一种三苯基氯甲烷的制备方法

文档序号:1926370 发布日期:2021-12-03 浏览:11次 >En<

阅读说明:本技术 一种三苯基氯甲烷的制备方法 (Preparation method of triphenylchloromethane ) 是由 张露 涂国良 许建跃 靳和平 王甦 胡奇 杨森 刘恒 于 2020-01-06 设计创作,主要内容包括:涉及一种三苯基氯甲烷的制备方法,其包括以下步骤:向三苯基甲醇和有机溶剂的混合液中加入盐酸或盐酸与路易斯酸的混合物,在搅拌条件下反应,反应结束后去除水层,得到含有三苯基氯甲烷的有机溶液;所述方法中,三苯基甲醇的转化率几乎是定量的,高达99%以上,所得产品中,三苯基氯甲烷含量达99%以上;而且操作简便,无废气产生,对环境友好,适合工业化放大,有较好的经济效益。(Relates to a preparation method of triphenylchloromethane, which comprises the following steps: adding hydrochloric acid or a mixture of hydrochloric acid and Lewis acid into a mixed solution of triphenylmethanol and an organic solvent, reacting under a stirring condition, and removing a water layer after the reaction is finished to obtain an organic solution containing triphenylchloromethane; in the method, the conversion rate of the triphenylmethanol is almost quantitative and reaches more than 99 percent, and the content of the triphenylchloromethane in the obtained product reaches more than 99 percent; and the method is simple and convenient to operate, free of waste gas generation, environment-friendly, suitable for industrial amplification and good in economic benefit.)

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