阅读说明：本技术 一种高温合金定向凝固装置及凝固方法 (High-temperature alloy directional solidification device and solidification method ) 是由 王富 刘洋 张碧璇 段倩 杨强 于 2021-06-18 设计创作，主要内容包括：本发明公开了一种高温合金定向凝固装置及凝固方法,属于金属铸造技术领域,旨在解决锚形模壳散热不均匀导致的晶体组织中雀斑等缺陷性问题和高温合金定向凝固过程中的晶体的浪费问题。本发明通过加热器便可以实现合金液的保温或过热状态,通过提拉杆将锚形模壳以恒定速度向上提拉,再对锚形模壳上设置水冷系统,此时锚形模壳逐渐浮出恒温流质使液面的部分热量散失,从而产生温度梯度,迫使接触子晶的合金液向下定向凝固形成单晶体,可以有效的解决锚形模壳的散热问题,也避免了晶体组织中雀斑等缺陷性问题,降低了定向凝固过程中的晶体的浪费。(The invention discloses a directional solidification device and a solidification method for a high-temperature alloy, belongs to the technical field of metal casting, and aims to solve the defect problems of freckles and the like in a crystal structure caused by uneven heat dissipation of an anchor-shaped formwork and the waste problem of crystals in the directional solidification process of the high-temperature alloy. The invention can realize the heat preservation or overheating state of the alloy liquid by the heater, the anchor-shaped mould shell is lifted upwards at a constant speed by the lifting rod, and then the water cooling system is arranged on the anchor-shaped mould shell, at the moment, the anchor-shaped mould shell gradually floats out constant-temperature fluid to dissipate partial heat of the liquid level, so that a temperature gradient is generated, the alloy liquid contacting with the crystal is forced to directionally solidify downwards to form a single crystal, the heat dissipation problem of the anchor-shaped mould shell can be effectively solved, the defect problems of freckles and the like in the crystal tissue are avoided, and the waste of the crystal in the directional solidification process is reduced.)

1. The high-temperature alloy directional solidification device is characterized by comprising a cabin body (1) and two lifting rods (3), wherein a cabin cover (2) is arranged above the cabin body (1), and the lifting rods (3) penetrate through the cabin cover (2) and extend into the cabin body (1); a pouring hole (201) is also formed in the hatch cover (2);

the improved aluminum alloy casting cabin is characterized in that a heater (4), a constant-temperature crucible (5), a water cooling system and an anchor-shaped formwork (7) are arranged in the cabin body (1), constant-temperature fluid (502) is filled in the constant-temperature crucible (5), the heater (4) is used for heating the constant-temperature fluid (502), the anchor-shaped formwork (7) is arranged in the constant-temperature crucible (5), a crystal (601) is arranged above the anchor-shaped formwork (7), the water cooling system is arranged above the crystal (601), a lifting rod (3) is used for lifting the anchor-shaped formwork (7) and the water cooling system upwards at a constant speed, a pouring gate (702) is formed in the anchor-shaped formwork (7), and the pouring gate (702) is arranged opposite to a pouring hole (201) in the cabin cover (2) and used for pouring alloy liquid into the anchor-shaped formwork (7).

2. The directional solidification device for the high-temperature alloy according to claim 1, wherein the anchor mold shell (7) further comprises a thick neck (701), a pouring channel (703), an alloy mold (704) and a runner (705), the pouring channel (703) is communicated below the pouring channel (702), the radial runner (705) is communicated below the pouring channel (703), the runner (705) comprises a plurality of branches, the end of each branch is communicated with 1 alloy mold (704), the daughter crystal (601) is arranged above the alloy mold (704), and the thick neck (701) is arranged at the joint of the pouring channel (703) and the pouring channel (702).

3. A superalloy directional solidification device as claimed in claim 2, characterised in that the anchor form (7) is an alumina ceramic.

4. The directional solidification device for the high-temperature alloy, as recited in claim 2, is characterized in that the lifting rod (3) is L-shaped, and the two lifting rods (3) are clamped and fixed at the bottom end of the thick neck (701).

5. The directional solidification device for the high-temperature alloy, according to the claim 1, is characterized in that the water cooling system comprises a chilling block (202), a water cooling ring (6) and a water cooling hose (602), the chilling block (202) is arranged above the cabin cover (2) in a surrounding mode, the water cooling ring (6) is located above the daughter crystal (601), the lower end of the water cooling hose (602) is connected with the water cooling ring (6), and the upper end of the water cooling hose (602) penetrates through the cabin cover (2) to be communicated with the chilling block (202).

6. The directional solidification apparatus for superalloy as claimed in claim 1, wherein a thermal resistance pad (501) is further provided between the inner bottom surface of the chamber (1) and the bottom wall of the thermostatic crucible (5).

7. A superalloy directional solidification device as claimed in claim 1, characterised in that a thermal insulating float (503) is applied to the surface of the isothermal fluid (502), the density of the thermal insulating float (503) being less than the density of the isothermal fluid (502).

8. A superalloy directional solidification device as claimed in claim 7, wherein the constant temperature fluid (502) is aluminum, copper, or an aluminum copper alloy;

the heat insulation floating blocks (503) are ceramic balls, ceramic tiles or irregular ceramic particles, and the size of the heat insulation floating blocks (503) is 2-10 mm.

9. The directional solidification apparatus for superalloy as claimed in claim 1, further comprising an air passage (101), wherein the air passage (101) is located on a sidewall of the chamber (1) for evacuating the chamber (1).

10. The solidification method based on the high-temperature alloy directional solidification device as set forth in any one of claims 1 to 9, comprising the steps of:

step 1: preparation phase

Installing a high-temperature alloy directional solidification device, and pouring constant-temperature fluid (502) into a constant-temperature crucible (5) to submerge the plane of the sub-crystal (601);

step 2: preheating constant temperature fluid (502)

Turning on the heater (4) to melt the constant-temperature fluid (502) in the constant-temperature crucible (5) into fluid;

and step 3: injecting alloy liquid

Injecting prepared superheated alloy liquid from the pouring hole (201), so that the alloy liquid is filled into the anchor-shaped formwork (7), the alloy liquid submerges the crystal (601), the alloy liquid level is close to the anchor-shaped formwork (7), and the pouring hole (201) is closed;

and 4, step 4: keep the temperature of the constant temperature crucible (5)

Controlling the power of the heater (4) to ensure that the temperature in the constant-temperature crucible (5) can ensure that the alloy liquid is overheated;

and 5: upward pull anchor form mould (7)

And (3) opening the water cooling system, controlling the lifting rod (3) to lift the anchor-shaped mould shell (7) upwards at a constant speed, and gradually floating the anchor-shaped mould shell (7) out of the constant-temperature fluid (502) to dissipate part of heat on the liquid surface so as to generate a temperature gradient to force the alloy liquid contacting the daughter crystal (601) to directionally solidify downwards to form a single crystal until the anchor-shaped mould shell (7) is completely separated from the constant-temperature fluid (502) and the lifting is finished.

Technical Field

The invention belongs to the field of metal casting, and relates to a directional solidification device and a solidification method for high-temperature alloy.

Background

The high-temperature alloy is an important key Ni-based metal material applied to core components of gas turbines and aerospace engines, and can still maintain excellent physical and chemical properties such as good strength, rigidity, creep resistance, corrosion resistance and the like under a high-temperature service condition. Most of the conventional high-temperature alloys at present are deformation, solid solution, aging and powder high-temperature alloys, such as the typical Inconel718, which can maintain good comprehensive performance at 650 ℃.

However, at higher temperatures (e.g. modern aircraft engine turbine front combustor temperatures have exceeded 1400 degrees celsius, even though the temperature carried by the superalloy under the heat resistant coating and air cooling has approached its theoretical liquidus), grain boundary defects instead become a weak phase. Therefore, in order to further improve the high-temperature alloy adaptation conditions, a single crystal body with crystal boundary defects eliminated must be developed for service.

Besides alloying design, the solidification growth condition is generally controlled by a directional solidification method in the field, so that the condition that the high-temperature alloy with nucleation and growth in the solidification process grows from only 1 crystal grain is ensured, and the generation of crystal boundary defects is avoided. High temperature alloys such as CMSX-4, CMSX-6 and the like are designed by the means and have great success in the field of engines.

To accomplish this, a down draw process (bridgman process) has been developed in the art. The core design is that the ceramic mould shell with the upper opening and the lower opening is vertically arranged, and the lower opening of the mould shell is provided with a crystal and a chill; during casting, molten alloy liquid enters the formwork from the upper part of the formwork and contacts with the sub-crystals at the lower part, and then the whole body is slowly drawn downwards so that the formwork enters a cold zone, thereby establishing a cooling gradient from bottom to top and forcing the alloy liquid to directionally solidify upwards.

However, the yield of directional solidification to obtain a single crystal is not 100%. During the directional solidification process, the alloy still has defects such as freckles, mosaics and the like in the single crystal structure due to unknown and accidental factors, and contains mixed crystals with the orientation different from that of the main crystal grains. Although these structures do not occur with high probability throughout the product, the reliability of the part is not as expected since they carry additional grain boundary defects.

It is considered that the cause of defects such as stray crystals in this solidification process is generally related to the segregation solidification process inherent to the alloy due to an undesirable temperature field. The solidification process of high temperature alloys is promoted toward the liquid phase by the dendritic mushy interface, and when solidification proceeds to a certain extent, the dendritic arms of the dendrites become enriched with high melting point high density phases (e.g., W, Re) and contain low melting point low density phases in the inter-dendritic liquid phase region. When the bridgman method is used for downward drawing, the residual liquid phase above the liquid-solid interface can generate convection with the low-density liquid between the dendrites in the liquid-solid interface, so that the damage to the dendrites is caused, and the possibility of generating mixed crystals is increased.

Disclosure of Invention

In order to overcome the defects of the prior art, the invention aims to provide a high-temperature alloy directional solidification device, which aims to solve the technical problems of defects such as freckles in a crystal structure and the like caused by uneven heat dissipation of an anchor-shaped formwork, waste of crystals in a high-temperature alloy directional solidification process, high impurity crystal content in the high-temperature alloy directional solidification process and the like in the prior art.

In order to achieve the purpose, the invention adopts the following technical scheme to realize the purpose:

the invention provides a high-temperature alloy directional solidification device, which comprises a cabin body and two lifting rods, wherein a cabin cover is arranged above the cabin body, and the lifting rods penetrate through the cabin cover and extend into the cabin body; the cabin cover is also provided with a pouring hole;

the cabin body is internally provided with a heater, a constant temperature crucible, a water cooling system and an anchor-shaped mould shell, constant temperature fluid is filled in the constant temperature crucible, the heater is used for heating the constant temperature fluid, the anchor-shaped mould shell is arranged in the constant temperature crucible, a crystal is arranged above the anchor-shaped mould shell, the water cooling system is arranged above the crystal, a lifting rod is used for lifting the anchor-shaped mould shell and the water cooling system upwards at a constant speed, a pouring gate is arranged on the anchor-shaped mould shell, and the pouring gate is arranged opposite to a pouring hole in the cabin cover and is used for injecting alloy liquid into the anchor-shaped mould shell.

Preferably, the anchor form further comprises a thick neck, a pouring channel, alloy dies and a flow channel, the pouring channel is communicated below the pouring gate, the radial flow channel is communicated below the pouring channel, the flow channel comprises a plurality of branches, the end of each branch is communicated with 1 alloy die, the sub-crystals are arranged above the alloy dies, and the thick neck is arranged at the connecting position of the pouring gate and the pouring channel.

Preferably, the anchor form is alumina ceramic.

Preferably, the lifting rod is L-shaped, and the two lifting rods are clamped and fixed at the bottom end of the thick neck.

Preferably, the water cooling system comprises a chiller, a water cooling ring and a water cooling hose, the chiller is arranged above the hatch cover in a surrounding mode, the water cooling ring is located above the daughter crystal, the lower end of the water cooling hose is connected with the water cooling ring, and the upper end of the water cooling hose penetrates through the hatch cover and is communicated with the chiller.

Preferably, a heat resistance pad is also arranged between the inner bottom surface of the cabin body and the bottom wall of the constant temperature crucible.

Preferably, the surface of the constant-temperature fluid is paved with an insulating floating block, and the density of the insulating floating block is less than that of the constant-temperature fluid.

Preferably, the constant-temperature fluid is aluminum, copper or aluminum-copper alloy;

the heat insulation floating blocks are ceramic balls, ceramic tiles or irregular ceramic particles, and the size of the heat insulation floating blocks is 2-10 mm.

Preferably, the vacuum chamber further comprises an air passage which is positioned on the side wall of the chamber and used for vacuumizing the chamber.

The invention also discloses a solidification method of the high-temperature alloy directional solidification device, which comprises the following steps,

step 1: preparation phase

Installing a high-temperature alloy directional solidification device, and pouring constant-temperature fluid into a constant-temperature crucible to be submerged in the plane of the sub-crystals;

step 2: preheating constant temperature fluid

Turning on a heater to melt the constant-temperature fluid in the constant-temperature crucible into fluid;

and step 3: injecting alloy liquid

Injecting prepared superheated alloy liquid from the pouring hole, so that the alloy liquid is filled into the anchor-shaped formwork, the alloy liquid submerges the crystal and the alloy liquid plane is close to the anchor-shaped formwork, and closing the pouring hole;

and 4, step 4: make constant temperature crucible keep warm

Controlling the power of the heater to ensure that the temperature in the constant-temperature crucible can ensure that the alloy liquid is overheated;

and 5: upward pulling anchor form

And opening the water cooling system, controlling the lifting rod to lift the anchor-shaped mould shell upwards at a constant speed, and gradually floating the anchor-shaped mould shell to dissipate part of heat on the liquid surface so as to generate a temperature gradient to force the alloy liquid contacting the sub-crystals to directionally solidify downwards to form a single crystal until the anchor-shaped mould shell is completely separated from the constant-temperature fluid and the lifting is finished.

Compared with the prior art, the invention has the following beneficial effects:

the invention discloses a high-temperature alloy directional solidification device, which is characterized in that constant-temperature fluid is added into a constant-temperature crucible, a heater is arranged on the outer wall of the constant-temperature crucible, the heater is convenient for heating the constant-temperature fluid in the constant-temperature crucible, an anchor-shaped mould shell is arranged in the constant-temperature crucible, and the heated constant-temperature fluid can be filled in the outer wall of the anchor-shaped mould shell; a pouring hole is formed in the hatch cover, a pouring gate is formed in the anchor-shaped formwork, so that alloy liquid can be conveniently poured into the anchor-shaped formwork from the pouring hole, and the alloy liquid in the anchor-shaped formwork is heated by adopting constant-temperature fluid; the alloy liquid in the anchor mould shell is ensured to be always in an overheat state by controlling the power of the heater; and when the water cooling system is opened, the anchor-shaped mould shell and the water cooling system stably lift the anchor-shaped mould shell and the water cooling system upwards at a constant speed under the action of the two lifting rods, the anchor-shaped mould shell gradually floats out constant-temperature fluid to dissipate part of heat of the liquid level, so that a temperature gradient is generated, and alloy liquid contacting the sub-crystals is forced to directionally solidify downwards to form single crystals until the anchor-shaped mould shell is completely separated from the constant-temperature fluid and the lifting is finished. The high-temperature alloy directional solidification device provided by the invention has a simple structure, can realize the heat preservation or overheating state of the alloy through the heater, is simple to operate, can generate a temperature gradient by adopting a water cooling system, effectively solves the heat dissipation problem of an anchor-shaped formwork, avoids the defect problems of freckles and the like in a crystal tissue, and reduces the waste of crystals in the directional solidification process.

Furthermore, the lower part of the pouring gate is communicated with a pouring gate, the lower part of the pouring gate is communicated with a radial runner, the end parts of a plurality of branches of the runner are communicated with 1 alloy die, the heat dissipation of the anchor-shaped die shell is more uniform, the daughter crystal is arranged above the alloy die, alloy liquid is convenient to contact with the daughter crystal to form a monocrystal, a thick neck is arranged at the joint of the pouring gate and the pouring gate, the lifting rod is L-shaped, the lifting rod is clamped and fixed at the bottom end of the thick neck, the thick neck of the anchor-shaped die shell is designed to enhance the strength of the anchor-shaped die shell on one hand, the tendency that the anchor-shaped die shell is damaged during lifting is reduced, and on the other hand, the pouring gate can form a heat insulation effect to prevent the surrounding water cooling ring from solidifying the pouring gate in advance.

Furthermore, the chilling block is arranged above the hatch cover in a surrounding mode so as to be convenient to carry out alignment, the water cooling ring is located above the daughter crystal, the lower end of the water cooling hose is connected with the water cooling ring, the upper end of the water cooling hose penetrates through the hatch cover to be communicated with the chilling block, and the water cooling system can play a role in all parts needing cooling through the design.

Furthermore, the heat-resistant pad is positioned between the inner bottom surface of the cabin body and the constant-temperature crucible, so that the constant-temperature crucible can be prevented from directly contacting with the cabin body when the constant-temperature crucible is heated, the temperature in the cabin body is overhigh, and the anchor-shaped formwork is not beneficial to cooling.

Furthermore, the heat insulation floating block is positioned above the constant-temperature fluid, so that the phenomenon that the heat of the liquid constant-temperature fluid is dissipated too fast and alloy liquid in the anchor-shaped formwork cannot be heated fully can be avoided.

Furthermore, because the alumina ceramics has high hardness, excellent wear resistance and light weight, the anchor-shaped formwork is made of alumina ceramics.

Further, the air passage is positioned on the side wall of the cabin body, so that the cabin body can be vacuumized.

Furthermore, a switch is arranged at the pouring hole, so that the alloy liquid is favorably poured and sealed.

Further, the constant temperature fluid is aluminum, copper, or aluminum-copper alloy, because conventional heating can be performed only by heat radiation, the heat transfer power is low due to the particularity of radiation, the uniformity of constant temperature is not good, and the temperature control is not facilitated. The metal liquid constant temperature control means is used, due to the high heat conduction characteristic of the metal fluid, the temperature field can be guaranteed to be almost ideal and uniform, the heat transfer efficiency of metal is high, the temperature control is more effective and sensitive, and the temperature and heating almost have no delay, but due to the fact that the heat exchange coefficient of the metal liquid for external heat dissipation is large, in order to prevent heat loss, irregular heat-resistant materials with density smaller than that of the metal are used as heat-insulating floating blocks, the heat-insulating floating blocks are ceramic balls, ceramic tiles or irregular ceramic particles, the size of the heat-insulating floating blocks is 2-10mm, heat loss can be effectively avoided, and the purposes of energy conservation and heat preservation are achieved.

The invention also discloses a solidification method of the high-temperature alloy directional solidification device, and the method can enable the anchor-shaped formwork to generate temperature gradient only through the water cooling system, thereby effectively solving the heat dissipation problem of the anchor-shaped formwork.

Drawings

FIG. 1 is a schematic view of a superalloy directional solidification apparatus of the present invention;

FIG. 2 is a schematic view of an anchor-shaped mold shell structure of the superalloy directional solidification apparatus of the present invention;

FIG. 3 is a layout of a water cooling ring and an alloy mold of the superalloy directional solidification device of the present invention;

FIG. 4 is a schematic flow diagram of the superalloy directional solidification method of the present invention; wherein, (a) is not injected with alloy liquid; (b) for injecting the alloy liquid; (c) is pulled upwards; (d) the solidification is completed for complete pulling.

Wherein: 1-a cabin body; 101-the airway; 2-a hatch cover; 201-pouring a hole; 202-chilling block; 3-lifting the pull rod; 4-a heater; 5-constant temperature crucible; 501-heat resistance pad; 502-constant temperature fluid; 503-heat insulation floating block; 6-water cooling ring; 601-daughter crystal; 602-a water-cooled hose; 7-anchor form shells; 701-thick neck; 702-a gate; 703-pouring channel; 704-alloy die; 705-flow channel.

Detailed Description

In order to make the technical solutions of the present invention better understood, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

It should be noted that the terms "first," "second," and the like in the description and claims of the present invention and in the drawings described above are used for distinguishing between similar elements and not necessarily for describing a particular sequential or chronological order. It is to be understood that the data so used is interchangeable under appropriate circumstances such that the embodiments of the invention described herein are capable of operation in sequences other than those illustrated or described herein. Furthermore, the terms "comprises," "comprising," and "having," and any variations thereof, are intended to cover a non-exclusive inclusion, such that a process, method, system, article, or apparatus that comprises a list of steps or elements is not necessarily limited to those steps or elements expressly listed, but may include other steps or elements not expressly listed or inherent to such process, method, article, or apparatus.

The invention is described in further detail below with reference to the accompanying drawings:

referring to fig. 1, a high-temperature alloy directional solidification device comprises a cabin body 1, a cabin cover 2, two lifting rods 3, a heater 4, a constant-temperature crucible 5, a heat-resistant pad 501, constant-temperature fluid 502, a heat-insulating floating block 503, a water cooling system, a crystal 601 and an anchor-shaped formwork 7; the water cooling system comprises a water cooling ring 6, a chiller 201 and a water cooling hose 602; an air passage 101 with a valve is arranged on the side wall of the cabin body 1 and is communicated with external vacuum equipment; the hatch cover 2 is positioned on the cabin body 1, and the center of the hatch cover 2 also comprises a vertically through openable pouring hole 201 to facilitate the pouring and sealing of alloy liquid; the cabin cover 2 is also provided with a chiller 202 communicated with water cooling relative to the outer side of the cabin body 1, and the chiller 202 is arranged above the cabin cover 2 in a surrounding manner; the constant temperature crucible 5 is fixedly arranged on the bottom of the inner part of the cabin body 1 through heat resistance pads 501 at intervals, constant temperature fluid 502 is also arranged in the constant temperature crucible 5, and a heat insulation floating block 503 is also arranged on the constant temperature fluid 502; the heater 4 is further installed on the outer wall of the constant-temperature crucible 5, so that when the constant-temperature crucible is designed, the constant-temperature fluid 502 in the constant-temperature crucible 5 can be heated to be in a liquid state through heating, and the heat insulation floating block 503 with the density smaller than that of the constant-temperature fluid 502 is suspended on the constant-temperature fluid to reduce heat loss, so that the constant-temperature effect is improved.

Referring to fig. 2, the anchor mold shell 7 comprises a thick neck 701, a gate 702, a pouring gate 703, an alloy mold 704 and a runner 705, the gate 702 is arranged at the upper part of the anchor mold shell 7, the pouring gate 703 is communicated with the lower part of the gate 702, the runner 703 is communicated with a radial runner 705, the runner 705 comprises a plurality of branches, the end parts of the branches of the runner 705 are communicated with 1 alloy mold 704, the upper end of the alloy mold 704 is provided with an opening and is provided with a crystal 601, and the thickened part at the connection part of the gate 702 and the pouring gate 703 is the thick neck 701, so that the alloy liquid can enter the crystal 601 contacting the upper part from the lower part of the alloy mold 704 after being flushed from the gate 702, and solidification can occur at the upper part.

Preferably, the alloy dies 704 communicated with the anchor form 7 can be 4 alloy dies 704 shown in fig. 3(a) or 6 alloy dies 704 shown in fig. 3(b), so that the heat dissipation of the anchor form is more uniform.

The upper part of the sub-crystal 601 is further provided with a water-cooling ring 6, the water-cooling ring 6 surrounds the sprue 702 and keeps an equal gap between the sprue and the sprue, one side of the water-cooling ring 6 is further connected with a water-cooling hose 602, and the other end of the water-cooling hose 602 penetrates through the hatch cover 2 and is connected to the chiller 202.

The lower end of an L-shaped lifting rod 3 is clamped at the thick neck 701 of the anchor-shaped formwork 7, the main body of the lifting rod 3 is vertically arranged to penetrate through the hatch cover 2 upwards, an electric device controls the upper part and the lower part of the lifting rod to be vertical, and the anchor-shaped formwork 7 can be vertically lifted upwards by the lifting rod 3; the design of the thick neck 701 of the anchor mold shell 7 can enhance the strength of the anchor mold shell 7, reduce the tendency of the anchor mold shell 7 to be damaged during lifting, and form a heat insulation effect at the pouring gate 702 to prevent the surrounding water cooling ring 6 from solidifying the pouring gate 702 in advance.

FIG. 4 is a schematic view of the directional solidification method of the superalloy of the present invention, wherein FIG. 4(a) is a schematic view of no molten alloy injection; FIG. 4(b) is a schematic view of the alloy liquid injection; FIG. 4(c) is a schematic view of the anchor form 7 and the water cooling system being pulled upward; FIG. 4(d) is a schematic view of complete lifting and completion of solidification. The invention also provides a solidification method of the high-temperature alloy directional solidification device, which comprises the following steps:

step 1 preparation:

according to the directional solidification single crystal superalloy device, all the elements are arranged at the positions set in the description; pouring a solid constant-temperature fluid 502 into a constant-temperature crucible 5, ensuring that a sufficient amount of heat insulation floating blocks 503 covering the surface are arranged on the constant-temperature fluid 502, ensuring that an anchor-shaped mold shell 7 with a crystal 601 arranged and connected with a water-cooling ring 6 is coaxial with a pouring hole 201 and a pouring gate 702 so that the pouring hole 201 is opposite to the pouring gate 702, and injecting alloy liquid into the anchor-shaped mold shell 7; the constant temperature fluid 502 must be submerged in the plane of the daughter crystal 601;

step 2, preheating and vacuum:

opening an air passage 101, vacuumizing the cabin body 1, after the vacuum is achieved, opening a heater 4 to melt a constant-temperature fluid 502 in a constant-temperature crucible 5 to form a fluid, enabling a heat insulation floating block 503 to float on the surface of the fluid, then closing the air passage 101, and closing the vacuum;

step 3, injecting alloy liquid:

injecting prepared superheated alloy liquid from the pouring hole 201, so that the alloy liquid is completely filled into the anchor mould shell 7, and the alloy liquid level is close to the thick neck 701 and passes through the crystal 601, and then closing the pouring hole 201;

step 4, heat preservation:

the power of the heater 4 is controlled, so that the temperature in the constant temperature crucible 5 is kept to be certain overheat relative to the alloy liquid;

step 5, upward pulling and solidifying:

opening a water cooling system to enable the chilling block 202 and the water cooling ring 6 to form a cold area, controlling the lifting rod 3 to lift the anchor-shaped formwork 7 (including the daughter crystals 601 and the water cooling ring 6 fixed on the anchor-shaped formwork) upwards at a constant speed, and enabling the anchor-shaped formwork 7 to gradually float out of the constant-temperature fluid 502 to enable the part on the liquid level to lose heat, so that a temperature gradient is generated, and alloy liquid contacting the daughter crystals 601 is forced to be directionally solidified downwards to form a single crystal; this process continues until all anchor molds 7 have pulled out the constant temperature fluid 502.

Example 1:

the CMSX-4 alloy is selected as an experimental material, an aluminum block is selected as a constant-temperature fluid 502, an alumina ceramic plate (10mm) is selected as a heat insulation floating block 503, an alumina ceramic anchor-shaped formwork 7 is selected, the arrangement of 4 alloy dies 704 is selected, the constant-temperature fluid 502 is kept at 1450 ℃, the casting temperature of alloy liquid is 1500 ℃, after the alloy liquid is completely filled, the upward pulling speed is controlled to be 1mm/min for upward solidification, and experiments show that a small amount of mixed crystals are found in single crystal samples in the 4 alloy dies 704.

Example 2:

the CMSX-4 alloy is selected as an experimental material, an aluminum block is selected as a constant-temperature fluid 502, an alumina ceramic ball (10mm) is selected as a heat insulation floating block 503, an alumina ceramic anchor-shaped formwork 7 is selected, 6 alloy dies 704 are arranged, the constant-temperature fluid 502 is kept at 1500 ℃, the casting temperature of alloy liquid is 1500 ℃, after the alloy liquid is completely filled, the upward pulling speed is controlled to be 2mm/min for upward solidification, and experiments show that only a small amount of mixed crystals are found in single crystal samples in 1 alloy die 704.

Example 3:

the CMSX-4 alloy is selected as an experimental material, a copper block is selected as a constant-temperature fluid 502, an alumina ceramic sheet (5mm) is selected as a heat insulation floating block 503, an alumina ceramic anchor-shaped formwork 7 is selected, 4 alloy molds 704 are arranged, the constant-temperature fluid 502 is kept at 1500 ℃, the casting temperature of alloy liquid is 1550 ℃, after the alloy liquid is completely filled, the upward pulling speed is controlled to be 3mm/min for upward solidification, and experiments show that no mixed crystal is found.

The above-mentioned contents are only for illustrating the technical idea of the present invention, and the protection scope of the present invention is not limited thereby, and any modification made on the basis of the technical idea of the present invention falls within the protection scope of the claims of the present invention.