阅读说明：本技术 一种铝合金晶粒细化剂的加入工艺 (Adding process of aluminum alloy grain refiner ) 是由 李彦勤 周建荣 于 2021-07-20 设计创作，主要内容包括：本发明涉及铝板带箔加工领域,具体涉及一种铝合金晶粒细化剂的加入工艺,工艺设备包括保温炉、除气箱、过滤箱和前箱,所述的保温炉出口通过溜槽连接除气箱入口,除气箱出口通过溜槽连接过滤箱入口,过滤箱入口通过溜槽连接前箱入口；通过改变晶粒细化剂的加入位置及加入方式,以此解决传统晶粒细化剂细化效果差的问题,解决了因连续铸轧铝板带材的晶粒细化效果不佳导致的连续铸轧铝板带材原始结晶组织晶粒度差、产品质量不稳定的问题。(The invention relates to the field of aluminum plate strip foil processing, in particular to an adding process of an aluminum alloy grain refiner, which comprises a holding furnace, a degassing tank, a filter tank and a front tank, wherein an outlet of the holding furnace is connected with an inlet of the degassing tank through a chute; by changing the adding position and the adding mode of the grain refiner, the problem of poor refining effect of the traditional grain refiner is solved, and the problems of poor original crystalline structure grain size and unstable product quality of the continuous cast-rolled aluminum plate strip caused by poor refining effect of the grains of the continuous cast-rolled aluminum plate strip are solved.)

1. An adding process of an aluminum alloy grain refiner is characterized in that: the process equipment comprises a holding furnace, a degassing tank, a filter tank and a front tank, wherein an outlet of the holding furnace is connected with an inlet of the degassing tank through a chute; the grain refiner is added at a position on the chute near the outlet of the filter box.

2. The process of claim 1 for adding an aluminum alloy grain refiner, wherein: the device also comprises a stirring device, and the stirring device is arranged on the chute at the position where the grain refiner is added.

Technical Field

The invention relates to the field of aluminum plate strip foil processing, in particular to an adding process of an aluminum alloy grain refiner.

Background

In the continuous casting and rolling process of the aluminum alloy plate strip, as the cooling strength is extremely high and the cooling speed is extremely high, crystals are formed without refining, the quality defect of large and thick crystals is easily formed, and the comprehensive performance of the aluminum plate strip foil material is reduced. In order to improve the coarseness of the crystal grains, the common practice is to refine the crystal grains in the continuous casting and rolling production process. In the continuous casting and rolling production process, the aluminum alloy grain refiner is the most important technical index for ensuring the final qualification and subsequent processing of the continuous casting and rolling aluminum plate strip, and if the original structure of the continuous casting and rolling aluminum plate strip has small grains or the sizes of the grains are not uniform, the quality of the final product of the continuous casting and rolling aluminum plate strip is influenced, and even waste products are generated. At present, most aluminum plate strip deep processing enterprises adopt a mode of adding a grain refiner at the outlet of a degassing tank, and the adding point of the aluminum titanium boron grain refiner is far away from a crystallization area and has larger grain size, so that the grain refiner is not beneficial to the grain refinement of the original structure of the continuous cast-rolled aluminum plate strip. And Ti element in the aluminum alloy grain refiner is easy to deposit, banded structure defects occur, and defective products are generated.

Disclosure of Invention

In order to overcome the problems in the prior art, the invention aims to provide an adding process of an aluminum alloy grain refiner, which solves the problem of poor refining effect of the traditional grain refiner by changing the adding position and the adding mode of the grain refiner, and solves the problems of poor original crystal structure grain size and unstable product quality of continuously cast and rolled aluminum plates and strips caused by poor refining effect of the grains of the continuously cast and rolled aluminum plates and strips.

The technical scheme adopted by the invention is as follows:

the utility model provides an add technology of aluminum alloy grain refiner, includes heat preservation stove, degassing tank, rose box and front box, the heat preservation stove export connect the degassing tank entry through the chute, the degassing tank export passes through the chute and connects the rose box entry, the rose box entry passes through the chute and connects the front box entry, the position of adding of grain refiner is on being close to the chute in rose box exit.

The stirring device is arranged on the chute at the position where the grain refiner is added, the grain refiner added into the chute is uniformly stirred by the stirring device, and meanwhile, the segregation of the grain refiner is avoided, and the product quality is effectively improved.

The adding position of the traditional grain refiner is arranged at the inlet or the outlet of the degassing box, the adding position is far away from the crystallization area of the continuous casting and rolling original structure, the timeliness of the grain refiner of the aluminum plate strip is not favorably brought into full play, and the grain refining effect is poor.

The invention has the beneficial effects that:

1. the adding position of the grain refiner is closer to the original structure crystallization area of the continuously cast and rolled aluminum plate strip, the absorptivity of the aluminum alloy grain refiner is higher, and the timeliness of the aluminum plate strip grain refiner is favorably exerted;

2. by changing the adding position of the grain refiner and additionally arranging a reciprocating stirring device at the adding point, the sedimentary property of Ti element in the grain refiner can be effectively reduced, and the problem of poor grain refining effect of pure aluminum alloy can be greatly solved;

3. the aluminum alloy grain refiner is added according to the process provided by the invention, so that not only can grains be refined, but also the refined grains are uniform in size, the segregation of Ti element in the chemical components of the aluminum alloy is avoided, and the anisotropy of the aluminum alloy plate strip is reduced.

Drawings

FIG. 1 is a flow diagram of the process equipment of the present invention;

FIG. 2 is a macrostructure diagram on an SEM of a grain refiner (A-Ti 5-B1) according to an embodiment of the invention;

FIG. 3 is a high magnification SEM of grain refiner (A-Ti 5-B1) in accordance with an embodiment of the present invention;

FIG. 4 is a cross-sectional microstructure of an embodiment of the present invention after an equivalent amount of grain refiner (A-Ti 5-B1) is added at the inlet of the filter box and the cast-rolled primary structure is refined;

FIG. 5 is a cross-sectional microstructure diagram of a cast-rolled original structure after an equal amount of grain refiner (A-Ti 5-B1) is added at the outlet of a filter box in the embodiment of the invention and the original structure is refined.

Detailed Description

The invention is described in detail below with reference to the following figures and detailed description:

fig. 1 shows a flow chart of a process equipment for adding a grain refiner, and a test method in a TP-1 type grain size test standard formulated by the international Aluminum Association (Aluminum Association) is adopted to compare grain refining effects of grain refiners of the same Aluminum alloy at different adding positions.

Fig. 2 and 3 are microstructure diagrams of an aluminum alloy grain refiner (a-Ti 5-B1) provided by a supplier, wherein a longitudinal section of the aluminum alloy grain refiner supplied by the supplier is cut, ground and polished, and then rubbed and etched by using a w (HF) =0.5% HF aqueous solution, and fig. 2 and 3 are microstructure diagrams of low-power and high-power structures observed on SEM.

According to the normal production process of the continuous cast-rolled plate and strip, if the solid material proportion, the refining medium and the refining frequency are the same, the degassing box and the filter box with the same type are used, the comparison test is carried out on the high-power structure of the 1060 aluminum alloy deep drawing product by using the same aluminum alloy grain refiner and different adding positions, after the aluminum alloy grain refiner is added at the same adding amount and different adding positions to refine the cast-rolled original structure, the cross section microstructure condition is shown in figures 4 and 5, and the obvious results can be obtained through figures 4 and 5, when the grain refiner is added between the degassing box outlet and the front box chute, the refining effect is obvious, the grains are fine and smooth, the distribution is uniform, and the Ti element segregation phenomenon does not exist.