for 38min to obtain a third mixed tea oil for later use;

fourthly, mixing: preheating the rest 1/5 of the tea oil to 120 deg.C, slowly adding the additive into the tea oil while stirring, and filtering after dissolving to obtain mixed tea oil IV;

fifthly, total mixing: adding the mixed tea oil I, the mixed tea oil II, the mixed tea oil III and the mixed tea oil IV into a mixing container, uniformly stirring, heating to 180 ℃ at a heating rate of 12 ℃/min, and stirring at a constant temperature for 2 hours to obtain total mixed tea oil; then 3.5 percent of neutral active carbon, 3A type molecular sieve, 300-mesh vermiculite powder and calcium chloride powder are mixed according to the weight ratio of 3: 1: 0.6: 0.18 weight percent of mixed decolorant is added, stirred and decolored for 35min, filtered, and the decolored mixed tea oil is collected for standby;

sixthly, fine filtering: subjecting the decolorized mixed tea oil to supercritical fine filtration or nano-membrane device fine filtration to obtain tea oil for preventing enteritis.

Example 2:

the tea oil for preventing enteritis of the embodiment is prepared by the following steps:

firstly, raw material pretreatment:

same as example 1;

(2) preparing materials:

respectively taking 90 parts of tea oil (edible tea oil meeting GB/T11765-2003 national standard), 2 parts of traditional Chinese medicine leaf powder, 7 parts of traditional Chinese medicine pollen, 4 parts of fruit powder, 5 parts of traditional Chinese medicine peel powder and 1 part of additive according to parts by weight for later use;

(3) and (3) preparation:

same as in example 1.

Example 3:

the tea oil for preventing enteritis of the embodiment is prepared by the following steps:

firstly, raw material pretreatment:

same as example 1;

(2) preparing materials:

according to the parts by weight, 85 parts of tea oil (edible tea oil meeting GB/T11765-2003 national standard), 3.5 parts of traditional Chinese medicine leaf powder, 4.5 parts of traditional Chinese medicine pollen, 7 parts of fruit powder, 3.5 parts of traditional Chinese medicine peel powder and 2 parts of additive are respectively taken for later use;

(3) and (3) preparation:

same as in example 1.

The tea oil for preventing enteritis is suitable for people of all ages to eat.