阅读说明：本技术 一种二聚体及多聚体臭氧油膏的制备方法 (Preparation method of dimer and polymer ozone ointment ) 是由 万炜 万明 苏天健 侯哲 于 2019-08-20 设计创作，主要内容包括：本发明涉及一种二聚体及多聚体臭氧油膏的制备方法,具体包括以下步骤：1)打开耐压反应罐的进料口,关闭岀料阀,将植物油投入到耐压反应罐中,关闭进料口；2)启动电解水臭氧发生器制备高浓度臭氧气体,启动注射泵；3)启动反应罐的搅拌器和齿轮泵；4)打开岀料阀,将高粘稠膏状二聚体及多聚体臭氧油膏包装入桶,关闭反应罐的搅拌器、关闭齿轮泵。本发明优点在于：臭氧油膏携带方便不渗漏；由于臭氧油膏的粘度浓稠,臭氧油膏中的臭氧气体也不会从臭氧油膏中溢出,可长期保证臭氧油膏中的臭氧含量不降低,从而延长了臭氧油膏的储存和使用时间,使臭氧油膏具备长效缓释的作用。(The invention relates to a preparation method of dimer and polymer ozone ointment, which specifically comprises the following steps: 1) opening a feed inlet of the pressure-resistant reaction tank, closing a discharge valve, putting vegetable oil into the pressure-resistant reaction tank, and closing the feed inlet; 2) starting an electrolyzed water ozone generator to prepare high-concentration ozone gas, and starting an injection pump; 3) starting a stirrer and a gear pump of the reaction tank; 4) opening a discharge valve, packaging the high-viscosity thick paste-like dimer and the polymer ozone ointment into a barrel, closing a stirrer of the reaction tank, and closing a gear pump. The invention has the advantages that: the ozone ointment is convenient to carry and does not leak; because the viscosity of the ozone ointment is thick, ozone gas in the ozone ointment can not overflow from the ozone ointment, and the ozone content in the ozone ointment can be ensured not to be reduced for a long time, so that the storage and use time of the ozone ointment is prolonged, and the ozone ointment has a long-acting slow-release effect.)

1. a method for preparing dimer and polymer ozone ointment is characterized by comprising the following steps:

1) opening a feed inlet of the pressure-resistant reaction tank, closing a discharge valve, putting vegetable oil into the pressure-resistant reaction tank, and closing the feed inlet;

2) Starting an electrolyzed water ozone generator to prepare high-concentration ozone gas at normal temperature, starting an injection pump, pressurizing the high-concentration ozone gas generated by the electrolyzed water ozone generator through the injection pump, and then feeding the high-concentration ozone gas into a spiral sheet type pipeline static mixer;

3) Starting the stirrer and gear pump of the reaction tank, pressurizing the vegetable oil in the reaction tank by the gear pump, and introducing the pressurized vegetable oil and the high-concentration vegetable oil by the injection pump

mixing ozone gas, high-speed turbulently mixing in a helical-blade pipeline static mixer, reacting in a pipeline reactor, reacting high-concentration purified ozone gas with vegetable oil fatty acid ester under pressure to generate peroxide, reacting the generated peroxide with vegetable oil fatty acid alkylene to make fatty acid alkylene in liquid single vegetable oil undergo the addition polymerization to generate dimer and polymer vegetable ointment,

The ozone gas reacts with the vegetable oil to generate ozone oil, the material passing through the pipeline reactor flows into the pressure-resistant reaction tank to be circulated repeatedly,

The content of the dimer and the polymer ozone ointment is increased after each circulation until the ozone content in the ozone ointment reaches a specified index and the viscosity of the ozone ointment reaches the specified index, then the ozone gas injection pump is turned off and the electrolytic water ozone generator is turned off;

4) opening a discharge valve, packaging the high-viscosity thick paste-like dimer and the polymer ozone ointment into a barrel, closing a stirrer of the reaction tank, and closing a gear pump.

2. The method of claim 1, wherein the high concentration ozone gas has an ozone gas concentration of 20-35%.

3. the method of claim 1, wherein the reaction pressure in step 3) is less than 5 MPa.

4. The method of claim 1, wherein the reaction temperature in step 3) is less than 50 ℃.

Technical Field

the invention relates to a method for preparing dimer and polymer ozone ointment

background

Ozone is also called as triatomic oxygen, is a natural oxidant, is a known broad-spectrum long-acting, quick, efficient, antibacterial, strong, safe and secondary pollution-free sterilizing gas, has a killing rate of over 99.99 percent on various bacteria, viruses, fungi, molds, mycoplasma, escherichia coli, streptococcus and staphylococcus aureus, and has the same killing effect on hepatitis viruses, SARS viruses, cold viruses, polio viruses and AIDS viruses. This is not comparable to any other antibiotic, antiviral drug and disinfectant. The ozone oil is a pure natural mixture generated by reacting pure ozone gas with edible vegetable oil by using an ozone curing technology. The ozone oil comprises the following components: ozone, edible vegetable oil, and ozone adduct. The ozone oil can be applied to the skin and mucous membrane in the aspects of antibiosis, antiphlogosis, itching relieving, detoxification and the like; the ozone oil has broad-spectrum sterilization, rapidness, safety, penetrability and no drug resistance, promotes blood circulation of focus parts, strengthens metabolism, seals wounds, prevents bacterial infection, eliminates inflammatory reaction, improves immune function and has no toxic or side effect; at present, the ozone oil is widely applied to departments such as gynecology, surgery, dermatology, pain department, burn and scald department and the like by gradually replacing antibiotics and hormones in medicine, and meanwhile, the ozone oil also becomes a common external medicament in families of people. However, the ozone oil is oily liquid in appearance, and is easy to flow and drip when being coated on the surface of human skin; when carrying ozone oil, if the packaging bottle is not sealed tightly, the ozone oil is easy to leak from the bottle; due to the low viscosity of the oily liquid, ozone gas in the ozone oil is easy to volatilize and overflow from the oil, so that the ozone content in the ozone oil is reduced, and the storage and use time of the ozone oil is shortened. The popularization and the application of the ozone oil are influenced by the problems of the currently prepared ozone oil.

disclosure of Invention

the invention aims to provide a preparation method of dimer and polymer ozone ointment, which aims to solve the problems in the background technology.

In order to solve the technical problems, the technical scheme provided by the invention is as follows: a method for preparing dimer and polymer ozone ointment specifically comprises the following steps:

1) opening a feed inlet of the pressure-resistant reaction tank, closing a discharge valve, putting vegetable oil into the pressure-resistant reaction tank, and closing the feed inlet;

2) Starting an electrolyzed water ozone generator to prepare high-concentration ozone gas at normal temperature, starting an injection pump, pressurizing the high-concentration ozone gas generated by the electrolyzed water ozone generator through the injection pump, and then feeding the high-concentration ozone gas into a spiral sheet type pipeline static mixer;

3) Starting a stirrer and a gear pump of a reaction tank, pressurizing vegetable oil in the reaction tank through the gear pump, mixing the pressurized vegetable oil with high-concentration ozone gas introduced by an injection pump, then feeding the mixture into a spiral sheet type pipeline static mixer for high-speed turbulent flow mixing, feeding the mixture into a pipeline reactor, reacting the high-concentration pure ozone gas with vegetable oil fatty acid ester under a pressure condition to generate peroxide, reacting the generated peroxide with vegetable oil fatty acid olefin, enabling the fatty acid olefin in liquid single vegetable oil to generate dimer and polymer vegetable ointment through addition polymerization, simultaneously reacting the ozone gas with the vegetable oil to generate ozone oil, feeding the material passing through the pipeline reactor into a pressure-resistant reaction tank, and circulating repeatedly, wherein the content of the dimer and polymer ozone ointment is increased once per circulation until the ozone content in the ozone ointment reaches a specified index and the viscosity of the ozone ointment reaches the specified index, and then closing the ozone injection pump until the ozone content in the ozone ointment reaches the specified index, Turning off the electrolyzed water ozone generator;

4) Opening a discharge valve, packaging the high-viscosity thick paste-like dimer and the polymer ozone ointment into a barrel, closing a stirrer of the reaction tank, and closing a gear pump.

Preferably, the high-concentration ozone gas has an ozone gas concentration of 20 to 35%.

Preferably, the reaction pressure in the step 3) is 5MPa or less.

Preferably, the reaction temperature in the step 3) is 50 ℃ or lower.

The invention has the advantages that: the ozone ointment provided by the invention has broad bactericidal spectrum, rapidness, safety, penetrability and no drug resistance, promotes blood circulation of focus parts, strengthens metabolism, seals wounds, prevents bacterial infection, eliminates inflammatory reaction, improves immune function, has no toxic or side effect, and has the advantages of no flowing and no dripping of the ozone ointment smeared on the surface of human skin; the ozone ointment is convenient to carry and does not leak; because the viscosity of the ozone ointment is thick, ozone gas in the ozone ointment can not overflow from the ozone ointment, and the ozone content in the ozone ointment can be ensured not to be reduced for a long time, so that the storage and use time of the ozone ointment is prolonged, and the ozone ointment has a long-acting slow-release effect.

Detailed Description

the invention is illustrated below by means of specific examples, without being restricted thereto.