阅读说明：本技术 一种土霉素的制备装置和方法 (Preparation device and method of oxytetracycline ) 是由 梁峙 张明胜 张猛 于 2019-08-01 设计创作，主要内容包括：本发明公开了一种土霉素的制备装置和方法,其中所述出渣控制阀包括：控制阀壳体、阀门弹簧、阀门板、阀门驱动臂、旋转臂、控制阀电机、齿轮A、齿轮B；所述阀门板位于控制阀壳体内部,阀门板的数量为2个,相邻阀门板之间固定连接有阀门弹簧；所述阀门弹簧数量为6个、等距离分布、不锈钢材质,阀门弹簧控制出渣控制阀弹性闭合,并能甩掉异物,实现出渣控制阀正常开闭功能；所述阀门驱动臂的一端通过支杆与阀门板固定连接,阀门驱动臂的另一端通过转动轴与旋转臂转动连接,其中旋转臂设在阀门驱动臂上部。本发明所述的一种土霉素的制备装置和方法,该装置采用自动控制,操作简单方便,工作效率高,具体有较强的稳定性。(The invention discloses a preparation device and a preparation method of oxytetracycline, wherein a slag discharge control valve comprises: the control valve comprises a control valve shell, a valve spring, a valve plate, a valve driving arm, a rotating arm, a control valve motor, a gear A and a gear B; the valve plates are positioned inside the control valve shell, the number of the valve plates is 2, and valve springs are fixedly connected between adjacent valve plates; the number of the valve springs is 6, the valve springs are distributed at equal intervals and made of stainless steel, the valve springs control the slag discharge control valve to be elastically closed, foreign matters can be thrown away, and the normal opening and closing functions of the slag discharge control valve are realized; one end of the valve driving arm is fixedly connected with the valve plate through a support rod, the other end of the valve driving arm is rotatably connected with a rotating arm through a rotating shaft, and the rotating arm is arranged at the upper part of the valve driving arm. The preparation device and the preparation method of the oxytetracycline have the advantages of automatic control, simple and convenient operation, high working efficiency and strong stability.)

1. A preparation facilities of oxytetracycline includes: the device comprises a dissolving tank (1), a delivery pump (2), a blending tank (3), a distillation tower input pump (4), a distillation tower (5), a trickle bed reactor (6), a precipitate discharge pipe (7), a sampling exhaust pipe (8), a high-level discharge pipe (9), a gas-liquid separator (10), an electric cabinet (11), an inoculation sampling return pipe (12), a main fermentation box (13), a bracket (14) and an adjusting wheel (15); the device is characterized in that the dissolving tank (1) positioned on one side is communicated with a main fermentation box (13) positioned on the upper left part through a delivery pump (2), and the top of the main fermentation box (13) is of a controllable opening and closing structure; the lower part of the main fermentation box (13) is provided with a blending tank (3), one side of the upper part is provided with an inoculation sampling return pipe (12) which is communicated with the main fermentation box and the inoculation sampling return pipe, wherein the inoculation sampling return pipe (12) is used for inoculation and sampling, and returns discharged water into the dissolving tank (1); an electric cabinet (11) is arranged at the upper part of the bracket (14); a distillation tower (5) is arranged on one side of the support (14), the distillation tower (5) is vertically arranged, the bottom of the distillation tower (5) is communicated with external steam, the distillation tower (5) is of a hollow structure, the shell of the distillation tower (5) is made of high polymer materials, the distillation tower (5) is communicated with a main fermentation box (13) through a distillation tower input pump (4), and the distillation tower (5) is communicated with a gas-liquid separator (10) on the upper part; the trickle bed reactor (6) is respectively communicated with the gas-liquid separator (10) and the distillation tower (5) in a gas-liquid parallel flow mode; a sediment discharge pipe (7) is arranged at the lower part of the trickle bed reactor (6), a high-level discharge pipe (9) is arranged at the upper part of the trickle bed reactor, a sampling exhaust pipe (8) is arranged at the waist part of the trickle bed reactor, and the trickle bed reactor (6) is communicated with the trickle bed reactor, the high-level discharge pipe and the sampling exhaust pipe; the regulating wheels (15) are positioned at the bottom of the distillation tower (5), and the number of the regulating wheels is four; the delivery pump (2) and the distillation tower input pump (4) are in control connection with an electric cabinet (11) through wires;

the distillation tower (5) is provided with a slag tapping control valve (5-2); the slag control valve (5-2) is positioned at the lower part of the lower connecting flange (5-4-2);

the tapping control valve (5-2) comprises: the control valve comprises a control valve shell (5-2-2), a valve spring (5-2-3), a valve plate (5-2-4), a valve driving arm (5-2-5), a rotating arm (5-2-6), a control valve motor (5-2-7), a gear A (5-2-8) and a gear B (5-2-9); the valve plates (5-2-4) are positioned inside the control valve shell (5-2-2), the number of the valve plates (5-2-4) is 2, and valve springs (5-2-3) are fixedly connected between adjacent valve plates (5-2-4); the number of the valve springs (5-2-3) is 6, the valve springs are distributed at equal intervals and made of stainless steel, the valve springs (5-2-3) control the slag control valve (5-2) to be elastically closed, foreign matters can be thrown away, and the normal opening and closing functions of the slag control valve (5-2) are realized; one end of the valve driving arm (5-2-5) is fixedly connected with the valve plate (5-2-4) through a support rod, the other end of the valve driving arm (5-2-5) is rotatably connected with the rotating arm (5-2-6) through a rotating shaft, and the rotating arm (5-2-6) is arranged at the upper part of the valve driving arm (5-2-5); the gear B (5-2-9) is rotationally connected with the rotating arm (5-2-6); one side of the gear B (5-2-9) is provided with a gear A (5-2-8) which is meshed and connected with the gear B; the control valve motor (5-2-7) is positioned on one side of the gear A (5-2-8) and is in transmission connection with the gear A, and the control valve motor (5-2-7) is in control connection with the electric cabinet (11) through a wire.

2. The oxytetracycline preparation device according to claim 1, characterized in that said distillation column (5) comprises: a slag outlet (5-1), a slag control valve (5-2), a distillation tower shell (5-3), a catalytic system (5-4), a liquid outlet pipe (5-5), a gas outlet pipe (5-6), a liquid inlet (5-7) and a steam pipe (5-8); the lower part of the distillation tower (5) is provided with a slag outlet (5-1) which is communicated with the distillation tower through a slag outlet control valve (5-2); a catalytic system (5-4) is arranged at the upper part of the slag control valve (5-2) and inside the distillation tower shell (5-3); a steam pipe (5-8) is arranged on one side of the distillation tower shell (5-3), a liquid outlet pipe (5-5) is arranged on the other side of the distillation tower shell, a liquid inlet (5-7) is arranged at the waist part of the distillation tower shell, an air outlet pipe (5-6) is arranged at the top of the distillation tower shell, and the distillation tower shell (5-3) is communicated with the four distillation tower shells;

the catalytic system (5-4) comprises: the device comprises a slag control valve (5-2), a lower connecting flange (5-4-2), a hot mixing chamber (5-4-3), a catalytic shell (5-4-4), a vaporization concentration sensor (5-4-5), a vaporization chamber (5-4-6), an upper connecting flange (5-4-7), catalytic reaction fillers (5-4-8), a net contacting tower plate (5-4-9), an accelerator spray ring (5-4-10) and a heat collecting hopper (5-4-11); the lower connecting flange (5-4-2) is positioned at the lower part of the whole catalytic system (5-4), the upper part of the lower connecting flange is provided with a vaporizing chamber (5-4-6) and an upper connecting flange (5-4-7), and the vaporizing chamber (5-4-6) is communicated with the upper connecting flange (5-4-7) and fixedly connected with the catalytic shell (5-4-4); the upper end and the lower end of the catalytic shell (5-4-4) are respectively fixedly connected with an upper connecting flange (5-4-7) and a lower connecting flange (5-4-2), wherein the lower connecting flange (5-4-2) is positioned at the lower part of the catalytic shell (5-4-4); the hot mixing chamber (5-4-3) is arranged in the catalytic shell (5-4-4) and above the slag control valve (5-2), the hot mixing chamber (5-4-3) is of a cylindrical hollow structure which is communicated up and down, and hot steam and mixed liquid are fully mixed in the hot mixing chamber; the other end of the hot mixing chamber (5-4-3) is communicated with a slag control valve (5-2) through a lower connecting flange (5-4-2), wherein the slag control valve (5-2) is positioned at the lower part of the lower connecting flange (5-4-2); the heat collecting hopper (5-4-11) is positioned at the upper part of the heat mixing chamber (5-4-3) and is communicated with the heat mixing chamber, the heat collecting hopper (5-4-11) is in a horn shape, is communicated from top to bottom, is small at the bottom and large at the top, is provided with a large number of through holes on the surface, is provided with a guide plate at the waist, and utilizes the horn shape to carry out sufficient heat exchange on hot steam and solution splashed by the screen contacting tower plate (5-4-9); the catalytic reaction fillers (5-4-8), the net contacting tower plates (5-4-9) and the promoter spraying rings (5-4-10) are arranged at the upper parts of the heat gathering hoppers (5-4-11), wherein the number of the catalytic reaction fillers (5-4-8) is 3, and the adjacent catalytic reaction fillers (5-4-8) are distributed at equal intervals; the surface of the net contacting tower plate (5-4-9) is provided with a large number of through holes, the number of the through holes is 20, and the through holes are equidistantly distributed in the catalytic shell (5-4-4); the promoter spray ring (5-4-10) sprays and adds the promoter into the catalytic shell (5-4-4); the accelerator spray ring (5-4-10), the catalytic reaction filler (5-4-8) and the net contacting tower plate (5-4-9) are used for accelerating the mixed liquor to carry out chemical reaction; the vaporization concentration sensor (5-4-5) is arranged at the waist of the catalytic shell (5-4-4), and the vaporization concentration sensor (5-4-5) is in control connection with the electric cabinet (11) through a wire;

the trickle-bed reactor (6) comprises: the device comprises a cleaning and spraying device (6-1), a catalyst adding pipe (6-2), a mixing stirrer (6-3), a stirring motor (6-4), an automatic cleaning machine (6-5) and a corrugation generator (6-6); one end of the cleaning and spraying device (6-1) positioned on one side is communicated with an external clean water pump, and the other end generates 5 horizontally-oriented spray heads; a catalyst adding pipe (6-2) is arranged on one side of the cleaning and spraying device (6-1), the catalyst adding pipe (6-2) is circular, hollow and vertically arranged, and a large number of through holes are formed in the surface of the catalyst adding pipe; a mixing stirrer (6-3) is arranged on one side of the catalyst adding pipe (6-2), the mixing stirrer (6-3) is in driving connection with a stirring motor (6-4) on the right side of the mixing stirrer, and the stirring motor (6-4) is of a waterproof design; an automatic cleaning machine (6-5) is arranged on one side inside the trickle bed reactor (6) and is in wireless control connection with the electric cabinet (11); the corrugation generator (6-6) is positioned inside the trickle bed reactor (6) and on one side of the mixing stirrer (6-3);

the mixing agitator (6-3) comprises: a mixed liquid inlet (6-3-1), a magnetic demetallization device (6-3-2), a side door (6-3-3), a mixing impeller (6-3-4), an antioxidant filling port (6-3-5) and a mixed liquid outlet (6-3-6); the mixed liquid inlet (6-3-1) at one side is communicated with the mixed liquid outlet (6-3-6) at the other side; a mixing impeller (6-3-4) is arranged at the inner side of the mixed liquid outlet (6-3-6), a certain number of blades are fixed on the surface, and the blades are driven by a motor to promote the mutual mixing and dissolution of the solution; a magnetic demetallization device (6-3-2) is arranged on one side inside the mixing stirrer (6-3), and the waterproof structure and the bottom sucker horizontally move along with the movable arm; a side door (6-3-3) is arranged opposite to the magnetic metal removing device, and a movable arm of the magnetic metal removing device (6-3-2) unloads an adsorbed object at the side door (6-3-3); an antioxidant filling port (6-3-5) is arranged at one side of the bottom of the mixing stirrer (6-3);

the magnetic demetallizer (6-3-2) comprises: the device comprises a fixed table (6-3-2-1), a horizontal telescopic arm (6-3-2-2), a large arm rotating shaft (6-3-2-3), a vertical telescopic arm (6-3-2-4), an electric control magnetic suction salient point (6-3-2-5), an electric control magnetic suction ring (6-3-2-6), an adsorption table (6-3-2-7) and a horizontal rotating shaft (6-3-2-8); the fixed station (6-3-2-1) positioned on one side is fixed on the base surface and is connected with the horizontal telescopic arm (6-3-2-2) in horizontal layout, and the horizontal telescopic arm (6-3-2-2) has a telescopic structure; the end part of the horizontal telescopic arm is provided with a big arm rotating shaft (6-3-2-3), and the horizontal telescopic arm (6-3-2-2) is hinged with the vertical telescopic arm (6-3-2-4) through the big arm rotating shaft (6-3-2-3); the vertical telescopic arm (6-3-2-4) is of a telescopic structure and is rotatably connected with the adsorption platform (6-3-2-7) at the lower part through a horizontal rotating shaft (6-3-2-8); a plurality of electric control magnetic suction salient points (6-3-2-5) are arranged on the lower surface of the adsorption table (6-3-2-7) and are distributed at equal intervals; a plurality of electric control magnetic suction rings (6-3-2-6) are arranged around the adsorption table (6-3-2-7) and are arranged at equal intervals, and the electric control magnetic suction salient points (6-3-2-5) and the electric control magnetic suction rings (6-3-2-6) are connected with an electric control box (11); the magnetic demetallization device (6-3-2) is waterproof.

3. A device for the preparation of oxytetracycline according to claim 2, characterized in that said automatic washing machine (6-5) comprises: the cleaning device comprises a cleaning shell (6-5-1), a battery motor storage box (6-5-2), a signal transceiver (6-5-3), a crawling adsorption device (6-5-4), a cleaning device (6-5-5) and a spot searching instrument (6-5-6); the automatic cleaning machine (6-5) is of a waterproof structure; a battery motor storage box (6-5-2) is arranged at the center of the cleaning shell (6-5-1), a drawing and fast-assembling structure is arranged in the cleaning shell, a battery, a driving motor and a vacuum pump are arranged in the cleaning shell, and a signal transceiver (6-5-3) is arranged on one side of the battery motor storage box (6-5-2); the crawling adsorption device (6-5-4) is positioned at the top corner of the cleaning shell (6-5-1), and 4 crawling adsorption devices (6-5-4) jointly form a movement mechanism; the cleaner (6-5-5) is positioned at the lower part of the center of the cleaning shell (6-5-1), and the lower surface of the cleaner (6-5-5) is provided with a spot searching instrument (6-5-6); the battery motor storage box (6-5-2), the signal transceiver (6-5-3) and the spot searching instrument (6-5-6) are in wireless control connection with the electric cabinet (11).

4. A device for the preparation of oxytetracycline according to claim 3, characterised in that said crawling adsorption means (6-5-4) comprise: the device comprises a left swing arm, a right swing arm (6-5-4-1), an extending arm (6-5-4-2), an extending hydraulic machine (6-5-4-3), a vertical moving arm (6-5-4-4), a vertical hydraulic machine (6-5-4-5), a positioning disc (6-5-4-6), an adsorption disc (6-5-4-7), a fixed column (6-5-4-8) and an adsorption disc spring (6-5-4-9); the end parts of the left and right swing arms (6-5-4-1) are provided with extending arms (6-5-4-2), the extending arms (6-5-4-2) are rotatably connected with the left and right swing arms (6-5-4-1), the left and right swing arms (6-5-4-1) are used as rotating shafts to swing up and down, extending hydraulic machines (6-5-4-3) are arranged between the extending arms and the left and right swing arms, and the extending hydraulic machines (6-5-4-3) are in wireless control connection with the electric cabinet (11); the vertical moving arm (6-5-4-4) is positioned at the end part of the extending arm (6-5-4-2), the vertical moving arm (6-5-4-4) is rotatably connected with the extending arm (6-5-4-2), a vertical hydraulic machine (6-5-4-5) is arranged between the vertical moving arm (6-5-4-4) and the extending arm (6-5-4-2), and the vertical hydraulic machine (6-5-4-5) is in wireless control connection with the electric cabinet (11); the positioning disc (6-5-4-6) is positioned on the lower surface of the vertical moving arm (6-5-4-4), an adsorption disc (6-5-4-7) is arranged below the positioning disc (6-5-4-6), the adsorption disc (6-5-4-7) and the positioning disc (6-5-4-6) are fixedly connected through a fixing column (6-5-4-8), an air pipe is arranged inside the fixing column (6-5-4-8), one end of the air pipe is communicated with the vacuum pump, and the other end of the air pipe is communicated with the adsorption disc (6-5-4-7); one end of the adsorption disc spring (6-5-4-9) is connected with the positioning disc (6-5-4-6), and the other end is connected with the adsorption disc (6-5-4-7).

5. A device for the preparation of oxytetracycline according to claim 4, characterized in that said washing means (6-5-5) comprise: cleaning a driving machine (6-5-5-1), a fan (6-5-5-2), a transmission gear (6-5-5-3), a rotating disc (6-5-5-4), a cleaning brush head (6-5-5), and a clean water pipeline (6-5-5-6); the cleaning driving machine (6-5-5-1) is in wireless control connection with the electric cabinet (11), a fan (6-5-5-2) is arranged at the output end of the cleaning driving machine (6-5-5-1), and the surface is dried after cleaning is finished; the transmission gear (6-5-5-3) is positioned below the fan (6-5-5-2), and the transmission gear (6-5-5-3) is meshed and connected with an output main shaft of the cleaning driver (6-5-5-1); the rotating disks (6-5-5-4) are positioned on the lower surface of the transmission gear (6-5-5-3), the number of the rotating disks (6-5-5-4) is 3, and the lower surface of each rotating disk (6-5-5-4) is provided with a cleaning brush head (6-5-5-5); the clean water pipeline (6-5-5-6) is positioned on the upper surface of the transmission gear (6-5-5-3), and the clean water pipeline (6-5-5-6) is communicated with the rotating disk (6-5-5-4).

6. A device for preparing oxytetracycline according to claim 5, characterized in that said stent (14) comprises: the support driving machine comprises a support driving machine (14-1), a transmission case (14-2), a support gear (14-3), a support track (14-4), a support shell (14-5), a counterweight body (14-6) and a support body (14-7); the bracket shell (14-5) is positioned at the upper part of the base of the bracket (14) and is independent; the support shell (14-5) is of a hollow structure, and the support track (14-4) is arranged inside the support shell (14-5) and is vertical to and fixedly connected with the base of the support (14); the support body (14-7) is arranged at one side of the transmission case (14-2) and is connected with the transmission case; a bracket gear (14-3) is arranged in the transmission case (14-2) and is meshed and connected with a rack on the surface of the bracket track (14-4); the support body (14-7) is in sliding fit with the support rail (14-4) through the engagement of the support gear (14-3) and the support rail (14-4); the counterweight body (14-6) is positioned outside the support body (14-7) and fixed with the support body, the end part of the counterweight body (14-6) extends out of the support shell (14-5), and the waist part of the counterweight body is fixedly connected with the support shell (14-5); the support driving machine (14-1) is located on one side of the lower end of the transmission case (14-2), the support driving machine (14-1) is in transmission connection with the support gear (14-3), the support driving machine (14-1) is connected with the electric control case (11) in a control mode through a lead, and the support driving machine (14-1) drives the support gear (14-3) to rotate and drives the transmission case (14-2), the support shell (14-5), the counterweight body (14-6) and the support body (14-7) to ascend or descend along the support rail (14-4).

7. Device for the preparation of oxytetracycline according to claim 6, characterized in that said regulation wheel (15) comprises: the oil spray device comprises an adjusting wheel U plate (15-1), a lubricating oil tank (15-2), a moving wheel rotating shaft (15-3), a moving wheel (15-4), an oil nozzle (15-5) and a wheel track (15-6); the U plate (15-1) of the adjusting wheel is of an inverted concave structure and is made of a steel plate, and the side walls of two sides of the U plate are inverted trapezoidal; the movable wheel rotating shaft (15-3) is connected between the side walls of the two sides of the U plate (15-1) of the adjusting wheel, the movable wheel rotating shaft (15-3) is in transmission connection with an external motor, and the movable wheel (15-4) is arranged on the movable wheel rotating shaft (15-3); the moving wheel (15-4) is rotationally connected with the moving wheel rotating shaft (15-3), and an external motor of the moving wheel (15-4) is in control connection with the electric cabinet (11) through a wire; the wheel track (15-6) is positioned at the lower part of the moving wheel (15-4) and is in rolling connection with the moving wheel; the lubricating oil tank (15-2) is fixedly connected to the outer portion of the side wall of one side of the adjusting wheel U plate (15-1), the oil spray nozzle (15-5) is fixedly connected to the inner side of the upper wall of the adjusting wheel U plate (15-1), and the lubricating oil tank (15-2) is connected with the oil spray nozzle (15-5) through an oil guide pipe inside the lubricating oil tank.

8. The oxytetracycline preparation device according to claim 7, characterized in that said lubricating oil tank (15-2) comprises: the device comprises an oil lubricating pump (15-2-1), a distribution box (15-2-2), a filter box (15-2-3), an oil filling pipe (15-2-4), a radiator (15-2-5), a fixing plate (15-2-6), a positioning sleeve (15-2-7) and an oil filling pipe outlet (15-2-8); a lubricating oil pump (15-2-1) positioned at the bottom is communicated with a distribution box (15-2-2) at the upper part, a rectangular box body of the distribution box (15-2-2) is provided with two semicircular short shafts at two ends, two groups of stirring impellers with different diameters are arranged in the distribution box, the diameter of the large stirring impeller is 30cm, the diameter of the small stirring impeller is 9cm, the large stirring impeller and the small stirring impeller are horizontally arranged side by side and stirred in different directions, two branch pipes extend upwards from the two semicircular end points of the distribution box (15-2-2), the two branch pipes are communicated with a filter box (15-2-3) through valves, the diameters of the two branch pipes are different, the diameter of a thick pipe is 8cm, the diameter of a thin pipe is 2cm, and the thick pipe and the thin pipe are respectively arranged at one side; the filter box (15-2-3) is positioned at the upper part of the distribution box (15-2-2) and is communicated with the distribution box (15-2-2), and a filter screen, a settling chamber and a screen impurity remover are arranged in the filter box (15-2-3); the radiator (15-2-5) is positioned at the upper part of the filter box (15-2-3), and the radiator (15-2-5) is made of red copper and is formed by overlapping a plurality of groups of copper plates, and gaps exist among the copper plates; an oil filling pipe (15-2-4) is wound on the outer surface of the radiator (15-2-5), the wound section is made of pressure-resistant red copper, one end of the oil filling pipe (15-2-4) is communicated with the filter box (15-2-3), and the other end of the oil filling pipe penetrates through the positioning sleeve (15-2-7) and is communicated with an outlet (15-2-8) of the oil filling pipe; one end of the fixing plate (15-2-6) is sleeved on the outer surface of the positioning sleeve (15-2-7), and the other end is connected with the fixing wall.

9. The oxytetracycline preparation device of claim 8, characterized in that said oil nozzles (15-5) comprise: the device comprises a main branch pipe (15-5-1), a cover shell (15-5-2), an inclined angle oil injection body (15-5-3) and an oil injection adjusting nozzle (15-5-4); the cover surface shell (15-5-2) is of a hollow inverted circular truncated cone structure with the upper part closed and the bottom opened, a main branch pipe (15-5-1) is arranged right above the cover surface shell (15-5-2), wherein the bottom end of the main branch pipe (15-5-1) is inserted into the cover surface shell (15-5-2), and the top end of the main branch pipe (15-5-1) is communicated with an oil guide pipe on the upper part; the dip angle oil spray bodies (15-5-3) are positioned in the cover surface shell (15-5-2), the number of the dip angle oil spray bodies (15-5-3) is 4-8, the adjacent dip angle oil spray bodies (15-5-3) are distributed at equal angles by taking the main branch pipe (15-5-1) as a central shaft, and each dip angle oil spray body (15-5-3) is communicated with the main branch pipe (15-5-1) through an oil distribution pipe; the oil injection adjusting nozzle (15-5-4) is fixedly connected to the lower part of the cover shell (15-5-2) and can be controlled to adjust a retractable structure so as to control the injection flow and angle;

the inclination angle oil jet body (15-5-3) comprises: the oil pump comprises an oil inlet (15-5-3-1), a tangential oil outlet (15-5-3-2), an oil injection shell (15-5-3-3), a staggered spoiler (15-5-3-4), a shell driver (15-5-3-5) and a shell reinforcing hoop (15-5-3-6); an oil inlet (15-5-3-1) is arranged at the top of the oil injection shell (15-5-3-3), a large number of tangential oil outlets (15-5-3-2) are arranged on the side wall of the oil injection shell (15-5-3-3), and lubricating oil is tangentially sprayed out along the surface of the oil injection shell (15-5-3-3); a large number of staggered spoilers (15-5-3-4) are arranged on the inner wall of the oil injection shell (15-5-3-3) and are fixed on the surface of the inner wall in a staggered manner, the staggered spoilers (15-5-3-4) are of a thin plate stainless steel structure, the length of the staggered spoilers is 4/5 the length of the oil injection shell (15-5-3-3), and the height of the staggered spoilers is 1/10 the radius of the oil injection shell (15-5-3-3); a shell reinforcing hoop (15-5-3-6) and a shell driver (15-5-3-5) are arranged outside the oil injection shell (15-5-3-3); wherein, the shell drivers (15-5-3-5) are arranged in the upper and lower 2 groups and simultaneously drive the oil injection shell (15-5-3-3) to rotate;

the housing driver (15-5-3-5) includes: a shell flange (15-5-3-5-1), a first shaft (15-5-3-5-2), a circumferential rack (15-5-3-5-3), a connecting plate (15-5-3-5-4), a horizontal positioning wheel (15-5-3-5-5), a circumferential driving wheel (15-5-3-5-6) and a second shaft (15-5-3-5-7); a circumferential rack (15-5-3-5-3) is surrounded outside the oil injection shell (15-5-3-3), and the oil injection shell and the circumferential rack are fixedly connected through a connecting plate (15-5-3-5-4); a group of horizontal positioning wheels (15-5-3-5-5) are respectively arranged above and below the circumferential rack (15-5-3-5-3) to prevent the circumferential driving wheel (15-5-3-5-6) from deviating, and the horizontal positioning wheels (15-5-3-5-5) rotate around the shaft I (15-5-3-5-2); two sides of the horizontal positioning wheel (15-5-3-5-5) are respectively provided with a group of circumferential driving wheels (15-5-3-5-6) which are fixedly connected; a second shaft (15-5-3-5-7) drives a circumferential driving wheel (15-5-3-5-6) to rotate, and a gear structure of the circumferential driving wheel (15-5-3-5-6) is in meshing transmission with a circumferential rack (15-5-3-5-3); the shell flange (15-5-3-5-1) realizes the up-and-down butt joint of the oil injection shell (15-5-3-3).

10. A device for preparing oxytetracycline according to claim 9, characterised in that said circumferential rack (15-5-3-5-3) comprises: the oil filling machine comprises a circumferential tooth surface (15-5-3-5-3-1), sector teeth (15-5-3-5-3-2), an oil filling machine (15-5-3-5-3-3), a bottom transverse plate (15-5-3-5-3-4), a damping spring (15-5-3-5-3-5) and a blowing pipe (15-5-3-5-3-6); the circumferential tooth surfaces (15-5-3-5-3-1) are 2 groups, are oppositely arranged and are connected through a bottom transverse plate (15-5-3-5-3-4); fan-shaped teeth (15-5-3-5-3-2) are equidistantly distributed on the surface of the circumferential tooth surface (15-5-3-5-3-1); an oiling machine (15-5-3-5-3-3) is arranged on the bottom transverse plate (15-5-3-5-3-4) and is used for gear meshing lubrication; the damping spring (15-5-3-5-3-5) is fixed on the surface of the bottom transverse plate (15-5-3-5-3-4), and the top of the damping spring is provided with a balancing weight; one end of the air blowing pipe (15-5-3-5-3-6) is in threaded connection with the damping spring (15-5-3-5-3-5) and penetrates through the balancing weight, the damping spring (15-5-3-5-3-5) and the bottom transverse plate (15-5-3-5-3-4) to extend to the outside, the outlet of the other end of the air blowing pipe is aligned with the fan-shaped teeth (15-5-3-5-3-2), and the air blowing pipe (15-5-3-5-3-6) freely swings along with the vibration of the damping spring (15-5-3-5-3-5);

the oiling machine (15-5-3-5-3-3) comprises: a protective cover (15-5-3-5-3-3-1), an oil storage bag (15-5-3-5-3-3-2), a stirring oil separator (15-5-3-5-3-3), a filtering round platform box (15-5-3-5-3-4), a settling box (15-5-3-5-3-3-5), an overflow pipe (15-5-3-5-3-3-6), an oil-water separator (15-5-3-5-3-7), a standing separation box (15-5-3-3-8), a recovery oil pipe (15-5-3-5-3-3-9), a separation water pipe (15-5-3-5-3-3-10), a sediment pipe (15-5-3-5-3-3-11), a metal sediment pipe (15-5-3-5-3-3-12), an oil inlet pipeline (15-5-3-5-3-3-13) and a threaded oil outlet pipe (15-5-3-5-3-3-14); an oil inlet channel (15-5-3-5-3-3-13) positioned at the lower part, external oil enters from the oil inlet channel and is communicated with an upper stirring oil distributor (15-5-3-5-3-3-3), 2 groups of stirring impellers are arranged in the stirring oil distributor (15-5-3-5-3-3-3), the stirring impellers are horizontally distributed and stir at low speed in different directions, wherein the upper part of the stirring impeller at the left side is provided with a channel which is communicated with an oil storage bag (15-5-3-5-3-3-2), the periphery of the oil storage bag (15-5-3-5-3-3-2) is provided with a protective cover (15-5-3-3-1), and the upper part of the oil storage bag is provided with a threaded oil outlet pipe (15-5-3-5-3-3-3-14), the two are communicated; a filtering circular truncated cone box (15-5-3-5-3-3-4) is arranged at the lower part of the left stirring impeller of the stirring oil separator (15-5-3-5-3-3) and communicated with the stirring impeller through a conduit, and a filter screen is arranged in the filtering circular truncated cone box (15-5-3-5-3-3-4); the sedimentation tank (15-5-3-5-3-3-5) is positioned at the lower part of the filtering circular truncated cone tank (15-5-3-5-3-3-4) and is communicated with the filtering circular truncated cone tank, a metal sediment pipe (15-5-3-5-3-3-12) is arranged at the lower part of the right side of the sedimentation tank (15-5-3-5), an overflow pipe (15-5-3-3-6) is arranged at the upper part of the left side of the sedimentation tank (15-5-3-5-3-3-6), and an oil inlet of the overflow pipe (15-5-3-5-3-3-6) is always positioned on the surface of the solution in the sedimentation tank (15-5-3-5-3; the oil-water separator (15-5-3-5-3-3-7) positioned at the lower part is communicated with the settling tank (15-5-3-5-3-3-5) through an overflow pipe (15-5-3-3-6), the left end part of the oil-water separator is closed, the right end part of the oil-water separator is provided with a settling pipe (15-5-3-5-3-3-11), the oil-water separator (15-5-3-5-3-3-7) is horizontally inserted into the standing separation tank (15-5-3-5-3-3-8), wherein the insertion section of the standing separation tank (15-5-3-5-3-3-8), controllable rotation is realized, and the surface of the rotary shaft is provided with a large number of small through holes; a recovery oil pipe (15-5-3-5-3-3-9) is arranged at the upper part of the standing separation box (15-5-3-5-3-8), and a separation water pipe (15-5-3-5-3-3-10) is arranged at the lower part;

the stirring oil separator (15-5-3-5-3-3-3) comprises: a damping spring (15-5-3-5-3-3-3-1), a first stirring wheel (15-5-3-5-3-3-2), an auxiliary paddle (15-5-3-5-3-3-3), and a second stirring wheel (15-5-3-5-3-3-4); a stirring wheel (15-5-3-5-3-3-2) and a stirring wheel II (15-5-3-5-3-3-4) are arranged in the stirring oil separator (15-5-3-5-3-3-3), the stirring wheel II and the stirring wheel II are horizontally arranged and stirred in different directions, wherein an oil inlet channel (15-5-3-5-3-3-13) is arranged at the lower part of the axle center of the stirring wheel II (15-5-3-5-3-4), a clear oil outlet is arranged at the upper part of the axle center of the stirring wheel I (15-5-3-5-3-3-2), and a waste oil outlet is arranged at the lower part of the axle center of the stirring wheel II (15-5-3-5-3; a damping spring (15-5-3-5-3-3-3-1) is arranged at one end in a shell of the oil separator (15-5-3-5-3-3-3), an auxiliary paddle (15-5-3-5-3-3-3-3) is arranged at the other end, wherein the root of the damping spring (15-5-3-5-3-3-1) is fixed on the shell, and the upper part of the damping spring freely swings; the lower part of the auxiliary paddle (15-5-3-5-3-3-3-3) is provided with a cylinder, one end of the cylinder is rotatably connected with the upper paddle, and the other end of the cylinder is fixed in the shell of the oil separator (15-5-3-5-3-3-3).

11. The apparatus for preparing oxytetracycline according to claim 10, wherein the apparatus is produced by a method comprising:

step 1: in a terramycin preparation device; various raw materials are cooked into clinker, beaten and mixed in a dissolving tank (1) according to a proportion, the mixture enters a main fermentation box (13) through a delivery pump (2) for fermentation treatment, in the process, strains are inoculated through an inoculation sampling return pipe (12), the temperature, the pH value, the dissolved oxygen value and the stirring rotating speed of the main fermentation box (13) are adjusted, meanwhile, a mixing tank (3) is used for preparing a mixed solution from various auxiliary raw materials and injecting the mixed solution into the main fermentation box (13) for fermentation process optimization, and the generated overflowing solution flows back into the dissolving tank (1) through the inoculation sampling return pipe (12) and is mixed with the raw materials as pretreatment water; fermentation liquor enters a distillation tower (5) through a distillation tower input pump (4), wherein a gas-liquid separator (10) separates a gas phase into a trickle bed reactor (6), other solutions directly enter the trickle bed reactor (6) to carry out biochemical reaction under the action of a catalyst, an obtained product flows out of a high-level discharge pipe (9), generated waste gas is discharged through a sampling exhaust pipe (8), and sediment is discharged from a sediment discharge pipe (7) after treatment; in the reaction process, an operator monitors the reaction process in real time through the sampling exhaust pipe (8);

step 2: in the working process of the distillation tower (5), heating steam enters the distillation tower (5) from the steam pipes (5-8) and the distribution branch pipes of each layer of tower plate, the mixed solution before treatment enters the distillation tower (5) from the liquid inlet (5-7) and flows through each layer of tower plate, under the action of the catalytic system (5-4), one part flows out from the gas outlet pipe (5-6) in a gaseous state, the other part flows out from the liquid outlet pipe (5-5) in a liquid state, and simultaneously, generated precipitate is discharged from the slag outlet (5-1); wherein the slag control valve (5-2) controls the sediment discharge process;

and 3, step 3: in the working process of the slag control valve (5-2), the electric cabinet (11) controls the control valve motor (5-2-7) to operate to drive the gear A (5-2-8) and the gear B (5-2-9) to rotate, and further drives the valve plate (5-2-4) to open or close through the valve driving arm (5-2-5) and the rotating arm (5-2-6); when foreign matters block the valve plate (5-2-4), the control valve motor (5-2-7) controls the valve driving arm (5-2-5) and the rotating arm (5-2-6) to shake in a reciprocating manner, so that the valve spring (5-2-3) drives the valve plate (5-2-4) to vibrate strongly, the foreign matters are thrown away, and the slag control valve (5-2) is restored to a normal function;

and 4, step 4: in the working process of the catalytic system (5-4), hot steam enters from the bottom, and mixed liquor flowing in from the upper part splashes onto the multistage meshed tower plates (5-4-9) respectively to exchange heat with the hot steam, wherein the hot steam and the mixed liquor are fully mixed in the hot mixing chamber (5-4-3) to promote reaction; the heat collecting hopper (5-4-11) fully exchanges heat between the hot steam and the solution splashed by the net contacting tower plate (5-4-9) by utilizing a trumpet-shaped structure, a large number of through holes on the surface and a waist guide plate; the accelerator spray ring (5-4-10), the catalytic reaction filler (5-4-8) and the net contacting tower plate (5-4-9) further promote the chemical reaction of the mixed solution; the hot mixing chamber (5-4-3) further promotes the hot steam to be fully mixed with the mixed liquid by utilizing the vertically-through cylindrical hollow structure of the hot mixing chamber; the vaporized gas enters the next procedure from the upper part, and the sediment is discharged from a slag discharge control valve (5-2);

and 5, step 5: when the trickle bed reactor (6) works, a gas-liquid parallel flow mode is adopted, gas and liquid enter the trickle bed reactor (6) from one side in the same direction, a catalyst flowing out of the catalyst adding pipe (6-2) slowly enters the trickle bed reactor to be mixed with the gas and the solution to react, a stirring motor (6-4) drives a mixing stirrer (6-3) to promote the reaction to be carried out under the slow stirring action, precipitates are discharged from the bottom, and products are discharged from the top; when the interior of the trickle bed reactor (6) needs to be cleaned after the material is discharged, the automatic cleaning machine (6-5) and the cleaning and spraying device (6-1) jointly act to jointly undertake cleaning work;

and 6, step 6: in the working process of the mixing stirrer (6-3), the mixed solution enters the mixing stirrer (6-3) through a mixed liquid inlet (6-3-1), metal chips are removed through a magnetic metal remover (6-3-2), an antioxidant is injected into an antioxidant injection port (6-3-5) to prevent oxidative deterioration, and the solution is discharged through the mixed liquid outlet (6-3-6) under the action of a mixing stirring impeller (6-3-4);

and 7, step 7: in the working process of the magnetic metal removing device (6-3-2), external current is conveyed to the electric control magnetic suction salient point (6-3-2-5) and the electric control magnetic suction ring (6-3-2-6) under the control of the electric cabinet (11) to generate magnetic suction force to adsorb metal chips at the bottom and the periphery of the container, meanwhile, the electric cabinet (11) controls the horizontal telescopic arm (6-3-2-2) and the vertical telescopic arm (6-3-2-4) to extend or retract, controls the large arm rotating shaft (6-3-2-3) and the horizontal rotating shaft (6-3-2-8) to rotate, adsorbs metal chips at each corner in the whole container, and unloads the adsorbed metal chips from the side door (6-3-3);

and 8, step 8: in the cleaning process of the automatic cleaning machine (6-5), the spot searching instrument (6-5-6) detects the spot condition of the wall surface of the tank body in real time, when the spot searching instrument (6-5-6) detects that the spot exists on the wall surface, the spot searching instrument (6-5-6) transmits a signal to the electric cabinet (11) through the signal transceiver (6-5-3), the electric cabinet (11) controls the crawling adsorption device (6-5-4) to walk to the spot, the cleaning machine (6-5-5) is operated, and the spot is cleaned;

step 9: when the crawling adsorption device (6-5-4) works, the left swing arm and the right swing arm (6-5-4-1) promote the adsorption disc (6-5-4-7) to move left and right, the extending arm (6-5-4-2) promotes the adsorption disc to move front and back, and the vertical moving arm (6-5-4-4) promotes the adsorption disc to move up and down; the vacuum pump pumps air to promote the adsorption disc (6-5-4-7) to be tightly adsorbed on the wall surface of the vessel; the electric cabinet (11) starts the extension hydraulic machine (6-5-4-3) and the vertical hydraulic machine (6-5-4-5), and controls the crawling adsorption device (6-5-4) to move continuously through the extension movement of the extension hydraulic machine (6-5-4-3) and the vertical hydraulic machine (6-5-4-5);

step 10: when the cleaner (6-5-5) works, the electric cabinet (11) starts the cleaning driving machine (6-5-5-1) to drive the transmission gear (6-5-5-3) to carry out gear power transmission, and the transmission gear (6-5-5-3) drives the rotating disc (6-5-5-4) and the cleaning brush head (6-5-5-5) to carry out rotary motion, so that the surface of the wall of the cleaner is cleaned; after the cleaning, the driving machine (6-5-5-1) drives the fan (6-5-5-2) to rotate at a high speed through the output main shaft, and the surface moisture is dried and cleaned;

and 11, step 11: in the operation process of the support (14), a power supply is switched on and the electric cabinet (11) is started, the electric cabinet (11) controls the support driver (14-1) to operate and drives the support gear (14-3) to rotate through the transmission case (14-2), so that the support gear (14-3) and the support rail (14-4) are driven to be in meshing transmission, and as the counterweight body (14-6) is fixed with the support shell (14-5), the support shell (14-5) is separated from the support (14) base, and the support rail (14-4) is fixed with the support (14) base, only the support driver (14-1), the support gear (14-3), the transmission case (14-2), the support shell (14-5), the counterweight body (14-6) and the support body (14-7) move up and down, thereby realizing that the bracket shell (14-5) drives the top plate of the bracket (14) to move up and down;

step 12: in the working process of the adjusting wheel (15), the rotating shaft (15-3) of the moving wheel runs under the driving of an external motor and drives the moving wheel (15-4) to roll on the upper part of the wheel track (15-6), so that the position of the distillation tower (5) is adjusted; meanwhile, the lubricating oil tank (15-2) injects lubricating oil into the movable wheel (15-4) through an oil nozzle (15-5);

step 13: in the working process of the lubricating oil tank (15-2), the lubricating oil is injected into the distribution tank (15-2-2) by the lubricating oil pump (15-2-1); when a high-viscosity lubricant is needed, a small stirring impeller of the distribution box (15-2-2) is started, and the lubricant enters the filter box (15-2-3) through the control of a thin tube and a valve; when a low-viscosity lubricant is needed, a large stirring impeller of a distribution box (15-2-2) is started, the low-viscosity lubricant enters a filter box (15-2-3) under the control of a thick pipe and a valve, clean oil enters an oil injection pipe (15-2-4) under the action of a filter screen, a settling chamber and a screen impurity remover in the filter box, and meanwhile, a radiator (15-2-5) cools the clean oil, passes through a positioning sleeve (15-2-7) and flows into the next working procedure from an oil injection pipe outlet (15-2-8);

step 14: in the working process of the oil nozzle (15-5), lubricating oil enters the main branch pipe (15-5-1) from the oil guide pipe; then, the lubricating oil in the main branch pipe (15-5-1) is branched from the oil distribution pipe into the inclined angle oil injection body (15-5-3) and flows out of an oil injection hole on the surface of the inclined angle oil injection body (15-5-3) to inject oil for the rotating shaft of the object for lubrication;

step 15: in the working process of the inclined angle oil injection body (15-5-3), the upper and lower 2 groups of shell drivers (15-5-3-5) drive the oil injection shell (15-5-3-3) to rotate, and as a plurality of staggered spoilers (15-5-3-4) are arranged in the oil injection shell, when lubricating oil enters from the oil inlet (15-5-3-1), the staggered spoilers (15-5-3-4) promote the lubricating oil in the oil injection shell (15-5-3-3) to rotate and tangentially spray from the tangential oil outlet (15-5-3-2), so that uniform spraying is facilitated;

step 16: in the working process of the shell driver (15-5-3-5), an external motor drives a circumferential driving wheel (15-5-3-5-6) to rotate through a second shaft (15-5-3-5-7), and then drives an oil injection shell (15-5-3-3) to rotate through a circumferential rack (15-5-3-5-3);

step 17: in the working process of the circumferential rack (15-5-3-5-3), the oiling machine (15-5-3-5-3-3) is used for gear meshing oiling lubrication; meanwhile, the vibration generated in the gear walking process is absorbed by a damping spring (15-5-3-5-3-5), a balancing weight and a blowing pipe (15-5-3-5-3-6), because the blowpipe (15-5-3-5-3-6) is only in threaded connection with the damping spring (15-5-3-5-3-5) and the two ends are communicated, the damping spring (15-5-3-5-3-5) is prompted to drive the blowpipe (15-5-3-5-3-6) to swing left and right by the vibration generated in the gear walking process, and the peripheral fan-shaped teeth (15-5-3-5-3-2) are blown to cool;

step 18: in the working process of the oiling machine (15-5-3-5-3-3), external lubricating oil enters the stirring oil distributor (15-5-3-5-3-3-3) through the oil inlet channel (15-5-3-5-3-13) to be stirred, and after separation, the stirring oil distributor (15-5-3-5-3-3-3) conveys high-quality oil to the threaded oil outlet pipe (15-5-3-5-3-3-14) to be sprayed out through the oil storage bag (15-5-3-5-3-3-2) so as to provide lubrication for moving workpieces; the separated waste oil enters a filtering circular truncated cone box (15-5-3-5-3-3-4) from the stirring oil separator (15-5-3-5-3-3-3) for filtering, and then enters a settling box (15-5-3-5-3-3-5), wherein the metal scrap precipitate is discharged from a metal slag settling pipe (15-5-3-5-3-3-12); an overflow pipe (15-5-3-5-3-3-3-6) collects the solution on the inner surface of the precipitation tank (15-5-3-5-3-3-5), and transmits the solution to an oil-water separator (15-5-3-5-3-7), the solution enters a standing separation tank (15-5-3-5-3-3-8) through a large number of small through holes on the surface of the pipe, the oil-water separator (15-5-3-5-3-7) is started to rotate to promote oil-water separation, an oil-water separation layer is formed in the standing separation tank (15-5-3-5-3-3-8) after standing, the recovered oil is discharged from a recovered oil pipe (15-5-3-5-3-3-3-9), The separated water is discharged from a separated water pipe (15-5-3-5-3-3-10) and the precipitate is discharged from a precipitate pipe (15-5-3-5-3-3-11);

step 19: in the working process of the stirring oil separator (15-5-3-5-3-3-3), external lubricating oil enters the stirring oil separator (15-5-3-5-3-3) through the oil inlet channel (15-5-3-5-3-13), flows along the inner ring and the outer ring of the shell of the stirring oil separator (15-5-3-5-3-3) under the non-co-directional stirring of the stirring wheel I (15-5-3-5-3-3-2) and the stirring wheel II (15-5-3-5-3-3-4) and is subjected to the damping spring (15-5-3-5-3-3-3-1), The damping action of an auxiliary paddle (15-5-3-5-3-3-3) ensures that high-quality oil flows out from the upper clear oil outlet and waste oil flows out from the lower waste oil outlet;

the strain selects streptomyces rimosus, spores of the streptomyces rimosus are inoculated into a first-level seed tank for culture, and first-level seeds are obtained; inoculating the obtained single colony into a liquid culture medium for shake culture to obtain a secondary seed; inoculating the second-level seeds into the fermentation liquor, and performing shaking culture to obtain third-level seeds, so as to prepare activated fermentation strains; the raw materials are two of corn starch, potato starch, corn mash, cassava starch, wheat starch, sweet potato starch, sorghum starch or bean starch, or a mixture of the starch; simultaneously adding cellulose hydrolysate, diammonium hydrogen phosphate, corn steep liquor, potassium chloride, magnesium sulfate heptahydrate, dipotassium hydrogen phosphate, ferrous sulfate heptahydrate and water, and mixing to obtain slurry; the auxiliary raw materials comprise fish meal, peptone, yeast extract, sodium chloride, soybean meal, diammonium hydrogen phosphate, ferrous sulfate, sodium citrate, potassium dihydrogen phosphate, zinc sulfate, magnesium sulfate, calcium chloride, amylase, vegetable oil and a defoaming agent.

Technical Field

The invention belongs to the technical field of medicine and health, and particularly relates to a preparation device and method of oxytetracycline.

Background

Terramycin is a broad-spectrum antibiotic, has an inhibiting effect on gram-positive bacteria and gram-negative bacteria, and also has a certain inhibiting effect on chlamydia, rickettsia, mycoplasmas, spirochetes and the like. The terramycin is mainly used for preventing and treating livestock and poultry Escherichia coli, salmonella infection (such as calf white dysentery, lamb dysentery, piglet yellow and white dysentery, young animal paratyphoid, etc.), pasteurella infection, brucella infection, swine enzootic pneumonia and chicken chronic respiratory disease; it is also used for treating rickettsial disease in dogs and infectious anemia in cats, and preventing chlamydia disease and leptospirosis in dogs; it can be topically applied to treat endometritis and tissue necrosis caused by necrobacillus. And terramycin is used as a feed additive, and has the effects of promoting growth and improving feed conversion rate.

With the further development of animal husbandry, the market demand of terramycin is continuously expanded in recent years, the quality requirement of domestic and foreign customers on terramycin is higher and higher, and the existing preparation device for terramycin mainly has the defects of low yield, high cost and low quality, so that improvement on preparation equipment for terramycin is necessary.

Disclosure of Invention

In order to solve the above technical problems, the present invention relates to a oxytetracycline preparation device, comprising: the system comprises a dissolving tank 1, a delivery pump 2, a blending tank 3, a distillation tower input pump 4, a distillation tower 5, a trickle bed reactor 6, a sediment discharge pipe 7, a sampling exhaust pipe 8, a high-level discharge pipe 9, a gas-liquid separator 10, an electric cabinet 11, an inoculation sampling return pipe 12, a main fermentation box 13, a bracket 14 and an adjusting wheel 15; the dissolving tank 1 positioned on one side is communicated with a main fermentation box 13 positioned on the upper left part through a delivery pump 2, and the top of the main fermentation box 13 is of a controllable opening and closing structure; the lower part of the main fermentation box 13 is provided with a blending tank 3, one side of the upper part is provided with an inoculation sampling return pipe 12 which is communicated with the main fermentation box and the inoculation sampling return pipe 12, wherein the inoculation sampling return pipe 12 is used for inoculation and sampling, and returns the discharged water to the dissolving tank 1; an electric cabinet 11 is arranged at the upper part of the bracket 14; a distillation tower 5 is arranged on one side of the support 14, the distillation tower 5 is vertically arranged, the bottom of the distillation tower 5 is communicated with external steam, the distillation tower 5 is of a hollow structure, the shell of the distillation tower 5 is made of high polymer materials, the distillation tower 5 is communicated with a main fermentation box 13 through a distillation tower input pump 4, and the distillation tower 5 is communicated with a gas-liquid separator 10 on the upper part; the trickle bed reactor 6 is respectively communicated with a gas-liquid separator 10 and a distillation tower 5 in a gas-liquid parallel flow mode; a sediment discharge pipe 7 is arranged at the lower part of the trickle bed reactor 6, a high-level discharge pipe 9 is arranged at the upper part of the trickle bed reactor 6, a sampling exhaust pipe 8 is arranged at the waist part of the trickle bed reactor, and the trickle bed reactor 6 is communicated with the three parts; the regulating wheels 15 are positioned at the bottom of the distillation tower 5, and the number of the regulating wheels is four; the delivery pump 2 and the distillation tower input pump 4 are in control connection with an electric cabinet 11 through wires.

Further, the distillation column 5 includes: 5-1 parts of slag outlet, 5-2 parts of slag control valve, 5-3 parts of distillation tower shell, 5-4 parts of catalytic system, 5-5 parts of liquid outlet pipe, 5-6 parts of gas outlet pipe, 5-7 parts of liquid inlet and 5-8 parts of steam pipe; the lower part of the distillation tower 5 is provided with a slag outlet 5-1 which is communicated with the distillation tower through a slag outlet control valve 5-2; a catalytic system 5-4 is arranged at the upper part of the slag control valve 5-2 and inside the distillation tower shell 5-3; a steam pipe 5-8 is arranged on one side of the distillation tower shell 5-3, a liquid outlet pipe 5-5 is arranged on the other side, a liquid inlet 5-7 is arranged at the waist part, an air outlet pipe 5-6 is arranged at the top part, and the distillation tower shell 5-3 is communicated with the four parts.

Further, the slag control valve 5-2 includes: 5-2-2 parts of a control valve shell, 5-2-3 parts of a valve spring, 5-2-4 parts of a valve plate, 5-2-5 parts of a valve driving arm, 5-2-6 parts of a rotating arm, 5-2-7 parts of a control valve motor, a gear A5-2-8 part and a gear B5-2-9 part; the valve plates 5-2-4 are positioned inside the control valve shell 5-2-2, the number of the valve plates 5-2-4 is 2, and valve springs 5-2-3 are fixedly connected between the adjacent valve plates 5-2-4; the number of the valve springs 5-2-3 is 6, the valve springs are distributed at equal intervals and made of stainless steel, the valve springs 5-2-3 control the slag control valve 5-2 to be elastically closed, foreign matters can be thrown away, and the normal opening and closing functions of the slag control valve 5-2 are realized; one end of the valve driving arm 5-2-5 is fixedly connected with the valve plate 5-2-4 through a support rod, the other end of the valve driving arm 5-2-5 is rotatably connected with a rotating arm 5-2-6 through a rotating shaft, and the rotating arm 5-2-6 is arranged at the upper part of the valve driving arm 5-2-5; the gear B5-2-9 is rotationally connected with the rotating arm 5-2-6; one side of the gear B5-2-9 is provided with a gear A5-2-8 which are meshed and connected; the control valve motor 5-2-7 is positioned on one side of the gear A5-2-8 and is in transmission connection with the gear A5-2-8, and the control valve motor 5-2-7 is in control connection with the electric cabinet 11 through a wire.

Further, the catalytic system 5-4 includes: 5-2 parts of a slag control valve, 5-4-2 parts of a lower connecting flange, 5-4-3 parts of a hot mixing chamber, 5-4-4 parts of a catalytic shell, 5-4-5 parts of a vaporization concentration sensor, 5-4-6 parts of a vaporization chamber, 5-4-7 parts of an upper connecting flange, 5-4-8 parts of catalytic reaction fillers, 5-4-9 parts of a net contacting tower plate, 5-4-10 parts of an accelerator spray ring and 5-4-11 parts of a heat collecting hopper; the lower connecting flange 5-4-2 is positioned at the lower part of the whole catalytic system 5-4, the upper part of the lower connecting flange is provided with a vaporization chamber 5-4-6 and an upper connecting flange 5-4-7, and the vaporization chamber 5-4-6 is communicated with the upper connecting flange 5-4-7 and fixedly connected with the catalytic shell 5-4-4; the upper end and the lower end of the catalytic shell 5-4-4 are respectively fixedly connected with an upper connecting flange 5-4-7 and a lower connecting flange 5-4-2, wherein the lower connecting flange 5-4-2 is positioned at the lower part of the catalytic shell 5-4-4; the hot mixing chamber 5-4-3 is arranged in the catalytic shell 5-4-4 and above the slag control valve 5-2, the hot mixing chamber 5-4-3 is a cylindrical hollow structure which is communicated up and down, and hot steam and mixed liquid are fully mixed in the hot mixing chamber; the other end of the hot mixing chamber 5-4-3 is communicated with a slag control valve 5-2 through a lower connecting flange 5-4-2, wherein the slag control valve 5-2 is positioned at the lower part of the lower connecting flange 5-4-2; the heat collecting hopper 5-4-11 is positioned at the upper part of the heat mixing chamber 5-4-3 and is communicated with the heat mixing chamber 5-4-3, the heat collecting hopper 5-4-11 is in a horn shape, is communicated up and down, is small at the bottom and large at the top, is provided with a large number of through holes on the surface, and is provided with a guide plate at the waist part, and the heat collecting hopper can be used for carrying out full heat exchange on hot steam and a solution splashed by the screen contacting tower plate 5-4-9 by; 5-4-8 parts of catalytic reaction fillers, 5-4-9 parts of net contacting tower plates and 5-4-10 parts of accelerator spraying rings are arranged at the upper parts of the heat collecting hoppers 5-4-11, wherein the number of the catalytic reaction fillers 5-4-8 is 3, and the catalytic reaction fillers 5-4-8 adjacent to each other are distributed at equal intervals; the surface of the net contacting tower plate 5-4-9 is provided with a large number of through holes, the number of the through holes is 20, and the through holes are equidistantly distributed in the catalytic shell 5-4-4; injecting an accelerant into the catalytic shell 5-4-4 by using the accelerant injection ring 5-4-10; 5-4-10 parts of accelerator spray ring, 5-4-8 parts of catalytic reaction filler and 5-4-9 parts of net contacting tower plate promote the mixed solution to carry out chemical reaction; the vaporization concentration sensor 5-4-5 is arranged at the waist of the catalytic shell 5-4-4, and the vaporization concentration sensor 5-4-5 is connected with the electric cabinet 11 in a wire control way.

Further, the trickle bed reactor 6 includes: cleaning and spraying device 6-1, catalyst adding pipe 6-2, mixing stirrer 6-3, stirring motor 6-4, automatic cleaning machine 6-5 and corrugation generator 6-6; one end of the cleaning and spraying device 6-1 positioned at one side is communicated with an external clean water pump, and the other end generates 5 horizontally-oriented spray heads; a catalyst adding pipe 6-2 is arranged on one side of the cleaning and spraying device 6-1, the catalyst adding pipe 6-2 is circular, hollow and vertically arranged, and a large number of through holes are formed in the surface of the catalyst adding pipe; a mixing stirrer 6-3 is arranged on one side of the catalyst adding pipe 6-2, the mixing stirrer 6-3 is in driving connection with a stirring motor 6-4 on the right side of the mixing stirrer, and the stirring motor 6-4 is of a waterproof design; an automatic cleaning machine 6-5 is arranged on one side inside the trickle bed reactor 6 and is in wireless control connection with an electric cabinet 11; the corrugation generator 6-6 is located inside the trickle bed reactor 6 on the side of the mixing agitator 6-3.

Further, the mixing agitator 6-3 includes: 6-3-1 parts of a mixed liquid inlet, 6-3-2 parts of a magnetic demetallization device, 6-3-3 parts of a side door, 6-3-4 parts of a mixing impeller, 6-3-5 parts of an antioxidant filling port and 6-3-6 parts of a mixed liquid outlet; the mixed liquid inlet 6-3-1 at one side is communicated with the mixed liquid outlet 6-3-6 at the other side; a mixing impeller 6-3-4 is arranged at the inner side of the mixed liquid outlet 6-3-6, a certain number of blades are fixed on the surface, and the blades are driven by a motor to promote the mutual mixing and dissolution of the solution; a magnetic demetallization device 6-3-2 is arranged on one side inside the mixing stirrer 6-3, and the waterproof structure and the bottom sucker horizontally move along with the movable arm; a side door 6-3-3 is arranged opposite to the magnetic metal removing device, and a movable arm of the magnetic metal removing device 6-3-2 unloads an adsorbed object at the side door 6-3-3; an antioxidant filling port 6-3-5 is arranged at one side of the bottom of the mixing stirrer 6-3.

Further, the magnetic demetallizer 6-3-2 comprises: the device comprises a fixed table 6-3-2-1, a horizontal telescopic arm 6-3-2-2, a large arm rotating shaft 6-3-2-3, a vertical telescopic arm 6-3-2-4, an electric control magnetic suction salient point 6-3-2-5, an electric control magnetic suction ring 6-3-2-6, an adsorption table 6-3-2-7 and a horizontal rotating shaft 6-3-2-8; the fixed station 6-3-2-1 positioned at one side is fixed on the base surface and is connected with the horizontal telescopic arm 6-3-2-2 in horizontal layout, and the horizontal telescopic arm 6-3-2-2 can be in a telescopic structure; the end part of the horizontal telescopic boom is provided with a large boom rotating shaft 6-3-2-3, and the horizontal telescopic boom 6-3-2-2 is hinged with the vertical telescopic boom 6-3-2-4 through the large boom rotating shaft 6-3-2-3; the vertical telescopic arm 6-3-2-4 is of a telescopic structure and is rotatably connected with the adsorption platform 6-3-2-7 at the lower part through a horizontal rotating shaft 6-3-2-8; a plurality of electric control magnetic suction salient points 6-3-2-5 are arranged on the lower surface of the adsorption table 6-3-2-7 and are distributed at equal intervals; a plurality of electric control magnetic suction rings 6-3-2-6 are arranged around the adsorption table 6-3-2-7 and are distributed at equal intervals, and the electric control magnetic suction salient points 6-3-2-5 and the electric control magnetic suction rings 6-3-2-6 are connected with an electric control box 11; the magnetic demetallization device 6-3-2 is waterproof.

Further, the automatic washing machine 6-5 includes: the cleaning device comprises a cleaning shell 6-5-1, a battery motor storage box 6-5-2, a signal transceiver 6-5-3, a crawling adsorption device 6-5-4, a cleaning device 6-5-5 and a spot searching instrument 6-5-6; the automatic cleaning machine 6-5 is of a waterproof structure; a battery motor storage box 6-5-2 is arranged at the center of the cleaning shell 6-5-1, a drawing and fast-assembling structure is arranged in the cleaning shell, a battery, a driving motor and a vacuum pump are arranged in the cleaning shell, and a signal transceiver 6-5-3 is arranged on one side of the battery motor storage box 6-5-2; the crawling adsorption device 6-5-4 is positioned at the top corner of the cleaning shell 6-5-1, and 4 crawling adsorption devices 6-5-4 jointly form a movement mechanism; the cleaner 6-5-5 is positioned at the lower part of the center of the cleaning shell 6-5-1, and the lower surface of the cleaner 6-5-5 is provided with a spot searching instrument 6-5-6; the battery motor storage box 6-5-2, the signal transceiver 6-5-3 and the spot searching instrument 6-5-6 are in wireless control connection with the electric cabinet 11.

Further, the crawling adsorption device 6-5-4 comprises: 6-5-4-1 parts of a left swing arm, a right swing arm, 6-5-4-2 parts of an extending arm, 6-5-4-3 parts of an extending hydraulic machine, 6-5-4-4 parts of a vertical moving arm, 6-5-4-5 parts of a vertical hydraulic machine, 6-5-4-6 parts of a positioning disc, 6-5-4-7 parts of an adsorption disc, 6-5-4-8 parts of a fixed column and 6-5-4-9 parts of an adsorption disc spring; the end parts of the left and right swing arms 6-5-4-1 are provided with extending arms 6-5-4-2, the extending arms 6-5-4-2 are rotatably connected with the left and right swing arms 6-5-4-1 and swing up and down by taking the left and right swing arms 6-5-4-1 as rotating shafts, an extending hydraulic machine 6-5-4-3 is arranged between the extending arms and the left and right swing arms, and the extending hydraulic machine 6-5-4-3 is in wireless control connection with the electric cabinet 11; the vertical moving arm 6-5-4-4 is positioned at the end part of the extending arm 6-5-4-2, the vertical moving arm 6-5-4-4 is rotatably connected with the extending arm 6-5-4-2, a vertical hydraulic machine 6-5-4-5 is arranged between the vertical moving arm 6-5-4-4 and the extending arm 6-5-4-2, and the vertical hydraulic machine 6-5-4-5 is in wireless control connection with the electric cabinet 11; the positioning disc 6-5-4-6 is positioned on the lower surface of the vertical moving arm 6-5-4-4, the adsorption disc 6-5-4-7 is arranged below the positioning disc 6-5-4-6, the adsorption disc 6-5-4-7 is fixedly connected with the positioning disc 6-5-4-6 through a fixed column 6-5-4-8, an air pipe is arranged inside the fixed column 6-5-4-8, one end of the air pipe is communicated with a vacuum pump, and the other end of the air pipe is communicated with the adsorption disc 6-5-4-7; one end of the adsorption disc spring 6-5-4-9 is connected with the positioning disc 6-5-4-6, and the other end is connected with the adsorption disc 6-5-4-7.

Further, the washer 6-5-5 includes: cleaning a driving machine 6-5-5-1, a fan 6-5-5-2, a transmission gear 6-5-3, a rotating disk 6-5-5-4, a cleaning brush head 6-5-5 and a clean water pipeline 6-5-5-6; the cleaning driving machine 6-5-5-1 is in wireless control connection with the electric cabinet 11, the output end of the cleaning driving machine 6-5-5-1 is provided with a fan 6-5-5-2, and the surface is dried after cleaning is finished; the transmission gear 6-5-5-3 is positioned below the fan 6-5-5-2, and the transmission gear 6-5-5-3 is meshed with an output main shaft of the cleaning driving machine 6-5-5-1; the rotating disks 6-5-5-4 are positioned on the lower surfaces of the transmission gears 6-5-5-3, the number of the rotating disks 6-5-5-4 is 3, and the cleaning brush heads 6-5-5 are arranged on the lower surfaces of the rotating disks 6-5-5-4; the clean water pipeline 6-5-5-6 is positioned on the upper surface of the transmission gear 6-5-5-3, and the clean water pipeline 6-5-5-6 is communicated with the rotating disc 6-5-5-4.

Further, the holder 14 includes: the support driving machine comprises a support driving machine 14-1, a transmission case 14-2, a support gear 14-3, a support rail 14-4, a support shell 14-5, a counterweight 14-6 and a support body 14-7; the bracket shell 14-5 is positioned at the upper part of the base of the bracket 14 and is independent; the support shell 14-5 is of a hollow structure, and the support track 14-4 is arranged inside the support shell 14-5, is vertical to the base of the support 14 and is fixedly connected with the base; the support body 14-7 is arranged at one side of the transmission case 14-2 and is connected with the transmission case; a bracket gear 14-3 is arranged in the transmission case 14-2 and is meshed and connected with a rack on the surface of the bracket track 14-4; the support body 14-7 is in sliding contact with the bracket track 14-4 through the engagement of the bracket gear 14-3 and the bracket track 14-4; the counterweight body 14-6 is positioned at the outer side of the support body 14-7 and fixed with the support body 14-7, the end part of the counterweight body 14-6 extends out of the support shell 14-5, and the waist part of the counterweight body is fixedly connected with the support shell 14-5; the support driving machine 14-1 is located on one side of the lower end of the transmission case 14-2, the support driving machine 14-1 is in transmission connection with the support gear 14-3, the support driving machine 14-1 is in control connection with the electric cabinet 11 through a lead, and the support driving machine 14-1 drives the support gear 14-3 to rotate and drive the transmission case 14-2, the support shell 14-5, the counterweight body 14-6 and the support body 14-7 to ascend or descend along the support rail 14-4.

Further, the adjustment wheel 15 includes: the oil spray device comprises an adjusting wheel U plate 15-1, a lubricating oil tank 15-2, a movable wheel rotating shaft 15-3, a movable wheel 15-4, an oil nozzle 15-5 and a wheel track 15-6; the U plate 15-1 of the adjusting wheel is of an inverted concave structure and is made of a steel plate, and the side walls on the two sides are in inverted trapezoidal design; the movable wheel rotating shaft 15-3 is connected between the side walls of the two sides of the U-shaped plate 15-1 of the adjusting wheel, the movable wheel rotating shaft 15-3 is in transmission connection with an external motor, and the movable wheel 15-4 is arranged on the movable wheel rotating shaft 15-3; the moving wheel 15-4 is rotationally connected with the moving wheel rotating shaft 15-3, and an external motor of the moving wheel 15-4 is in control connection with the electric cabinet 11 through a wire; the wheel track 15-6 is positioned at the lower part of the moving wheel 15-4 and is in rolling connection with the moving wheel; the lubricating oil tank 15-2 is fixedly connected to the outer portion of the side wall of one side of the adjusting wheel U plate 15-1, the oil nozzle 15-5 is fixedly connected to the inner side of the upper wall of the adjusting wheel U plate 15-1, and the lubricating oil tank 15-2 is connected with the oil nozzle 15-5 through an oil guide pipe inside the lubricating oil tank.

Further, the lubricating oil tank 15-2 includes: 15-2-1 parts of an oil lubricating pump, 15-2-2 parts of a distribution box, 15-2-3 parts of a filter box, 15-2-4 parts of an oil filling pipe, 15-2-5 parts of a radiator, 15-2-6 parts of a fixing plate, 15-2-7 parts of a positioning sleeve and 15-2-8 parts of an oil filling pipe outlet; the lubricating oil pump 15-2-1 positioned at the bottom is communicated with the distribution box 15-2-2 at the upper part, the short shafts at two ends of the rectangular box body 15-2-2 are semicircular, two groups of stirring impellers are arranged in the rectangular box body, the short shafts at two ends of the rectangular box body are different in diameter, the diameter of each large stirring impeller is 30cm, the diameter of each small stirring impeller is 9cm, the large stirring impeller and the small stirring impeller are horizontally arranged side by side and stirred in different directions, two branch pipes extend upwards from the two semicircular end points of the distribution box 15-2-2 and are communicated with the filter box 15-2-3 through valves, the diameters of the two branch pipes are different, the diameter of each thick pipe is 8cm, the diameter of each thin pipe is 2cm, and the thin pipes are respectively arranged; the filter box 15-2-3 is positioned at the upper part of the distribution box 15-2-2 and is communicated with the distribution box 15-2-2, and a filter screen, a settling chamber and a screen impurity remover are arranged in the filter box 15-2-3; the radiator 15-2-5 is positioned at the upper part of the filter box 15-2-3, and the radiator 15-2-5 is made of red copper and is formed by overlapping a plurality of groups of copper plates, and gaps exist among the copper plates; an oil filling pipe 15-2-4 is wound on the outer surface of the radiator 15-2-5, the wound section is made of pressure-resistant red copper, one end of the oil filling pipe 15-2-4 is communicated with the filter box 15-2-3, and the other end of the oil filling pipe penetrates through a positioning sleeve 15-2-7 to be communicated with an outlet 15-2-8 of the oil filling pipe; one end of the fixing plate 15-2-6 is sleeved on the outer surface of the positioning sleeve 15-2-7, and the other end is connected with the fixing wall.

Further, the oil jet 15-5 includes: 15-5-1 parts of a main branch pipe, 15-5-2 parts of a cover shell, 15-5-3 parts of an inclined angle oil injection body and 15-5-4 parts of an oil injection adjusting nozzle; the cover shell 15-5-2 is a hollow inverted circular truncated cone structure with the upper part closed and the bottom opened, a main branch pipe 15-5-1 is arranged right above the cover shell 15-5-2, the bottom end of the main branch pipe 15-5-1 is inserted into the cover shell 15-5-2, and the top end of the main branch pipe 15-5-1 is communicated with an oil guide pipe on the upper part; the inclined angle oil spray bodies 15-5-3 are positioned in the cover surface shell 15-5-2, the number of the inclined angle oil spray bodies 15-5-3 is 4-8, the adjacent inclined angle oil spray bodies 15-5-3 are distributed in an equal angle mode by taking the main branch pipe 15-5-1 as a central shaft, and each inclined angle oil spray body 15-5-3 is communicated with the main branch pipe 15-5-1 through an oil distribution pipe; the oil injection adjusting nozzle 15-5-4 is fixedly connected to the lower part of the cover shell 15-5-2 and can be controlled to adjust the retractable structure, and the injection flow and angle are controlled.

Further, the inclined angle oil jet 15-5-3 includes: 15-5-3-1 parts of an oil inlet, 15-5-3-2 parts of a tangential oil outlet, 15-5-3-3 parts of an oil injection shell, 15-5-3-4 parts of a staggered spoiler, 15-5-3-5 parts of a shell driver and 15-5-3-6 parts of a shell reinforcing hoop; an oil inlet 15-5-3-1 is arranged at the top of the oil injection shell 15-5-3-3, a large number of tangential oil outlets 15-5-3-2 are arranged on the side wall of the oil injection shell 15-5-3-3, and lubricating oil is tangentially sprayed out along the surface of the oil injection shell 15-5-3-3; a large number of staggered spoilers 15-5-3-4 are arranged on the inner wall of the oil injection shell 15-5-3-3 and fixed on the surface of the inner wall in a staggered manner, the staggered spoilers 15-5-3-4 are made of thin stainless steel structures, the length of the staggered spoilers is 4/5 the length of 15-5-3-3 of the oil injection shell, and the height of the staggered spoilers is 1/10 the radius of 15-5-3-3 of the oil injection shell; a shell reinforcing hoop 15-5-3-6 and a shell driver 15-5-3-5 are arranged outside the oil injection shell 15-5-3-3; wherein, the shell drivers 15-5-3-5 are arranged in the upper and lower 2 groups and simultaneously drive the oil injection shell 15-5-3-3 to rotate.

Further, the case driver 15-5-3-5 includes: 15-5-3-5-1 of a shell flange, 15-5-3-5-2 of a first shaft, 15-5-3-5-3 of a circumferential rack, 15-5-3-5-4 of a connecting plate, 15-5-3-5-5 of a horizontal positioning wheel, 15-5-3-5-6 of a circumferential driving wheel and 15-5-3-5-7 of a second shaft; a circumferential rack 15-5-3-5-3 is surrounded outside the oil injection shell 15-5-3-3, and the oil injection shell and the circumferential rack are fixedly connected through a connecting plate 15-5-3-5-4; a group of horizontal positioning wheels 15-5-3-5-5 are respectively arranged above and below the circumferential rack 15-5-3-5-3 to prevent the circumferential driving wheel 15-5-3-5-6 from deviating, and the horizontal positioning wheels 15-5-3-5-5 rotate around a shaft I15-5-3-5-2; two sides of the horizontal positioning wheel 15-5-3-5-5 are respectively provided with a group of circumferential driving wheels 15-5-3-5-6 which are fixedly connected; the second shaft 15-5-3-5-7 drives the circumferential driving wheel 15-5-3-5-6 to rotate, and the circumferential driving wheel 15-5-3-5-6 is in meshed transmission with the circumferential rack 15-5-3-5-3; the shell flange 15-5-3-5-1 realizes the up-and-down butt joint of the oil injection shell 15-5-3-3.

Further, the circumferential rack 15-5-3-5-3 includes: 15-5-3-5-3-1 parts of circumferential tooth surface, 15-5-3-5-3-2 parts of fan-shaped tooth, 15-5-3-5-3-3 parts of oil injection machine, 15-5-3-5-3-4 parts of bottom transverse plate, 15-5-3-5-3-5 parts of damping spring and 15-5-3-5-3-6 parts of air blowing pipe; the circumferential tooth surfaces 15-5-3-5-3-1 are 2 groups, are oppositely arranged and are connected through a bottom transverse plate 15-5-3-5-3-4; fan-shaped teeth 15-5-3-5-3-2 are equidistantly distributed on the surface of the circumferential tooth surface 15-5-3-5-3-1; an oil injection machine 15-5-3-5-3-3 is arranged on the bottom transverse plate 15-5-3-4 and is used for gear meshing lubrication; the damping spring 15-5-3-5-3-5 is fixed on the surface of the bottom transverse plate 15-5-3-5-3-4, and the top of the damping spring is provided with a balancing weight; one end of the air blowing pipe 15-5-3-5-3-6 is in threaded connection with the damping spring 15-5-3-5-3-5 and penetrates through the balancing weight, the damping spring 15-5-3-5 and the bottom transverse plate 15-5-3-4 to extend to the outside, the outlet of the other end of the air blowing pipe is aligned with the fan-shaped teeth 15-5-3-5-3-2, and the air blowing pipe 15-5-3-5-3-6 freely swings along with the vibration of the damping spring 15-5-3-5-3-5.

Further, the oiling machine 15-5-3-5-3-3 includes: 15-5-3-5-3-3-1 protective cover, 15-5-3-5-3-3-2 oil storage bag, 15-5-3-5-3-3 stirring oil separator, 15-5-3-5-3-3-4 filtering round platform box, 15-5-3-5-3-3-5 settling tank, 15-5-3-3-5 overflow pipe, 15-5-3-3-6 overflow pipe, 15-5-3-5-3-3-7 oil-water separator, 15-5-3-5-3-3-8 standing separation tank, 15-5-3-5-3-9 recovery oil pipe, 15-5-3-5-3-3-10 parts of a separation water pipe, 15-5-3-5-3-3-11 parts of a sediment pipe, 15-5-3-5-3-3-12 parts of a metal sediment pipe, 15-5-3-5-3-3-13 parts of an oil inlet pipeline and 15-5-3-5-3-3-14 parts of a threaded oil outlet pipe; an oil inlet channel 15-5-3-5-3-3-13 positioned at the lower part, wherein external oil enters from the oil inlet channel and is communicated with an upper stirring oil separator 15-5-3-5-3-3-3, 2 groups of stirring impellers are arranged in the stirring oil separator 15-5-3-5-3-3-3, the stirring impellers are horizontally distributed and stir at low speed in different directions, the upper part of the stirring impeller at the left side is provided with a channel which is communicated with an oil storage bag 15-5-3-5-3-3-2, the periphery of the oil storage bag 15-5-3-3-2 is provided with a protective cover 15-5-3-3-1, the upper part of the protective cover is provided with a threaded oil outlet pipe 15-5-3-5-3-3-14, the two are communicated; a filtering circular truncated cone box 15-5-3-5-3-3-4 is arranged at the lower part of the left stirring impeller of the stirring oil separator 15-5-3-5-3-3, the filtering circular truncated cone box and the filtering circular truncated cone box are communicated through a guide pipe, and a filtering net is arranged in the filtering circular truncated cone box 15-5-3-5-3-3-4; the sedimentation tank 15-5-3-5-3-3-5 is positioned at the lower part of the filtering circular truncated cone tank 15-5-3-5-3-4 and is communicated with the filtering circular truncated cone tank, the lower part of the right side of the sedimentation tank 15-5-3-5-3-3-5 is provided with a metal sediment pipe 15-5-3-5-3-3-12, the upper part of the left side is provided with an overflow pipe 15-5-3-5-3-6, and an oil inlet of the overflow pipe 15-5-3-5-3-3-6 is always positioned on the surface of the solution in the sedimentation tank 15-5-3-5-3-3-5; the oil-water separator 15-5-3-5-3-3-7 positioned at the lower part is communicated with the settling tank 15-5-3-5-3-3-5 through an overflow pipe 15-5-3-5, the left end part of the oil-water separator is closed, the right end part of the oil-water separator is provided with a sediment pipe 15-5-3-5-3-3-11, the oil-water separator 15-5-3-5-3-3-7 is horizontally inserted into the standing separation box 15-5-3-5-3-8, wherein, the controllable rotation is realized at the insertion section of the static separation box 15-5-3-5-3-3-8, and the surface of the static separation box is provided with a large number of small through holes; the upper part of the standing separation box 15-5-3-5-3-3-8 is provided with a recovery oil pipe 15-5-3-5-3-3-9, and the lower part is provided with a separation water pipe 15-5-3-5-3-3-10.

Further, the stirring oil separator 15-5-3-5-3-3-3 includes: 15-5-3-5-3-3-1 damping spring, 15-5-3-5-3-3-2 stirring wheel I, 15-5-3-5-3-3-3-3 auxiliary paddle and 15-5-3-5-3-3-4 stirring wheel II; a stirring wheel 15-5-3-5-3-3-2 and a stirring wheel II 15-5-3-3-4 are arranged in the stirring oil separator 15-5-3-3-3, and are horizontally arranged and stirred in different directions, wherein an oil inlet passage 15-5-3-5-3-3-4 is arranged at the lower part of the axle center of the stirring wheel II 15-5-3-3-4, a clear oil outlet is arranged at the upper part of the axle center of the stirring wheel I15-5-3-3-3-2, and a waste oil outlet is arranged at the lower part of the axle center of the stirring wheel II 15-5-3-5-3-3-3-2; one end of the interior of the shell of the oil separator 15-5-3-5-3-3-3 is provided with a damping spring 15-5-3-5-3-3-1, and the other end is provided with an auxiliary paddle 15-5-3-5-3-3-3-3, wherein the root of the damping spring 15-5-3-5-3-3-1 is fixed on the shell, and the upper part of the damping spring freely swings; the lower part of the auxiliary paddle 15-5-3-5-3-3-3-3 is provided with a cylinder, one end of the cylinder is rotationally connected with the upper paddle, and the other end of the cylinder is fixed in the oil separator 15-5-3-5-3-3-3 shell.

The invention discloses a preparation device and a preparation method of oxytetracycline, which have the advantages that: the device adopts automatic control, convenient operation, and work is high-efficient steady, and the reaction unit of integration is resistant to load and is strikeed and reduced equipment input, and treatment facility is compact, has practiced thrift the cost effectively.

Drawings

FIG. 1 is a diagram of an apparatus for preparing oxytetracycline in the present invention.

FIG. 2 is a view of a distillation column 5 in the present invention.

FIG. 3 is a view of the tapping control valve 5-2 according to the invention.

FIG. 4 is a diagram of catalytic system 5-4 of the present invention.

Figure 5 is a diagram of a trickle bed reactor 6 according to the present invention.

FIG. 6 is a view of a mixing agitator 6-3 according to the present invention.

FIG. 7 is a diagram of the magnetic demetallizer 6-3-2 of the present invention.

Fig. 8 is a view of an automatic cleaning machine 6-5 according to the present invention.

FIG. 9 is a view of the crawling adsorption device 6-5-4 in the invention.

FIG. 10 is a view of the washer 6-5-5 of the present invention.

Fig. 11 is a view of the bracket 14 of the present invention.

Fig. 12 is a view of the adjustment wheel 15 of the present invention.

Fig. 13 is a view of the lubricating oil tank 15-2 in the invention.

FIG. 14 is a view of an oil jet 15-5 of the present invention.

FIG. 15 is a view of the angled jet 15-5-3 of the present invention.

Fig. 16 is a view of the housing driver 15-5-3-5 of the present invention.

Fig. 17 is a view of circumferential rack 15-5-3-5-3 in accordance with the present invention.

FIG. 18 is a view of the oiling machine 15-5-3-5-3-3 according to the present invention.

FIG. 19 is a view showing an agitation oil separator 15-5-3-5-3-3-3 according to the present invention.

Detailed Description

The device and the method for preparing oxytetracycline provided by the invention are further described below with reference to the accompanying drawings and examples.