Construction process of water-soluble pressure-sensitive adhesive

文档序号:1350350 发布日期:2020-07-24 浏览:34次 中文

阅读说明:本技术 一种水溶性压敏胶的施工工艺 (Construction process of water-soluble pressure-sensitive adhesive ) 是由 陈家路 陈彦会 陈家坤 李洪夫 陈世烛 王伯学 于 2020-06-01 设计创作,主要内容包括:本发明公开了一种水溶性压敏胶的施工工艺,水溶性压敏胶组分按重量份数包括醋酸乙烯-N-正丁氧基甲基丙烯酰胺丁酯共聚体20-30份、苯乙烯-丁二烯-苯乙烯嵌段共聚物15-30份、过氧化苯甲酰10-20份、石油树脂15-25份、萜烯树脂10-30份、抗氧剂4-10份、纳米二氧化硅2-6份、碳酸钙4-10份、活性白土4-10份,本发明制备工艺简单,得到的压敏胶具有耐磨、抗老化性能,粘性好、粘结强度高、密封性能和耐久性能好,具有耐高温、良好的抗冲击性,防震缓冲效果好的优点。(The invention discloses a construction process of a water-soluble pressure-sensitive adhesive, which comprises 20-30 parts of vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, 15-30 parts of styrene-butadiene-styrene block copolymer, 10-20 parts of benzoyl peroxide, 15-25 parts of petroleum resin, 10-30 parts of terpene resin, 4-10 parts of antioxidant, 2-6 parts of nano silicon dioxide, 4-10 parts of calcium carbonate and 4-10 parts of activated clay by weight.)

1. A water-soluble pressure-sensitive adhesive is characterized in that: the water-soluble pressure-sensitive adhesive comprises, by weight, 20-30 parts of vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, 15-30 parts of styrene-butadiene-styrene block copolymer, 10-20 parts of benzoyl peroxide, 15-25 parts of petroleum resin, 10-30 parts of terpene resin, 4-10 parts of antioxidant, 2-6 parts of nano silicon dioxide, 4-10 parts of calcium carbonate and 4-10 parts of activated clay.

2. The water-soluble pressure-sensitive adhesive according to claim 1, wherein: the preferable component proportion of the water-soluble pressure-sensitive adhesive component comprises 25 parts of vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, 22 parts of styrene-butadiene-styrene block copolymer, 15 parts of benzoyl peroxide, 20 parts of petroleum resin, 20 parts of terpene resin, 7 parts of antioxidant, 4 parts of nano silicon dioxide, 7 parts of calcium carbonate and 7 parts of activated clay.

3. The construction process for realizing the water-soluble pressure-sensitive adhesive of claim 1 is characterized in that: the construction process comprises the following steps:

A. firstly, mixing vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, styrene-butadiene-styrene block copolymer, benzoyl peroxide, petroleum resin and terpene resin, adding the mixture into a stirring kettle, and stirring at the stirring speed of 1000-2000 rpm for 20-30 min to obtain a mixture A;

B. mixing an antioxidant, nano silicon dioxide, calcium carbonate and activated clay, and adding the mixture into a ball mill for ball milling to obtain a mixture B;

C. and fully mixing the mixture A and the mixture B, putting the mixture A and the mixture B into a water bath, stirring the mixture B in the water bath at the temperature of 15-20 ℃ and the stirring speed of 800-.

4. The construction process of the water-soluble pressure-sensitive adhesive according to claim 3, wherein: and C, adopting cooling circulating water as water in the water bath kettle in the step C.

Technical Field

The invention relates to the technical field of water-soluble pressure-sensitive adhesive construction, in particular to a construction process of a water-soluble pressure-sensitive adhesive.

Background

Pressure-sensitive adhesives are short for pressure-sensitive adhesives. Is a type of adhesive that is sensitive to pressure. The preparation method is mainly used for preparing the pressure-sensitive adhesive tape. The pressure-sensitive adhesive must have a higher adhesive force (the peeling force exhibited after the pressure-sensitive adhesive tape is pressure-adhered to the adherend surface) than cohesive force (i.e., so-called sticky feeling exhibited when the adhesive tape is lightly touched with a finger). It can be classified into rubber type and resin type according to its main component. Besides the main components, other auxiliary components such as tackifying resin, plasticizer, filler, viscosity regulator, vulcanizing agent, anti-aging agent, solvent and the like are added to prepare the adhesive. The existing preparation process of the water-soluble pressure-sensitive adhesive is complex and needs to be improved.

Disclosure of Invention

The invention aims to provide a construction process of a water-soluble pressure-sensitive adhesive, which aims to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme: the water-soluble pressure-sensitive adhesive comprises, by weight, 20-30 parts of vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, 15-30 parts of styrene-butadiene-styrene block copolymer, 10-20 parts of benzoyl peroxide, 15-25 parts of petroleum resin, 10-30 parts of terpene resin, 4-10 parts of antioxidant, 2-6 parts of nano silicon dioxide, 4-10 parts of calcium carbonate and 4-10 parts of activated clay.

Preferably, the water-soluble pressure-sensitive adhesive component preferably comprises 25 parts of vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, 22 parts of styrene-butadiene-styrene block copolymer, 15 parts of benzoyl peroxide, 20 parts of petroleum resin, 20 parts of terpene resin, 7 parts of antioxidant, 4 parts of nano silicon dioxide, 7 parts of calcium carbonate and 7 parts of activated clay.

Preferably, the construction process comprises the following steps:

A. firstly, mixing vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, styrene-butadiene-styrene block copolymer, benzoyl peroxide, petroleum resin and terpene resin, adding the mixture into a stirring kettle, and stirring at the stirring speed of 1000-2000 rpm for 20-30 min to obtain a mixture A;

B. mixing an antioxidant, nano silicon dioxide, calcium carbonate and activated clay, and adding the mixture into a ball mill for ball milling to obtain a mixture B;

C. and fully mixing the mixture A and the mixture B, putting the mixture A and the mixture B into a water bath, stirring the mixture B in the water bath at the temperature of 15-20 ℃ and the stirring speed of 800-.

Preferably, the water in the water bath kettle in the step C is cooling circulating water.

Compared with the prior art, the invention has the beneficial effects that: the preparation process is simple, and the obtained pressure-sensitive adhesive has the advantages of wear resistance, ageing resistance, good viscosity, high bonding strength, good sealing performance and durability, high temperature resistance, good impact resistance and good shockproof buffer effect.

Detailed Description

The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention provides the following technical scheme: the water-soluble pressure-sensitive adhesive comprises, by weight, 20-30 parts of vinyl acetate-N-N-butoxy methyl acrylamide butyl ester copolymer, 15-30 parts of styrene-butadiene-styrene block copolymer, 10-20 parts of benzoyl peroxide, 15-25 parts of petroleum resin, 10-30 parts of terpene resin, 4-10 parts of antioxidant, 2-6 parts of nano silicon dioxide, 4-10 parts of calcium carbonate and 4-10 parts of activated clay.

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