Purification equipment for producing and preparing columns of taxus chinensis

文档序号:1884132 发布日期:2021-11-26 浏览:28次 中文

阅读说明:本技术 红豆杉生产制备柱提纯设备 (Purification equipment for producing and preparing columns of taxus chinensis ) 是由 朱久武 喻凯祥 谢方健 于 2021-09-03 设计创作,主要内容包括:本发明涉及红豆杉加工技术领域,具体涉及红豆杉生产制备柱提纯设备;包括支撑组件、两个提纯组件和清理组件,所述清理组件包括反洗泵、水箱、第一水管、两个第二水管、两个清洗环、两个气缸和两个活塞,反洗泵连接水箱和第一水管,第二水管连接第一水管和提纯组件,活塞连接气缸和清洗环,在清理残渣时,反洗泵将水箱内的水抽出,并导入第一水管内,再通过第二水管将水导入提纯组件内冲洗清理残渣,在冲洗的过程中,真空泵运作推动活塞移动,使活塞带动清洗环上下移动,将粘贴在提纯组件内的残渣清理排出,解决现有提纯设备提纯红豆杉后清理不便,残渣影响后续提纯纯度的问题。(The invention relates to the technical field of Chinese yew processing, in particular to a purifying device for a Chinese yew production preparation column; including supporting component, two purification subassemblies and clearance subassemblies, the clearance subassembly includes the backwash pump, the water tank, first water pipe, two second water pipes, two purge rings, two cylinders and two pistons, backwash pump connects water tank and first water pipe, first water pipe of second water piping connection and purification subassembly, piston connection cylinder and purge ring, when the clearance residue, the backwash pump takes out the water in the water tank, and leading-in first water pipe is intraductal, the leading-in purification subassembly of rethread second water pipe will be washed the clearance residue in water, at the in-process that washes, the vacuum pump function promotes the piston and removes, make the piston drive the purge ring reciprocate, the residue clearance discharge in the purification subassembly will be pasted, it is inconvenient to solve clearance behind the purification chinese yew of current purification equipment, the problem of the follow-up purity of residue influence.)

1. The purification equipment for the production and preparation column of the taxus chinensis is characterized in that,

the device comprises a supporting component, a purification component and a cleaning component, wherein the cleaning component comprises a backwashing pump, a water tank, a first water pipe, two second water pipes, two cleaning rings, two air cylinders and two pistons, the backwashing pump is fixedly connected with the water tank and positioned on one side of the water tank, the first water pipe is fixedly connected with the backwashing pump and positioned on one side of the backwashing pump, one sides of the two second water pipes are respectively and fixedly connected with the first water pipe and positioned on one side of the first water pipe, the other sides of the two second water pipes are respectively and fixedly connected with the purification component and positioned on one side of the purification component, the two pistons are respectively and fixedly connected with the two cleaning rings and positioned on one side of the cleaning rings, the two air cylinders are respectively and fixedly connected with the two pistons and respectively and fixedly connected with the purification component and positioned on one side of the purification component, the two cleaning rings are respectively and fixedly connected with the two pistons and are positioned on one side of the piston, which is far away from the cylinder.

2. The purification apparatus for producing column of yew as claimed in claim 1, wherein,

the cleaning assembly further comprises two high-pressure nozzles and two visual mirrors, the two high-pressure nozzles are respectively fixedly connected with the two second water pipes and are all located in the purification assembly, and the two visual mirrors are respectively fixedly connected with the two purification assemblies and are all located at the top of the purification assembly.

3. The purification apparatus for producing column of yew as claimed in claim 1, wherein,

the cleaning assembly further comprises a water quality detector and a filter screen, the filter screen is fixedly connected with the water tank and is located in the water tank, and the water quality detector is fixedly connected with the water tank and is located in the water tank.

4. The purification apparatus for producing column of yew as claimed in claim 1, wherein,

the cleaning ring comprises a connector, a cleaning ring body and a brush layer, the connector is fixedly connected with the piston and is located at the position where the piston is far away from one side of the air pump, the cleaning ring body is fixedly connected with the connector and is located at the position where the connector is far away from one side of the piston, the brush layer is fixedly connected with the cleaning ring body and is located at the position where the cleaning ring body is far away from the purification assembly.

5. The purification apparatus for producing column of yew as claimed in claim 1, wherein,

the support component comprises a base and a support, the base is fixedly connected with the water tank and is positioned on one side of the water tank, and the support is fixedly connected with the base and is fixedly connected with the purification component and is positioned on one side close to the purification component.

6. The purification apparatus for producing column of yew as claimed in claim 5, wherein,

the purification subassembly includes first purification post, pipe and second purification post, first purification post with support fixed connection, and be located support one side, second purification post with support fixed connection, and be located and be close to first purification post one side, the pipe with first purification post body fixed connection, and with second purification post fixed connection, and be located first purification post with between the second purification post.

7. The purification apparatus for producing column of yew as claimed in claim 6, wherein,

the purification assembly further comprises a control valve and a vacuum pump, the vacuum pump is fixedly connected with the first purification column and is positioned on one side of the first purification column, and the control valve is fixedly connected with the guide pipe.

Technical Field

The invention relates to the technical field of Chinese yew processing, in particular to a purifying device for a Chinese yew production preparation column.

Background

At present, separation and purification of taxus chinensis are carried out, and besides primary separation and purification by using silica gel packing, secondary purification by using resin is also needed.

After the existing purification column cannot be cleaned and purified smoothly, the purification column is not convenient to clean, and the residue remains to influence the subsequent purification purity.

Disclosure of Invention

The invention aims to provide purifying equipment for a production and preparation column of taxus chinensis, and aims to solve the problems that the existing purifying equipment is inconvenient to clean after purifying the taxus chinensis, and the subsequent purification purity is influenced by residues.

In order to achieve the purpose, the invention provides a purifying device for a taxus chinensis production and preparation column, which comprises a supporting component, a purifying component and a cleaning component, wherein the cleaning component comprises a backwashing pump, a water tank, a first water pipe, two second water pipes, two cleaning rings, two air cylinders and two pistons, the backwashing pump is fixedly connected with the water tank and is positioned at one side of the water tank, the first water pipe is fixedly connected with the backwashing pump and is positioned at one side of the backwashing pump, one sides of the two second water pipes are respectively and fixedly connected with the first water pipe and are positioned at one side of the first water pipe, the other sides of the two second water pipes are respectively and fixedly connected with the purifying component and are both positioned at one side of the purifying component, the two pistons are respectively and fixedly connected with the two cleaning rings and are both positioned at one side of the cleaning rings, and the two air cylinders are respectively and fixedly connected with the two pistons, and respectively with purification subassembly fixed connection all is located purification subassembly one side, two wash the ring respectively with two piston fixed connection all is located the piston is kept away from cylinder one side the supporting component is right purification subassembly with the clearance subassembly provides support and installation condition, purification subassembly separation purification chinese yew preparation taxol, the clearance subassembly clearance the chinese yew residue in the purification subassembly.

The cleaning assembly further comprises two high-pressure nozzles and two visible mirrors, the two high-pressure nozzles are respectively fixedly connected with the second water pipes and are all located in the purification assembly, the two visible mirrors are respectively fixedly connected with the purification assembly and are all located at the top of the purification assembly, the high-pressure nozzles spray water guided into the second water pipes in a pressurized mode, the cleaning effect on residues is enhanced, and the arrangement of the visible mirrors is convenient for observing whether the residues in the purification assembly are cleaned up or not.

The cleaning assembly further comprises a water quality detector and a filter screen, the filter screen is fixedly connected with the water tank and located in the water tank, the water quality detector is fixedly connected with the water tank and located in the water tank, the filter screen filters water in the water tank, the cleaning effect is prevented from being influenced by the fact that other impurities are contained in cleaning water, and the water quality detector detects whether the cleaning water in the water tank reaches the standard or not.

Wherein, the purge ring includes connector, purge ring body and brush layer, the connector with piston fixed connection just is located the piston and keeps away from air pump one side, purge ring body with connector fixed connection just is located the connector is kept away from piston one side, the brush layer with purge ring body fixed connection just is located and keeps away from purge ring body with between the purification subassembly, the connector is connected purge ring body with the piston, purge ring body removes and makes the brush layer removes, and the clearance is pasted residue in the purification subassembly.

The support assembly comprises a base and a support, the base is fixedly connected with the water tank and is located on one side of the water tank, the support is fixedly connected with the base and is fixedly connected with the purification assembly and is located close to one side of the purification assembly, and the base and the support provide support and installation conditions for the purification assembly and the cleaning assembly.

Wherein, the purification subassembly includes first purification post, pipe and second purification post, first purification post with support fixed connection, and be located support one side, second purification post with support fixed connection, and be located and be close to first purification post one side, the pipe with first purification post body fixed connection, and with second purification post fixed connection, and be located first purification post with between the second purification post, through first purification post with the purification chinese yew is cascaded to the second purification post, pipe connection first purification post with the second purification post.

The purification assembly further comprises a control valve and a vacuum pump, the vacuum pump is fixedly connected with the first purification column and is positioned on one side of the first purification column, the control valve is fixedly connected with the guide pipe, the vacuum pump is pressurized to enable the first purification column and the second purification column to accelerate the purification rate, and the control valve controls the flow rate of the guide pipe. Thereby controlling the purification rate of the second purification column.

Wherein, the purification subassembly still includes the inlet pipe and arranges the material pipe, the inlet pipe with first purification post fixed connection, and be located first purification post one side, arrange the material pipe with second purification post fixed connection, and be located second purification post one side, the leading-in kibbling chinese yew powder of inlet pipe is used for the purification, arrange the taxol after the material pipe discharge purification.

Wherein, purification subassembly still includes the groove of gathering materials, gather the groove with base fixed connection, and be located arrange material pipe one side, the groove of gathering materials is collected arrange material pipe exhaust taxol.

The support component provides support and installation conditions for the purification component and the cleaning component, the purification component separates and purifies the taxus chinensis to prepare paclitaxel, the cleaning component cleans the taxus chinensis residues in the purification component when the residues need to be cleaned after the purification component purifies the taxus chinensis, specifically, the backwashing pump is electrified to pump out water in the water tank and guide the water into the first water pipe, the first water pipe guides the water into the second water pipe, the second water pipe guides the water into the purification component to flush and clean the residues, in the process of flushing the residues, the air cylinder is electrified to drive the piston to move, so that the piston drives the cleaning ring to move up and down, the residues adhered to the inner wall of the purification component are driven by the cleaning ring, and finally the residues and the water are discharged out of the purification component to be completely cleaned, the method disclosed by the invention is full-automatic in cleaning, does not need manual participation, is convenient and fast to clean the taxus chinensis residues, and solves the problems that the existing purification equipment is inconvenient to clean after purifying the taxus chinensis, and the subsequent purification purity is influenced by the residues.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.

FIG. 1 is a schematic structural diagram of a purification apparatus for producing and preparing a column from Taxus chinensis provided in the present invention;

FIG. 2 is a front view of a purification apparatus for producing and preparing columns of Taxus chinensis provided in the present invention;

FIG. 3 is a side view of a purification apparatus for producing and preparing columns of Taxus chinensis provided in the present invention;

FIG. 4 is a cross-sectional view taken along plane A-A of FIG. 3;

fig. 5 is an enlarged view of detail B of fig. 1.

In the figure: 1-supporting component, 2-purifying component, 3-cleaning component, 11-base, 12-bracket, 21-first purifying column, 22-guide pipe, 23-second purifying column, 24-control valve, 25-vacuum pump, 26-feeding pipe, 27-discharging pipe, 28-collecting groove, 31-backwashing pump, 32-water tank, 33-first water pipe, 34-second water pipe, 35-cleaning ring, 36-cylinder, 37-piston, 38-high pressure nozzle, 39-visible mirror, 310-water quality detector, 311-filter screen, 351-cleaning ring body, 352-brush layer and 353-connector.

Detailed Description

Reference will now be made in detail to embodiments of the present invention, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are illustrative and intended to be illustrative of the invention and are not to be construed as limiting the invention.

In the description of the present invention, it is to be understood that the terms "length", "width", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships illustrated in the drawings, and are used merely for convenience in describing the present invention and for simplicity in description, and do not indicate or imply that the devices or elements referred to must have a particular orientation, be constructed in a particular orientation, and be operated, and thus, are not to be construed as limiting the present invention. Further, in the description of the present invention, "a plurality" means two or more unless specifically defined otherwise.

Referring to fig. 1 to 5, the invention provides a purification apparatus for a taxus chinensis production preparation column, comprising a support assembly 1, a purification assembly 2 and a cleaning assembly 3, wherein the cleaning assembly 3 comprises a backwash pump 31, a water tank 32, a first water pipe 33, two second water pipes 34, two cleaning rings 35, two cylinders 36 and two pistons 37, the backwash pump 31 is fixedly connected with the water tank 32 and is positioned at one side of the water tank 32, the first water pipe 33 is fixedly connected with the backwash pump 31 and is positioned at one side of the backwash pump 31, one sides of the two second water pipes 34 are respectively fixedly connected with the first water pipe 33 and are positioned at one side of the first water pipe 33, the other sides of the two second water pipes 34 are respectively fixedly connected with the purification assembly 2 and are positioned at one side of the purification assembly 2, the two pistons 37 are respectively fixedly connected with the two cleaning rings 35, all be located wash ring 35 one side, two cylinder 36 respectively with two piston 37 fixed connection, and respectively with purification subassembly 2 fixed connection, all be located purification subassembly 2 one side, two wash ring 35 respectively with two piston 37 fixed connection, all be located piston 37 keeps away from cylinder 36 one side.

In this embodiment, the supporting component 1 provides supporting and mounting conditions for the purifying component 2 and the cleaning component 3, the purifying component 2 separates and purifies taxus chinensis to prepare paclitaxel, when the purifying component 2 needs to clean residues after purifying taxus chinensis, the cleaning component 3 cleans the taxus chinensis residues in the purifying component 2, specifically, the backwash pump 31 is electrified to pump water in the water tank 32 out and guide the water into the first water pipe 33, the first water pipe 33 guides the water into the second water pipe 34, the second water pipe 34 guides the water into the purifying component 2 to flush and clean the residues, in the process of flushing the residues, the air cylinder 36 is electrified to push the piston 37 to move, so that the piston 37 drives the cleaning ring 35 to move up and down, so that the cleaning ring 35 can flush the residues adhered to the inner wall of the purifying component 2, and finally, discharging the residue and water out of the purification assembly 2 together for complete cleaning, wherein the method is full-automatic cleaning, does not need manual participation, is convenient and fast to clean the taxus chinensis residue, and solves the problems that the existing purification equipment is inconvenient to clean after purifying the taxus chinensis, and the subsequent purification purity is influenced by the residue.

Further, the cleaning assembly 3 further includes two high pressure nozzles 38, two visible mirrors 39, a water quality detector 310 and a filter screen 311, wherein the two high pressure nozzles 38 are respectively fixedly connected to the two second water pipes 34 and are located in the purification assembly 2, the two visible mirrors 39 are respectively fixedly connected to the two purification assemblies 2 and are located at the top of the purification assembly 2, the filter screen 311 is fixedly connected to the water tank 32 and is located in the water tank 32, the water quality detector 310 is fixedly connected to the water tank 32 and is located in the water tank 32, the cleaning ring 35 includes a connector 353, a cleaning ring body 351 and a brush layer 352, the connector 353 is fixedly connected to the piston 37 and is located at a position where the piston 37 is far away from the air pump 36, the cleaning ring body 351 is fixedly connected to the connector 353 and is located at a position where the connector 353 is far away from one side of the piston 36, brush layer 352 is fixedly attached to purge ring body 351 and is positioned between purge ring body 351 and purifier module 2.

In this embodiment, through the high pressure nozzle 38 will the leading-in water pressurization blowout of second water pipe 34 strengthens the clearance effect to the residue, but the setting of visual mirror 39 is convenient for observe whether the residue in purification subassembly 2 is clean up, filter screen 311 filters water in the water tank 32 prevents to contain all the other impurity in the cleaning water and influences the clearance effect, water quality testing appearance 310 detects whether the cleaning water reaches standard in the water tank 32, connector 353 connects wash ring body 351 with piston 37, wash ring body 351 removes and makes brush layer 352 removes, the clearance paste the residue in purification subassembly 2, brush layer 352 is made by artificial fiber.

Further, supporting component 1 includes base 11 and support 12, base 11 with water tank 32 fixed connection, and be located water tank 32 one side, support 12 with base 11 fixed connection, and with purification subassembly 2 fixed connection, and be located and be close to purification subassembly 2 one side.

In this embodiment, base 11 and frame 12 provide support and mounting conditions for purifier assembly 2 and cleaning assembly 3.

Further, the purifying assembly 2 comprises a first purifying column 21, a conduit 22, a second purifying column 23, a control valve 24, a vacuum pump 25, a feeding pipe 26, a discharging pipe 27 and a collecting tank 28, wherein the first purifying column 21 is fixedly connected with the bracket 12 and positioned on one side of the bracket 12, the second purifying column 23 is fixedly connected with the bracket 12 and positioned on one side close to the first purifying column 21, the conduit 22 is fixedly connected with the body of the first purifying column 21 and fixedly connected with the second purifying column 23 and positioned between the first purifying column 21 and the second purifying column 23, the vacuum pump 25 is fixedly connected with the first purifying column 21 and positioned on one side of the first purifying column 21, the control valve 24 is fixedly connected with the conduit 22, the feeding pipe 26 is fixedly connected with the first purifying column 21 and positioned on one side of the first purifying column 21, arrange material pipe 27 with second purification post 23 fixed connection, and be located second purification post 23 one side, material collecting groove 28 with base 11 fixed connection, and be located arrange material pipe 27 one side.

In this embodiment, the first purifying column 21 and the second purifying column 23 are used for purifying the taxus chinensis in a cascade manner, the conduit 22 is connected with the first purifying column 21 and the second purifying column 23, the vacuum pump 25 pressurizes to enable the first purifying column 21 and the second purifying column 23 to accelerate the purifying rate, the control valve 24 controls the flow rate of the conduit 22 so as to control the purifying rate of the second purifying column 23, the feeding pipe 26 guides the smashed taxus chinensis powder for purification, and the discharging pipe 27 discharges the purified taxol to be collected through the collecting groove 28.

The purification device comprises a support component 1, two purification components 2 and a cleaning component 3, wherein the support component 1 comprises a base 11 and a bracket 12, the purification component 2 comprises a first purification column 21, a guide pipe 22, a second purification column 23, a control valve 24, a vacuum pump 25, a feeding pipe 26, a discharging pipe 27 and a collecting tank 28, the cleaning component 3 comprises a backwashing pump 31, a water tank 32, a first water pipe 33, two second water pipes 34, two cleaning rings 35, two cylinders 36, two pistons 37, two high-pressure nozzles 38, two visible mirrors 39, a water quality detector 310 and a filter screen 311, the cleaning rings 35 comprise cleaning ring bodies 351, brush layer connectors 352 and 353, the base 11 and the bracket 12 provide support and installation conditions for the purification components 2 and the cleaning component 3, the feeding pipe 26 introduces crushed red cedar powder for purification, the first purifying column 21 and the second purifying column 23 perform cascade purification of the taxus chinensis, the vacuum pump 25 and the control valve 24 control, the purification rate of the first purifying column 21 and the second purifying column 23, the purified paclitaxel discharged from the discharging pipe 27 is collected by the collecting tank 28, the water in the water tank 32 is filtered by the filter screen 311 to prevent the cleaning water containing other impurities from affecting the cleaning effect, the water quality detector 310 detects whether the cleaning water in the water tank 32 reaches the standard, when the first purifying column 21 and the second purifying column 23 purify and clean the residue, the backwashing pump 31 is electrified to pump the water in the water tank 32 and guide the water into the first water pipe 33, the first water pipe 33 guides the water into the second water pipe 34, the second water pipe 34 guides the water into the high-pressure nozzle 38, and the high-pressure nozzle 38 sprays water to flush and clean the residue, the high-pressure spray head 38 pressurizes and sprays water to enhance the cleaning effect on the residues, and in the process of washing the residues, the air cylinder 36 is electrified to operate to push the piston 37 to move, so that the piston 37 drives the cleaning ring body 351 to move up and down, and the brush layer 352 discharges the residues adhered to the inner wall of the purification assembly 2 and finally the residues and the water out of the purification assembly 2 for complete cleaning.

While the invention has been described with reference to a preferred embodiment, it will be understood by those skilled in the art that various changes in form and detail may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.

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