Pesticide suspending agent and preparation method thereof

文档序号:1866939 发布日期:2021-11-23 浏览:34次 中文

阅读说明:本技术 一种农药悬浮剂及其制备方法 (Pesticide suspending agent and preparation method thereof ) 是由 焦清清 李桂福 王成龙 于 2021-09-03 设计创作,主要内容包括:本发明公开了一种农药悬浮剂及其制备方法,组分比为:悬浮剂原药为:51-90%;环保溶剂5%-10%;表面活性剂2%-10%;稳定剂2%-15%;其余为水。其中悬浮剂原药有效成分为:20-60%双亲油基改性双酚A型环氧树脂;15-40%十二烷基苯磺酸三乙醇胺;15-30%苯乙基苯酚聚氧乙烯醚;9-20%烷基糖苷。本发明的优点是:提供一种农药悬浮剂及其制备方法,该农药悬浮剂配方简易,制备方法简单,该制剂性能稳定,易降解,对农作物害虫持效期长高,对环境污染很小。(The invention discloses a pesticide suspending agent and a preparation method thereof, and the pesticide suspending agent comprises the following components in percentage by weight: the suspending agent comprises the following raw materials: 51-90%; 5% -10% of an environment-friendly solvent; 2% -10% of a surfactant; 2% -15% of a stabilizer; the balance of water. The suspending agent comprises the following active ingredients: 20-60% of amphiphilic oil-based modified bisphenol A epoxy resin; 15-40% of triethanolamine dodecylbenzene sulfonate; 15-30% of phenethylphenol polyoxyethylene ether; 9-20% of alkyl glycoside. The invention has the advantages that: the pesticide suspending agent has the advantages of simple formula, simple preparation method, stable performance, easy degradation, long lasting period for crop pests and little environmental pollution.)

1. A pesticide suspending agent is characterized by comprising the following components in percentage by weight:

the suspending agent comprises the following raw materials: 51-90%;

5% -10% of an environment-friendly solvent;

2% -10% of a surfactant;

2% -15% of a stabilizer;

the balance of water.

2. A pesticidal suspension according to claim 1 characterized in that:

the suspending agent comprises the following active ingredients:

20-60% of amphiphilic oil-based modified bisphenol A epoxy resin;

15-40% of triethanolamine dodecylbenzene sulfonate;

15-30% of phenethylphenol polyoxyethylene ether;

9-20% of alkyl glycoside.

3. A pesticidal suspension according to claim 1 characterized in that:

wherein the environment-friendly solvent is one or the combination of more than two of ethanol, normal propyl alcohol, isopropanol, butanol, isobutanol and N-methylpyrrolidone.

4. A pesticidal suspension according to claim 1 characterized in that:

wherein the surfactant is a combination of two or more of sodium lignosulphonate, sodium dodecyl sulfonate, sodium dodecyl sulfate, sodium laureth sulfate, sorbitan fatty acid ester, alkylaryl phenol polyoxyethylene ether phosphate and sodium di-sec-octyl maleate sulfonate.

5. A pesticidal suspension according to claim 1 characterized in that:

wherein the stabilizer is one or two of hydrochloric acid, sulfuric acid, acetic acid, urea, polyethylene glycol, phosphoric acid, ethylene glycol and glycerol.

6. The method for preparing a pesticide suspension concentrate as claimed in claim 1, characterized by the following method steps:

(1) accurately weighing the original medicine, fully and uniformly dissolving the original medicine by using a proper amount of solvent, adding an emulsifier, and uniformly mixing for later use;

(2) adding an environment-friendly solvent under the condition of stirring in the step 1;

(3) adding a surfactant under the stirring condition in the step 2;

(4) adding a stabilizer under the stirring condition in the step 3;

(5) and (4) under the condition of stirring in the step (4), supplementing deionized water to 100%, and cooling at normal temperature to obtain a finished product.

Technical Field

The invention belongs to the technical field of processing of suspending agents, and particularly relates to a pesticide suspending agent and a preparation method thereof.

Background

The suspending agent, the international code of which is SC, is a silk-sticky flowable suspension which is prepared by mixing an original pesticide, a carrier and a dispersing agent and carrying out superfine grinding by a wet method. The liquid-solid system is formed by dispersing solid raw medicine which is insoluble or slightly soluble in water uniformly through superfine grinding by means of certain auxiliary agents. The suspending agent is generally composed of active ingredients, a dispersing agent, a thickening agent, an anti-settling agent, an antifoaming agent, an antifreezing agent, water and the like. The content of the effective components is generally 5 to 50 percent. The average particle size is typically around 3 microns. Is a new formulation for processing pesticides. The existing suspending agent has complex formula, complex processing process flow, incapability of continuous production and low production rate.

Disclosure of Invention

The invention aims to provide a pesticide suspending agent and a preparation method thereof, the pesticide suspending agent and the preparation method thereof can overcome the content in the background technology, a simple formula is provided, the processing technology can realize continuous production, and the production rate is high.

The technical scheme adopted by the invention is as follows: a pesticide suspending agent is characterized by comprising the following components in percentage by weight:

the suspending agent comprises the following raw materials: 51-90%;

5% -10% of an environment-friendly solvent;

2% -10% of a surfactant;

2% -15% of a stabilizer;

the balance of water.

The suspending agent comprises the following active ingredients:

20-60% of amphiphilic oil-based modified bisphenol A epoxy resin;

15-40% of triethanolamine dodecylbenzene sulfonate;

15-30% of phenethylphenol polyoxyethylene ether;

9-20% of alkyl glycoside.

Wherein the environment-friendly solvent is one or the combination of more than two of ethanol, normal propyl alcohol, isopropanol, butanol, isobutanol and N-methylpyrrolidone.

Wherein the surfactant is a combination of two or more of sodium lignosulphonate, sodium dodecyl sulfonate, sodium dodecyl sulfate, sodium laureth sulfate, sorbitan fatty acid ester, alkylaryl phenol polyoxyethylene ether phosphate and sodium di-sec-octyl maleate sulfonate.

Wherein the stabilizer is one or two of hydrochloric acid, sulfuric acid, acetic acid, urea, polyethylene glycol, phosphoric acid, ethylene glycol and glycerol.

The other technical scheme of the invention is as follows: a preparation method of a pesticide suspending agent is characterized by comprising the following steps:

1. accurately weighing the original medicine, fully and uniformly dissolving the original medicine by using a proper amount of solvent, adding an emulsifier, and uniformly mixing for later use;

2. adding an environment-friendly solvent under the condition of stirring in the step 1;

3. adding a surfactant under the stirring condition in the step 2;

4. adding a stabilizer under the stirring condition in the step 3;

5. and (4) under the condition of stirring in the step (4), supplementing deionized water to 100%, and cooling at normal temperature to obtain a finished product.

The invention has the advantages that: the pesticide suspending agent has the advantages of simple formula, simple preparation method, stable performance, easy degradation, long lasting period for crop pests and little environmental pollution.

Detailed Description

The technical scheme adopted by the invention is operated and implemented in such a way.

Example 1:

a pesticide suspending agent is characterized by comprising the following components in percentage by weight:

the suspending agent comprises the following raw materials: 51 percent;

10% of an environment-friendly solvent;

10% of a surfactant;

15% of a stabilizer;

the balance is 14 percent of deionized water.

The suspending agent comprises the following active ingredients:

20% of amphiphilic oil-based modified bisphenol A epoxy resin;

40% triethanolamine dodecylbenzene sulfonate;

30% phenethylphenol polyoxyethylene ether;

10% alkyl glycoside.

Example 2:

a pesticide suspending agent is characterized by comprising the following components in percentage by weight:

the suspending agent comprises the following raw materials: 60 percent;

9% of an environment-friendly solvent;

9% of a surfactant;

12% of a stabilizer;

the balance is 10 percent of deionized water.

The suspending agent comprises the following active ingredients: 30% of amphiphilic oil-based modified bisphenol A epoxy resin; 30% triethanolamine dodecylbenzene sulfonate;

25% phenethylphenol polyoxyethylene ether; 15% alkyl glycoside.

Example 3:

a pesticide suspending agent is characterized by comprising the following components in percentage by weight:

the suspending agent comprises the following raw materials: 70 percent;

7% of an environment-friendly solvent;

7% of a surfactant;

9% of a stabilizer;

the balance is 7 percent of deionized water.

The suspending agent comprises the following active ingredients: 50% of amphiphilic oil-based modified bisphenol A epoxy resin; 20% triethanolamine dodecylbenzene sulfonate;

20% phenethylphenol polyoxyethylene ether; 10% alkyl glycoside.

Example 3:

a pesticide suspending agent is characterized by comprising the following components in percentage by weight:

the suspending agent comprises the following raw materials: 80 percent;

5% of an environment-friendly solvent;

6% of a surfactant;

4% of a stabilizer;

the balance is 5 percent of deionized water.

The suspending agent comprises the following active ingredients: 60% of amphiphilic oil-based modified bisphenol A epoxy resin; 15% triethanolamine dodecylbenzene sulfonate; 15% phenethylphenol polyoxyethylene ether;

10% alkyl glycoside.

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