阅读说明：本技术 一种金刚石生产电解用电解液 (Electrolyte for electrolysis in diamond production ) 是由 邹林汇 于 2020-11-12 设计创作，主要内容包括：本发明公开了一种金刚石生产电解用电解液,涉及电解液技术领域,其原料包含以下重量份的组分：柠檬酸30-100份,氯化铵100-150份,本发明制备方法简单,采用该金刚石生产电解用电解液的制备设备制备时,能够将由于离心而靠近混合罐内壁的固态晶体破碎,使原料更易混合均匀,也大大提高了原料混合的速率,且通过设置的净化机构,能够净化生产过程中产生的氨气,避免尾气污染环境,健康环保,且本发明制备的电解液在金刚石生产电解过程中,所需的电解时间短,且由电化学电极电位顺序可知,镍、钴等金属均较铁为正,使得电解液的氧化还原性强,优先在阴极板上还原沉积,保证了金属的回收率,从而提高了金刚石生产电解的效率。(The invention discloses an electrolyte for diamond production electrolysis, which relates to the technical field of electrolytes and comprises the following raw materials in parts by weight: 30-100 parts of citric acid and 150 parts of ammonium chloride, and the preparation method is simple, when the preparation equipment for the electrolyte for diamond production and electrolysis is used for preparation, solid crystals close to the inner wall of a mixing tank due to centrifugation can be crushed, so that raw materials are more uniformly mixed, the rate of mixing the raw materials is greatly increased, ammonia gas generated in the production process can be purified through the arranged purification mechanism, tail gas pollution to the environment is avoided, the preparation method is healthy and environment-friendly, the required electrolysis time of the prepared electrolyte in the diamond production and electrolysis process is short, and the electrochemical electrode potential sequence shows that metals such as nickel, cobalt and the like are positive compared with iron, so that the redox property of the electrolyte is strong, reduction and deposition are preferentially carried out on a cathode plate, the recovery rate of the metals is ensured, and the efficiency of diamond production and electrolysis is improved.)

1. The electrolytic solution for diamond production is characterized by comprising the following raw materials in parts by weight: 30-100 parts of citric acid, 100-150 parts of ammonium chloride, 10-20 parts of boric acid, 2-4 parts of emulsifier, 2-4 parts of sodium chloride, 31,2-35.3 parts of iron, 40.5-48.6 parts of nickel, 0.2-0.6 part of cobalt, 0.1-0.3 part of manganese, 0.8-2.4 parts of copper, 1.2-4.8 parts of aluminum, 0.15-0.45 part of silicon, 0.15-0.45 part of magnesium and a plurality of parts of water.

2. An electrolyte for electrolysis in diamond production according to claim 1, wherein the raw material comprises the following components in parts by weight: 70 parts of citric acid, 90 parts of ammonium chloride, 16 parts of boric acid, 3 parts of emulsifier, 3 parts of sodium chloride, 33.4 parts of iron, 44.3 parts of nickel, 0.3 part of cobalt, 0.2 part of manganese, 1.4 parts of copper, 2.8 parts of aluminum, 0.25 part of silicon, 0.35 part of magnesium and a plurality of parts of water.

3. An electrolyte for electrolysis in diamond production according to claim 1, wherein the ammonium chloride, citric acid and boric acid are all solid crystals with a purity of 99% or more.

4. The preparation equipment of the electrolyte for electrolysis in diamond production according to claim 1, which comprises a mixing tank (2), wherein a plurality of support legs (1) are fixedly connected to the lower surface of the mixing tank (2), a discharge pipe (8) is fixedly communicated with the lower surface of the mixing tank (2), a matched control valve I (7) is installed on the discharge pipe (8), a plurality of uniformly distributed cavities (15) are formed in the side wall of the mixing tank (2), matched electric heating wires (14) are installed in the cavities (15), a feed pipe (4) is fixedly connected to the upper surface of the mixing tank (2), a matched cover body (5) is in threaded connection with the feed pipe (4), a motor I (6) is installed on the upper surface of the mixing tank (2), the output end of the motor I (6) penetrates through the upper surface of the mixing tank (2) and is fixedly connected with a rotating shaft I (16) through a coupler, the side fixedly connected with puddler (9) of a plurality of evenly distributed of pivot (16), the equal fixedly connected with in upper surface and the lower surface of puddler (9) move sword (17), the medial surface fixedly connected with of blending tank (2) a plurality of with move sword (17) matched with stationary knife (18), the lower extreme of pivot (16) still fixedly connected with scraper blade (10) that two symmetries set up, the last fixed surface of blending tank (2) is connected with blast pipe (11), the other end of blast pipe (11) is connected with purification mechanism.

5. The electrolytic preparation equipment for diamond production according to claim 4, wherein the purification mechanism comprises an air pump (12), an air pipe (28), a support plate (26), a support rod (25), a purification box (21), a liquid discharge pipe (24) and an air outlet pipe (22), the air pump (12) is installed on the side surface of the mixing tank (2), the other end of the air outlet pipe (11) is fixedly communicated with the inlet of the air pump (12), the air pipe (28) is fixedly communicated with the outlet of the air pump (12), the support plate (26) is fixedly connected to the side surface of the mixing tank (2), the purification box (21) is fixedly connected to the upper surface of the support plate (26) through a plurality of support rods (25), a plurality of saturated salt water is arranged in the purification box (21), the crushing mechanism is also installed in the purification box (21), the other end of the air pipe (28) penetrates through the side surface of the purification box (21) and is inserted in the saturated salt water, an air outlet pipe (22) is fixedly communicated with the upper surface of the purification box (21), a liquid discharge pipe (24) is fixedly communicated with the side surface of the purification box (21), and a second control valve (23) matched with the liquid discharge pipe (24) is installed on the liquid discharge pipe.

6. The electrolytic solution preparation device for diamond production according to claim 5, wherein the crushing mechanism comprises a second motor (19), a second rotating shaft (27) and a crushing rod (29), the second motor (19) is installed on the lower surface of the purifying box (21), the output end of the second motor (19) penetrates through the lower surface of the purifying box (21) and is fixedly connected with the second rotating shaft (27) through a coupler, two symmetrically arranged crushing rods (29) are fixedly connected to the side surface of the second rotating shaft (27), and a plurality of uniformly distributed convex blocks (30) are fixedly connected to the side surface of the crushing rods (29).

7. A diamond production electrolyte preparation apparatus according to claim 5, wherein the lower surface of the support plate (26) is fixedly connected with the side of the mixing tank (2) through two parallel ribs (20).

8. The electrolytic solution preparation device for diamond production according to claim 4, wherein the temperature sensor (13) is installed on the inner side surface of the mixing tank (2), the temperature controller (3) is installed on the side surface of the mixing tank (2), and the temperature sensor (13) and the electric heating wire (14) are both electrically connected with the temperature controller (3).

9. The preparation steps of the electrolytic solution for diamond production according to claims 1-8, characterized by comprising the following steps:

the method comprises the following steps: and (3) opening the cover body (5), and sequentially adding water, citric acid, ammonium chloride and boric acid into the mixing tank (2) through the feeding pipe (4).

Step two: under the temperature condition of normal temperature, a first motor (6) and an air pump (12) are started, the first motor (6) rotates to drive a first rotating shaft (16) to rotate, the first rotating shaft (16) rotates to drive a stirring rod (9) to rotate, the stirring rod (9) rotates to drive a movable cutter (17) to rotate, solid crystals close to the inner wall of a mixing tank (2) due to centrifugation can be crushed through shear stress generated by matching the movable cutter (17) with a fixed cutter (18), raw materials are more uniformly mixed, the speed of raw material mixing is greatly improved, the first rotating shaft (16) rotates to drive two scraping plates (10) to rotate, accumulation and precipitation at the bottom of the mixing tank (2) in the mixing process are avoided, the air pump (12) exhausts air through an exhaust pipe (11) in the mixing process, and ammonia gas generated in the mixing process is pumped into a purification tank (21) through the exhaust pipe (11) and an air delivery pipe (28) along with air flow, the ammonia gas is purified by the saturated salt water in the purifying box (21), and the purified gas is discharged by the gas outlet pipe (22), so that the tail gas is prevented from polluting the environment, and the stirring is carried out for 40-50 minutes in the environment.

Step three: after stirring, adding the emulsifier and boric acid into the mixing tank (2) through the feeding pipe (4), covering the cover body 5, starting the motor I (6) again, starting the electric heating wire (14), and heating and stirring for 10-20 minutes at the temperature of 60-70 ℃.

Step four: after stirring, adding metal elements of iron, nickel, cobalt, manganese, copper, aluminum, silicon and magnesium into the mixing tank (2) through the feeding pipe (4), covering the cover body 5, starting the motor I (6) and the electric heating wire (14) again, and heating and stirring for 30-40 minutes at the temperature of 60-70 ℃.

Step five: after stirring, starting the electric heating wire (14), and standing for more than 24 hours at the temperature of 60-70 ℃ to ensure that the raw materials with various properties fully play roles and are mutually permeated and fused.

Step six: and discharging the finished product from a discharge pipe (8), and filling and packaging the finished product.

Technical Field

The invention relates to the technical field of electrolyte, in particular to electrolyte for producing and electrolyzing diamond.

Background

The synthetic block is needed to be eliminated in order to ensure the quality of the artificial diamond, a common synthetic block elimination method comprises mechanical crushing, but the synthetic block is hard and difficult to break, the difficulty of crushing the diamond is high, equipment is easy to wear, the production efficiency is low, the quality of the produced diamond is poor, and a synthetic block elimination method also comprises a 'aqua regia method', wherein concentrated sulfuric acid, perchloric acid and hydrofluoric acid are used for dissolving out the synthetic block. The method for eliminating the synthesis block also comprises an electrolysis method, wherein the synthesis column is crushed and then electrolyzed, the catalyst metal in the synthesis block is oxidized into metal ions and then dissolved in the electrolyte, and then the metal ions are reduced and recovered on a cathode.

Disclosure of Invention

The invention aims to provide an electrolyte for diamond production electrolysis, which solves the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme:

an electrolyte for producing and electrolyzing diamond comprises the following raw materials in parts by weight: 30-100 parts of citric acid, 100-150 parts of ammonium chloride, 10-20 parts of boric acid, 2-4 parts of emulsifier, 2-4 parts of sodium chloride, 31,2-35.3 parts of iron, 40.5-48.6 parts of nickel, 0.2-0.6 part of cobalt, 0.1-0.3 part of manganese, 0.8-2.4 parts of copper, 1.2-4.8 parts of aluminum, 0.15-0.45 part of silicon, 0.15-0.45 part of magnesium and a plurality of parts of water.

As a further scheme of the invention: the raw materials comprise the following components in parts by weight: 70 parts of citric acid, 90 parts of ammonium chloride, 16 parts of boric acid, 3 parts of emulsifier, 3 parts of sodium chloride, 33.4 parts of iron, 44.3 parts of nickel, 0.3 part of cobalt, 0.2 part of manganese, 1.4 parts of copper, 2.8 parts of aluminum, 0.25 part of silicon, 0.35 part of magnesium and a plurality of parts of water.

As a further scheme of the invention: the ammonium chloride, the citric acid and the boric acid are all solid crystals, and the purity is more than 99%.

As a further scheme of the invention: a preparation device of electrolyte for electrolysis in diamond production comprises a mixing tank, wherein a plurality of supporting legs are fixedly connected to the lower surface of the mixing tank, a discharging pipe is fixedly communicated with the lower surface of the mixing tank, a first matched control valve is installed on the discharging pipe, a plurality of uniformly distributed cavities are formed in the side wall of the mixing tank, matched electric heating wires are installed in the cavities, a feeding pipe is fixedly connected to the upper surface of the mixing tank, a matched cover body is connected to the feeding pipe in a threaded manner, a first motor is installed on the upper surface of the mixing tank, the output end of the first motor penetrates through the upper surface of the mixing tank and is fixedly connected with a first rotating shaft through a coupler, a plurality of uniformly distributed stirring rods are fixedly connected to the side surface of the first rotating shaft, moving blades are fixedly connected to the upper surface and the lower surface of each stirring rod, a plurality of fixed blades matched with the moving blades are fixedly connected to the inner side surface, the upper surface of the mixing tank is fixedly connected with an exhaust pipe, and the other end of the exhaust pipe is connected with a purification mechanism.

As a further scheme of the invention: purifying mechanism includes the air pump, the gas-supply pipe, the backup pad, the bracing piece, the purifying box, fluid-discharge tube and outlet duct, the side-mounting of blending tank has the air pump, the other end of blast pipe and the fixed intercommunication of import of gas pump, the fixed intercommunication of export of gas pump has the gas-supply pipe, the side fixedly connected with backup pad of blending tank, the upper surface of backup pad is through a plurality of bracing piece fixedly connected with purifying boxes, set up a plurality of saturated salt solution in the purifying box, still install broken mechanism in the purifying box, the other end of gas-supply pipe runs through the side of purifying box and runs through and insert in saturated salt solution, the last fixed surface intercommunication of purifying box has the outlet duct, the fixed intercommunication in side of purifying box has the fluid-discharge tube, install assorted.

As a further scheme of the invention: the crushing mechanism comprises a second motor, a second rotating shaft and crushing rods, the second motor is mounted on the lower surface of the purifying box, the output end of the second motor penetrates through the lower surface of the purifying box and is fixedly connected with the second rotating shaft through a coupler, the two crushing rods are symmetrically arranged on the side surfaces of the second rotating shaft, and the side surfaces of the crushing rods are fixedly connected with a plurality of uniformly distributed lugs.

As a further scheme of the invention: the lower surface of the supporting plate is fixedly connected with the side surface of the mixing tank through two rib plates which are arranged in parallel.

As a further scheme of the invention: temperature sensor is installed to the medial surface of blending tank, and the side-mounting of blending tank has the temperature controller, and temperature sensor and electric heating wire all with temperature controller electric connection.

As a further scheme of the invention: the preparation method of the electrolyte for diamond production and electrolysis comprises the following specific steps:

the method comprises the following steps: and opening the cover body, and adding water, citric acid, ammonium chloride and boric acid into the mixing tank through the feeding pipe in sequence.

Step two: under the temperature condition of normal temperature, a first motor and an air pump are started, the first motor rotates to drive a first rotating shaft to rotate, the first rotating shaft drives a stirring rod to rotate, the stirring rod rotates to drive a movable cutter to rotate, solid crystals close to the inner wall of a mixing tank due to centrifugation can be crushed through the shear stress generated by the cooperation of the movable cutter and a fixed cutter, raw materials are mixed uniformly, the mixing speed of the raw materials is greatly improved, the rotation of the first rotating shaft drives two scraping plates to rotate, the accumulation and the precipitation at the bottom of the mixing tank in the mixing process are avoided, in the mixing process, the air pump conducts air draft through an exhaust pipe, ammonia gas generated in the mixing process is pumped into a purifying box along with air flow through the exhaust pipe and an air conveying pipe, the ammonia gas is purified through saturated saline water in the purifying box, and then the purified gas is discharged through an air outlet pipe, so that the tail gas is prevented from polluting the environment, stirring for 40-50 min.

Step three: after stirring, sequentially adding the emulsifier and boric acid into the mixing tank through the feeding pipe, covering the cover body, starting the motor I again, starting the electric heating wire at the same time, and heating and stirring for 10-20 minutes at the temperature of 60-70 ℃.

Step four: after stirring, adding metal elements of iron, nickel, cobalt, manganese, copper, aluminum, silicon and magnesium into the mixing tank through the feeding pipe in sequence, covering the cover body, starting the motor I and the electric heating wire again, and heating and stirring for 30-40 minutes at the temperature of 60-70 ℃.

Step five: after stirring, starting the electric heating wire, and standing for more than hours at the temperature of 60-70 ℃ to ensure that the raw materials with various properties fully exert the functions and are mutually permeated and fused.

Step six: and discharging the finished product from a discharge pipe, and filling and packaging the finished product.

Compared with the prior art, the invention has the beneficial effects that:

1. the preparation method is simple, when the preparation equipment for producing the electrolyte for electrolysis by using the diamond is used for preparation, the solid crystals close to the inner wall of the mixing tank due to centrifugation can be crushed, so that the raw materials are easy to mix uniformly, the raw material mixing speed is greatly improved, and the ammonia gas generated in the production process can be purified by the arranged purification mechanism, so that the environment pollution caused by tail gas is avoided, and the preparation equipment is healthy and environment-friendly.

2. The invention can break the bubbles in the saturated salt solution through the arranged crushing mechanism, so that the gas is more fully contacted with the saturated salt solution, and the purification effect is improved.

2. The electrolyte prepared by the invention has short electrolysis time in the diamond production electrolysis process, and the electrochemical electrode potential sequence shows that metals such as nickel, cobalt and the like are more positive than iron, so that the oxidation-reduction property of the electrolyte is strong, the reduction and the deposition are preferentially carried out on a negative plate, the recovery rate of the metals is ensured, and the diamond production electrolysis efficiency is improved.

Drawings

FIG. 1 is a schematic view of the structure of a production apparatus in the present invention;

FIG. 2 is a schematic sectional view of the manufacturing apparatus of the present invention;

FIG. 3 is a schematic rear view of the manufacturing apparatus of the present invention;

FIG. 4 is a rear sectional view schematically showing the construction of the manufacturing apparatus of the present invention;

fig. 5 is an enlarged schematic view of a portion a in fig. 4.

In the figure: 1. supporting legs; 2. a mixing tank; 3. a temperature controller; 4. a feed pipe; 5. a cover body; 6. a first motor; 7. a first control valve; 8. a discharge pipe; 9. a stirring rod; 10. a squeegee; 11. an exhaust pipe; 12. an air pump; 13. a temperature sensor; 14. an electric heating wire; 15. a cavity; 16. a first rotating shaft; 17. moving a knife; 18. fixing a cutter; 19. a second motor; 20. a rib plate; 21. a purification box; 22. an air outlet pipe; 23. a second control valve; 24. a liquid discharge pipe; 25. a support bar; 26. a support plate; 27. a second rotating shaft; 28. a gas delivery pipe; 29. a breaking bar; 30. and (4) a bump.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1 to 5, in an embodiment of the present invention, an electrolyte for electrolysis in diamond production includes the following components in parts by weight: 30-100 parts of citric acid, 100-150 parts of ammonium chloride, 10-20 parts of boric acid, 2-4 parts of emulsifier, 2-4 parts of sodium chloride, 31,2-35.3 parts of iron, 40.5-48.6 parts of nickel, 0.2-0.6 part of cobalt, 0.1-0.3 part of manganese, 0.8-2.4 parts of copper, 1.2-4.8 parts of aluminum, 0.15-0.45 part of silicon, 0.15-0.45 part of magnesium and a plurality of parts of water.

The raw materials comprise the following components in parts by weight: 70 parts of citric acid, 90 parts of ammonium chloride, 16 parts of boric acid, 3 parts of emulsifier, 3 parts of sodium chloride, 33.4 parts of iron, 44.3 parts of nickel, 0.3 part of cobalt, 0.2 part of manganese, 1.4 parts of copper, 2.8 parts of aluminum, 0.25 part of silicon, 0.35 part of magnesium, a plurality of parts of water, and the ammonium chloride, the citric acid and the boric acid are all solid crystals with the purity of more than 99%.

A preparation device of electrolyte for electrolysis in diamond production comprises a mixing tank 2, a plurality of supporting legs 1 are fixedly connected to the lower surface of the mixing tank 2, a discharge pipe 8 is fixedly communicated with the lower surface of the mixing tank 2, a matched control valve I7 is installed on the discharge pipe 8, a plurality of uniformly distributed cavities 15 are formed in the side wall of the mixing tank 2, matched electric heating wires 14 are installed in the cavities 15, a feed pipe 4 is fixedly connected to the upper surface of the mixing tank 2, a matched cover body 5 is connected to the feed pipe 4 in a threaded manner, a motor I6 is installed on the upper surface of the mixing tank 2, the output end of the motor I6 penetrates through the upper surface of the mixing tank 2 and is fixedly connected with a rotating shaft I16 through a coupler, a plurality of uniformly distributed stirring rods 9 are fixedly connected to the side surface of the rotating shaft I16, moving blades 17 are fixedly connected to the upper surface and the lower surface of each stirring rod 9, a plurality of fixed blades 18 matched with the, the lower end of the first rotating shaft 16 is fixedly connected with two symmetrically arranged scraping plates 10, the upper surface of the mixing tank 2 is fixedly connected with an exhaust pipe 11, and the other end of the exhaust pipe 11 is connected with a purification mechanism.

Purification mechanism includes air pump 12, gas-supply pipe 28, backup pad 26, bracing piece 25, purifying box 21, fluid-discharge tube 24 and outlet duct 22, the side-mounting of blending tank 2 has air pump 12, the other end of blast pipe 11 and the fixed intercommunication of the import of air pump 12, the fixed intercommunication of the export of air pump 12 has gas-supply pipe 28, the side fixedly connected with backup pad 26 of blending tank 2, the upper surface of backup pad 26 is through a plurality of bracing pieces 25 fixedly connected with purifying box 21, set up a plurality of saturated salt solution in the purifying box 21, still install broken mechanism in the purifying box 21, the other end of gas-supply pipe 28 runs through the side of purifying box 21 and runs through and insert in the saturated salt solution, the fixed intercommunication of upper surface of purifying box 21 has outlet duct 22, the fixed intercommunication in side of purifying box 21 has fluid-discharge tube 24, install two 23 of assorted control valve on.

The crushing mechanism comprises a second motor 19, a second rotating shaft 27 and a crushing rod 29, the second motor 19 is installed on the lower surface of the purifying box 21, the output end of the second motor 19 penetrates through the lower surface of the purifying box 21 and is fixedly connected with the second rotating shaft 27 through a coupler, the two crushing rods 29 are symmetrically arranged on the side surfaces of the second rotating shaft 27, a plurality of uniformly distributed convex blocks 30 are fixedly connected to the side surfaces of the crushing rods 29, and through the arranged crushing mechanism, in the tail gas purifying process, the second rotating shaft 27 is driven to rotate through the rotation of the second motor 19, the crushing rods 29 are driven to rotate through the rotation of the second rotating shaft 27, and through the rotating crushing rods 29 and the convex blocks 30 on the surfaces of the rotating crushing rods 29, bubbles in saturated salt water can be broken, so that gas is more fully contacted with the saturated salt water, and the.

The lower surface of the supporting plate 26 is fixedly connected with the side surface of the mixing tank 2 through two parallel ribbed plates 20, and the structure of the supporting plate 26 is more stable through the arranged ribbed plates 20.

Temperature sensor 13 is installed to the medial surface of blending tank 2, and the side-mounting of blending tank 2 has temperature controller 3, and temperature sensor 13 and electric heating wire 14 all with 3 electric connection of temperature controller, through the temperature controller 3 that sets up, be convenient for to the automatic control of blending tank 2 internal temperature (for prior art, do not many here and drag continuously).

The preparation method of the electrolyte for diamond production and electrolysis comprises the following specific steps:

the method comprises the following steps: the cover body 5 is opened, and water, citric acid, ammonium chloride and boric acid are sequentially added into the mixing tank 2 through the feeding pipe 4.

Step two: under the temperature condition of normal temperature, the first motor 6 and the air pump 12 are started, the first motor 6 rotates to drive the first rotating shaft 16 to rotate, the first rotating shaft 16 rotates to drive the stirring rod 9 to rotate, the stirring rod 9 rotates to drive the movable cutter 17 to rotate, solid crystals close to the inner wall of the mixing tank 2 due to centrifugation can be crushed through shear stress generated by the cooperation of the movable cutter 17 and the fixed cutter 18, raw materials are mixed uniformly, the speed of raw material mixing is greatly improved, the rotation of the first rotating shaft 16 drives the two scraping plates 10 to rotate, the bottom of the mixing tank 2 is prevented from being accumulated and precipitated in the mixing process, the air pump 12 performs air draft through the exhaust pipe 11 in the mixing process, ammonia gas generated in the mixing process is pumped into the purifying tank 21 through the exhaust pipe 11 and the air conveying pipe 28 along with air flow, the ammonia gas is purified through salt saturated water in the purifying tank 21, and then purified gas is discharged through the air outlet pipe 22, thereby avoiding the tail gas polluting the environment, and stirring for 40-50 minutes in the environment.

Step three: after stirring, sequentially adding the emulsifier and boric acid into the mixing tank 2 through the feeding pipe 4, covering the cover body 5, starting the motor I6 again, starting the electric heating wire 14 at the same time, and heating and stirring for 10-20 minutes at the temperature of 60-70 ℃.

Step four: after stirring, adding metal elements of iron, nickel, cobalt, manganese, copper, aluminum, silicon and magnesium into the mixing tank 2 from the feeding pipe 4 in sequence, covering the cover body 5, starting the first motor 6 and the electric heating wire 14 again, and heating and stirring for 30-40 minutes at the temperature of 60-70 ℃.

Step five: after the stirring is finished, metal elements of iron, nickel, cobalt, manganese, copper, aluminum, silicon and magnesium are sequentially added into the mixing tank 2 through the feeding pipe 4.

Step six: after stirring, starting the electric heating wire 14, and standing for more than 24 hours at the temperature of 60-70 ℃ to allow the raw materials with various properties to fully exert the functions to be mutually permeated and fused.

Step six: and discharging the finished product through a discharge pipe 8, and filling and packaging the finished product.

The electrolyte prepared by the invention has short electrolysis time in the diamond production electrolysis process, and the electrochemical electrode potential sequence shows that metals such as nickel, cobalt and the like are more positive than iron, so that the oxidation-reduction property of the electrolyte is strong, the reduction and the deposition are preferentially carried out on a negative plate, the recovery rate of the metals is ensured, and the diamond production electrolysis efficiency is improved.

The electric elements presented in the text are all electrically connected with an external main controller and 220V mains supply through a transformer, the main controller can be a conventional known device controlled by a computer and the like, the electric elements provided by the invention are only used according to the structural characteristics of the product, the product can be adjusted and modified after being purchased, so that the product is more matched with and accords with the technical scheme of the invention, the electric elements are a technical scheme which is the best application of the technical scheme, the model of the product can be replaced and modified according to the required technical parameters, and the product is familiar to the technical personnel skilled in the art, so that the technical scheme provided by the invention can clearly obtain the corresponding use effect.

Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.