Production equipment and process for gas-melting continuous-drawing quartz rod
阅读说明:本技术 一种气熔连拉石英棒的生产设备及工艺 (Production equipment and process for gas-melting continuous-drawing quartz rod ) 是由 花宁 王友军 徐肖飞 秦建鸿 李怀阳 隋镁深 孔敏 于 2019-12-18 设计创作,主要内容包括:本发明特指一种气熔连拉石英棒的生产设备及工艺,属于石英棒生产技术领域,包括炉体、熔池和牵引机,所述熔池设置于炉体内,所述炉体的顶端设置有用于进料的石英灯,所述熔池位于石英灯正下方,所述熔池的底部设置有下料口,所述牵引机位于炉体的下方,且牵引机上设置有引杆,所述引杆上移至下料口,并与下料口对接。实现一步法拉制石英棒,缩短了生产周期,并且通过燃烧控制装置能够将温度的变化控制在合理的范围,减少了重复加热的能源消耗,提高了熔拉石英棒的得料率,节约了成本;避免了对熔池直接加热进行石英砂的熔制,延长了熔池的使用寿命。(The invention relates to production equipment and a process for gas-smelting continuous-pulling quartz rods, belonging to the technical field of quartz rod production. The quartz rod is drawn by a one-step method, the production period is shortened, the change of the temperature can be controlled in a reasonable range by the combustion control device, the energy consumption of repeated heating is reduced, the material yield of the melt-drawn quartz rod is improved, and the cost is saved; the direct heating of the molten pool is avoided to melt the quartz sand, and the service life of the molten pool is prolonged.)
1. The utility model provides a production facility of gas-melt even draw quartz rod, includes furnace body, molten bath and tractor, the molten bath sets up in the furnace body, its characterized in that: the top of furnace body is provided with the quartz lamp that is used for the feeding, the molten bath is located under the quartz lamp, the bottom of molten bath is provided with the feed opening, the tractor is located the below of furnace body, and is provided with the guide rod on the tractor, the guide rod shifts up to the feed opening to dock with the feed opening.
2. The apparatus for producing a gas-fuse pulled quartz rod according to claim 1, characterized in that: one end of the quartz lamp is a combustion part, the other end of the quartz lamp is a feeding part, and the feeding part comprises a gas conveying pipe and a quartz sand feeding pipe.
3. The apparatus for producing a gas-fuse pulled quartz rod according to claim 2, characterized in that: the gas conveying pipe consists of an oxygen conveying pipe and a hydrogen conveying pipe which are respectively connected with a gas source.
4. The apparatus for producing a gas-fuse pulled quartz rod according to claim 3, characterized in that: the furnace body is provided with an observation port and a temperature measuring port.
5. The apparatus for producing a gas-fuse pulled quartz rod according to claim 4, characterized in that: the lower part of the furnace body is provided with an air suction opening, and the air suction opening is provided with an exhaust fan.
6. The apparatus for producing a gas-fuse pulled quartz rod according to claim 5, characterized in that: the furnace body is also provided with a combustion control device, the combustion control device comprises an ignition device, a gas control device and a monitoring device, and the ignition device, the gas control device and the monitoring device are electrically connected.
7. The apparatus for producing a gas-fuse pulled quartz rod according to claim 6, characterized in that: the ignition device comprises an igniter and a spark plug, and the spark plug is arranged at the combustion part of the quartz lamp and is close to the gas outlet of the hydrogen conveying pipe; the gas control device comprises a plurality of pneumatic valves and linear valves capable of adjusting opening degree, the pneumatic valves are respectively arranged on pipelines of the oxygen conveying pipe and the hydrogen conveying pipe, and the linear valves are arranged on the pipelines of the hydrogen conveying pipe; the monitoring device comprises a temperature sensor arranged at the temperature measuring port.
8. The apparatus for producing a gas-fuse pulled quartz rod according to claim 1, characterized in that: the furnace body comprises three-layer structure, and the inlayer is the corundum flame retardant coating, and the intermediate level is the main part layer of adopting the chamotte to build, and the skin is the heat preservation that adopts the cotton formation of heat preservation.
9. The apparatus for producing a gas-fuse pulled quartz rod according to claim 8, characterized in that: and a water cooling circulation system is arranged at the bottom of the furnace body.
10. The process for producing a gas-fuse continuous-pulling quartz rod according to claim 7, wherein the combustion control device is controlled by a PLC, and the process steps are as follows: s1: starting a combustion control device, starting a pneumatic valve, and igniting and combusting hydrogen and oxygen after the hydrogen and the oxygen are converged at a combustion part of the quartz lamp;
s2: the linear valve adjusts the delivery quantity of the hydrogen;
s3: a temperature sensor at the temperature measuring port monitors the temperature of the furnace body, and when the temperature T is less than 1725 ℃, the linear valve adjusts the delivery capacity of the hydrogen;
s4: when the temperature T of the furnace body is monitored to be higher than 2100 ℃, an exhaust fan at an air suction port is started, and exhaust air is cooled;
s5: monitoring the temperature of the furnace body again, and returning to the step S2 to continue to execute when the temperature T is more than 2100 ℃;
s6: when the temperature T of the furnace body is monitored to be between 1725 and 2100 ℃, quartz sand starts to be conveyed to a combustion part of a quartz lamp for heating;
s7: the quartz sand is heated to form fused quartz glass, the fused quartz glass enters a molten pool, and after the guide rod is fused with the fused quartz glass, the traction machine drives the guide rod to descend at a constant speed and the fused quartz glass is drawn into a quartz rod.
Technical Field
The invention belongs to the technical field of quartz rod production, and particularly relates to production equipment and a process for gas melting continuous drawing of a quartz rod.
Background
The existing gas-refining quartz glass process is to melt quartz sand by oxyhydrogen flame to prepare a quartz lead with the diameter of 250-1000mm, and the main mode is to heat the quartz sand at high temperature to change the quartz sand into fused quartz glass and form the quartz lead after cooling. The diameter of the quartz rod used in the optical fiber manufacturing industry is mainly 10-100mm, so that the quartz rod is prepared by heating, melting and pulling the quartz block. The process has several problems: firstly, two procedures are needed to realize the production of the product quartz rod, and the period is longer; secondly, a large amount of electric power and graphite consumables are consumed in the fusion drawing process, so that the cost is high; third, production discontinuity and a great deal of quartz product waste are caused, because the fused quartz glass in the graphite crucible is remained after each melting and pulling, and the yield is only 40% -65%.
According to Chinese classification number: TK175, literature identifier: a, article number: the 1001-5523(2017)06-0032-05 discloses that the temperature of the quartz sand reaching the molten state is about 1725 ℃, and when the temperature is lower than the temperature, the viscosity of the quartz glass in the molten state is too high, so that the discharging is not smooth, and the pulling of a quartz rod is influenced; when the temperature is too high, the drawing and forming of the quartz rod are also affected.
Disclosure of Invention
The invention aims to provide production equipment and a production process for a gas melting continuous-drawing quartz rod, which can be used for forming the quartz rod in one step.
The purpose of the invention is realized as follows: the utility model provides a gas-smelting is even draws production facility of quartz rod, includes furnace body, molten bath and tractor, the molten bath sets up in the furnace body, and the molten bath is the zirconia molten bath, wherein, the top of furnace body is provided with the quartz lamp that is used for the feeding, the molten bath is located under the quartz lamp, the bottom of molten bath is provided with the feed opening, the tractor is located the below of furnace body, and is provided with the pin on the tractor, the pin shifts up to the feed opening to dock with the feed opening.
According to the scheme, high-temperature heating of quartz sand is directly completed on the quartz lamp, the quartz sand processed by the quartz lamp at high temperature is changed into quartz glass in a molten state, then the quartz glass falls into the molten pool, then the quartz glass in the molten pool is pulled out from the feed opening at a constant speed through the guide rod to prepare the quartz rod, the quartz glass collected in the molten pool in the molten state is in a relatively stable state through the melting amount of the quartz sand and the control of the temperature, and the circulating state that the guide rod can stably pull the quartz rod is achieved.
Further: one end of the quartz lamp is a combustion part, the other end of the quartz lamp is a feeding part, and the feeding part comprises a gas conveying pipe and a quartz sand feeding pipe.
In the scheme, hydrogen, oxygen and quartz sand enter from the feeding part of the quartz lamp, and the quartz sand is melted in the combustion part of the quartz lamp to prepare fused quartz glass, so that the quartz glass is conveniently drawn after falling into a molten pool, and the production period is greatly shortened.
Further: the gas conveying pipe consists of an oxygen conveying pipe and a hydrogen conveying pipe which are respectively connected with a gas source.
Adopt hydrogen and oxygen as the heat source of heating in this scheme, direct and quartz sand contact and heating can improve the efficiency of heating, avoid thermal loss, and hydrogen and oxygen can save the cost as fuel moreover, prevent the pollution to the environment.
Further: the furnace body is provided with an observation port and a temperature measuring port.
The scheme is mainly convenient for observing the melting state of the quartz glass in the furnace body and monitoring the temperature change in the furnace body.
Further: the lower part of the furnace body is provided with an air suction opening, and the air suction opening is provided with an exhaust fan.
The exhaust fan can reduce the temperature in the furnace body and keep the temperature and the pressure in the furnace body stable.
Further: the furnace body is also provided with a combustion control device, the combustion control device comprises an ignition device, a gas control device and a monitoring device, and the ignition device, the gas control device and the monitoring device are electrically connected. The combustion control device can control the temperature in the furnace body, ensure the temperature stability and is beneficial to drawing the quartz rod.
Further: the ignition device comprises an igniter and a spark plug, and the spark plug is arranged at the combustion part of the quartz lamp and is close to the gas outlet of the hydrogen conveying pipe; the gas control device comprises a plurality of pneumatic valves and linear valves capable of adjusting opening degree, the pneumatic valves are respectively arranged on pipelines of the oxygen conveying pipe and the hydrogen conveying pipe, and the linear valves are arranged on the pipelines of the hydrogen conveying pipe; the monitoring device comprises a temperature sensor arranged at the temperature measuring port.
Further: the furnace body comprises three-layer structure, and the inlayer is the corundum flame retardant coating, and the intermediate level is the main part layer of adopting the chamotte to build, and the skin is the heat preservation that adopts the cotton formation of heat preservation.
Further: and a water cooling circulation system is arranged at the bottom of the furnace body.
Further, the combustion control device is controlled by a PLC, and the process steps are as follows: s1: starting a combustion control device, starting a pneumatic valve, and igniting and combusting hydrogen and oxygen after the hydrogen and the oxygen are converged at a combustion part of the quartz lamp;
s2: the linear valve adjusts the delivery quantity of the hydrogen;
s3: a temperature sensor at the temperature measuring port monitors the temperature of the furnace body, and when the temperature T is less than 1725 ℃, the linear valve adjusts the delivery capacity of the hydrogen;
s4: when the temperature T of the furnace body is monitored to be higher than 2100 ℃, an exhaust fan at an air suction port is started, and exhaust air is cooled;
s5: monitoring the temperature of the furnace body again, and returning to the step S2 to continue to execute when the temperature T is more than 2100 ℃;
s6: when the temperature T of the furnace body is monitored to be between 1725 and 2100 ℃, quartz sand starts to be conveyed to a combustion part of a quartz lamp for heating;
s7: the quartz sand is heated to form fused quartz glass, the fused quartz glass enters a molten pool, and after the guide rod is fused with the fused quartz glass, the traction machine drives the guide rod to descend at a constant speed and the fused quartz glass is drawn into a quartz rod.
Compared with the prior art, the invention has the outstanding and beneficial technical effects that: the quartz rod can be molded in one step, so that the energy consumption of repeated heating is reduced, the material yield of the fusion-drawn quartz rod is improved, the production period is shortened, and the cost is saved; the direct heating of the molten pool is avoided to melt the quartz sand, and the service life of the molten pool is prolonged.
Drawings
FIG. 1 is a schematic view of the construction of a production apparatus in the present invention;
FIG. 2 is a logic diagram of PLC control in the present invention;
FIG. 3 is a main circuit diagram of the combustion control apparatus of the present invention;
FIG. 4 is a circuit diagram of the PWM control of the present invention;
in the figure: 10-a furnace body; 101-corundum refractory layer; 102-a body layer; 103-an insulating layer; 104-a viewing port; 105-temperature measuring port; 106-air suction inlet; 107-water cooling circulation system; 11-a molten bath; 111-a feed opening; 12-a tractor; 121-a leader; 13-quartz lamp; 131-a combustion section; 132-quartz sand feed tube; 133-oxygen delivery pipe; 134-hydrogen conveying pipe; 14-a rectifier circuit; 15-igniter.
Detailed Description
The invention will be further described in the following with reference to specific embodiments thereof, with reference to the accompanying drawings, in which figures 1 to 4:
a production device of a gas-melting continuous-pulling quartz rod comprises a
the
After the quartz rod is pulled to the bottom, chuck claws for fixing the guide rods are loosened, quickly ascend to the position of the bottom of the furnace body along with a tractor and are clamped, then the quartz rod below is cut off, and the operation is repeated to realize continuous drawing.
In order to keep the temperature in the furnace body stable, a combustion control device is further arranged on the furnace body and controlled by a PLC (programmable logic controller), and the combustion control device comprises an ignition device, a gas control device and a monitoring device which are electrically connected. The combustion control device can control the temperature in the furnace body, ensure the temperature stability and is beneficial to drawing the quartz rod.
The ignition device comprises an igniter and a spark plug, wherein the spark plug (not shown in the figure) is arranged in the combustion part of the quartz lamp and is close to the gas outlet of the hydrogen conveying pipe; the gas control device comprises two pneumatic valves and a linear valve capable of adjusting the opening degree, the pneumatic valves are respectively arranged on the pipelines of the oxygen conveying pipe and the hydrogen conveying pipe, and the linear valve is arranged on the pipeline of the hydrogen conveying pipe; the monitoring device comprises a temperature sensor (not shown in the figure) arranged at the temperature measuring port.
The combustion control device of the present invention is such that the switch SW1 passing through the power source terminal L is connected to the input terminal of the
FIG. 4 is a circuit diagram of the PWM control circuit of the present invention. As shown in fig. 4, a Pulse Width Modulation (PWM) signal from the control chip is divided by resistors R1 and R2 to become a turn-on signal of the transistor Q1. The transistor Q1 is turned on to a different degree depending on the magnitude of the Pulse Width Modulation (PWM) signal. The operating state of the transistor Q1 determines the degree of conduction of the other transistor Q2 connected thereto. Transistor Q2 is connected directly to the 12 volt dc power supply and its operating state, in turn, determines the magnitude of the dc voltage provided to
The production process of the present invention is further understood by combining a specific control method, as shown in fig. 2. The method comprises the following specific steps:
s1: starting a combustion control device, wherein a rectification power supply in a
s2: the linear valve adjusts the delivery quantity of the hydrogen;
s3: the temperature sensor of the temperature measuring port monitors the temperature of the furnace body and sends a measured signal to the control chip, when the temperature T is less than 1725 ℃, a Pulse Width Modulation (PWM) signal controlled by the control chip is increased to provide voltage for the
s4: when the temperature T of the furnace body is more than 2100 ℃, the control chip controls the exhaust fan of the
s5: monitoring the temperature of the furnace body again, and returning to the step S2 to continue to execute when the temperature T is more than 2100 ℃;
s6: when the temperature T of the furnace body is monitored to be between 1725 and 2100 ℃, quartz sand starts to be conveyed to a combustion part of a quartz lamp for heating;
s7: the quartz sand is heated to form fused quartz glass, the fused quartz glass enters a molten pool, and after the guide rod is fused with the fused quartz glass, the traction machine drives the guide rod to descend at a constant speed and the fused quartz glass is drawn into a quartz rod.
Through foretell production technology can realize one-step method drawing quartz rod, production cycle has been shortened, and can be with the change control of temperature in reasonable scope, through in time adjustment temperature, remain throughout in the most suitable temperature range when making quartz sand founding, and through exhaust fan and combustion control device's cooperation, the product of burning in the furnace body of timely emission, not only stabilized the pressure in the furnace body, and solved hydrogen burning and made the hydroxyl unstable in the quartz rod, free hydrogen is more, the easy production gas in the quartz rod spills over, assemble and form the bubble, make the poor and short problem of life of product high temperature fragility.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, so: all equivalent changes made according to the structure, shape and principle of the invention are covered by the protection scope of the invention.
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